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    • 1. 发明公开
    • METHOD FOR ISOLATING CELLULOSE FROM A BIOMASS AND PRODUCTS PROVIDED THEREFROM
    • 从生物体中分离纤维素的方法和由此提供的产品
    • EP3177768A1
    • 2017-06-14
    • EP15830054.1
    • 2015-02-11
    • Green Extraction Technologies, Inc.
    • MITCHELL, Melvin Glenn
    • D21H11/16C08B15/08C12P19/04
    • C08H6/00C08B15/08C08B37/0057C08G63/06C08G63/912C08H8/00D21C1/02D21C3/02D21C3/224D21H11/00
    • A pretreated biomass is subjected to high frequency pulses and shear forces without denaturing and/or degrading the individual components of the biomass. The biomass is then subjected to compressive force to separate a first liquid fraction from a first fractionated biomass. The first fractionated biomass may again then be subjected to the same high frequency pulses and shear forces as previously, particularly if there are hemicellulose and/or sugars still present in the first fractionated biomass. Compressive forces are used to separate a second liquid fraction from a second fractionated biomass. The second fractionated biomass is subjected to oxidation. The second fractioned biomass is then subjected to compressive forces to separate out one or more water insoluble components of the biomass in water soluble form and to provide cellulose that has not been denatured and/or degraded and has a lignin contact of less than 7 percent.
    • 预处理的生物质经受高频脉冲和剪切力而不会使生物质的各个组分变性和/或降解。 然后使生物质经受压缩力以从第一分馏生物质中分离出第一液体部分。 第一分级生物质可再次经受与先前相同的高频脉冲和剪切力,特别是如果在第一分级生物质中仍存在半纤维素和/或糖。 使用压缩力从第二分馏生物质分离第二液体部分。 第二分馏生物质经受氧化。 然后使第二分馏生物质经受压缩力以分离出水溶性形式的生物质的一种或多种水不溶性组分并提供未变性和/或降解并且具有小于7%的木质素接触的纤维素。
    • 7. 发明公开
    • METHOD FOR ISOLATING LIGNIN FROM A BIOMASS AND PRODUCTS PROVIDED THEREFROM
    • 从生物体中分离木质素的方法和由此提供的产品
    • EP3180300A1
    • 2017-06-21
    • EP15829162.5
    • 2015-02-11
    • Green Extraction Technologies, Inc.
    • MITCHELL, Melvin Glenn
    • C07C37/54F15D1/00
    • C08H6/00C08B15/08C08B37/0057C08G63/06C08G63/912C08H8/00D21C1/02D21C3/02D21C3/224D21H11/00
    • The process includes pretreating the biomass to provide a fluidized biomass. The fluidized biomass is then subjected to high frequency pulses and shear forces without denaturing/degrading the individual components of the biomass. The biomass is then subjected to compressive force to separate a first liquid fraction from a first fractionated biomass. The first fractionated biomass may again then be subjected to the same high frequency pulses and shear forces as previously, particularly if there are hemicellulose and/or sugars still present in the first fractionated biomass. Compressive forces are used to separate a second liquid fraction from a second fractionated biomass. The second fractionated biomass is subjected to oxidation such as with hydrogen peroxide and base at a pH above 7. The second fractioned biomass is then subjected to compressive forces to provide water soluble lignin which may be precipitated by reducing the pH.
    • 该方法包括用第一种碱性溶液如氢氧化钠预处理生物质,并机械地改变纤维以提供流化的生物质。 然后使流化的生物质经受高频脉冲和剪切力,而不使生物质的各个组分变性。 然后使生物质经受压缩力以从第一分馏生物质中分离出第一液体部分。 第一分级生物质可再次经受与先前相同的高频脉冲和剪切力,特别是如果在第一分级生物质中仍存在半纤维素和/或糖。 使用压缩力从第二分馏生物质分离第二液体部分。 第二分级生物质例如用8-12的pH值的过氧化氢进行氧化。然后对第二分级生物质施加压缩力以分离水溶性形式的生物质的一种或多种水不溶性组分。
    • 8. 发明公开
    • VERFAHREN ZUR GEWINNUNG VON CELLULOSE
    • EP3024974A1
    • 2016-06-01
    • EP14744103.4
    • 2014-07-25
    • Fülling, Rainer
    • SCHLABACH, HeikoFÜLLING, Rainer
    • D21C1/10C08H8/00D21C7/00D21C7/14D21C11/00D21C11/04C08L97/02C02F9/00D21C5/02C12P7/10
    • D21C3/02C08B1/00C08H8/00C08L1/02C08L97/02D21C1/10D21C3/224D21C5/02D21C7/00D21C7/14D21C9/08D21C11/00D21C11/04Y02E50/16Y02W30/648
    • The present invention relates to a process for obtaining cellulose or a mixture containing at least cellulose and at least lignocellulose from at least one substrate that is at least to some extent amenable to fermentation comprising at least the steps of (1) to (3) and optionally (4), namely conversion of the substrate via addition of at least one inorganic base into an aqueous mixture with pH ≥ 8.5 (step 1), ultrasound treatment of the aqueous mixture obtained after step (1) (step 2), separation of the aqueous mixture obtained after step (2) into a liquid aqueous phase and a disperse mixture containing cellulose or a mixture containing at least cellulose and at least lignocellulose (step 3) and optionally purification of the disperse mixture obtained after step (3) containing cellulose or of the mixure containing at least cellulose and at least lignocellulose (step 4), where step (1) and step (2) of the process respectively are carried out at a temperature
    • 本发明涉及一种获得纤维素或至少含有纤维素和至少一种木质纤维素的混合物的方法,该至少一种底物至少在一定程度上适于发酵,其包括至少步骤(1)至(3)和 任选地(4),即通过将至少一种无机碱加入到具有pH≥8.5(步骤1)的水性混合物中的底物的转化,超声处理在步骤(1)(步骤2)之后获得的含水混合物,分离 步骤(2)中获得的含水混合物加入到液体水相中,以及含有至少纤维素和至少木质纤维素(步骤3)的纤维素或混合物的分散混合物,并任选地纯化在步骤(3)之后获得的分散混合物, 纤维素或至少含有纤维素和至少木质纤维素的混合物(步骤4),其中该方法的步骤(1)和步骤(2)分别在<100℃的温度下进行,其中u 步骤(2)中的超声处理在一个或多个处理阶段进行,其中处理阶段的瓷砖持续时间在0.2至60秒的范围内,并且每个处理阶段以超声波频率在14至22范围内进行 千赫。