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1. 发明公开

EP0243509A1 Process for the preparation of a mesophase pitch for preparing carbon fibres 失效
标题翻译： Verfahren zur Herstellung von mesophasern Pechfürdie Erzeugung von Kohlenstofffasern。
公开(公告)号：EP0243509A1
公开(公告)日：1987-11-04
申请号：EP86104841.1
申请日：1986-04-09
申请人： MARUZEN PETROCHEMICAL CO., LTD.
发明人： Tsuchitani, Masatoshi , Nakajima, Ryoichi
IPC分类号： C10C3/06 , C10C1/16 , D01F9/14
CPC分类号： C10C1/08 , C10C1/16 , C10C1/19 , C10C3/002 , C10C3/06 , D01F9/145
摘要： Until now, it has not yet been succeeded to prepare high performance carbon fibers having satisfactory strength from heavy oils of coal or petroleum origin. We now succeeded to prepare an excellent itnermediate pitch which allows the preparation of high performance carbon fibers having tensile strength of higher than 300 Kg/mm² and Young's modulus of 50 ton/mm².
The intermediate pitch can be obtained by heating a heavy oil of coal or petroleum origin in a tubular heater under a specific conditions, and then flash distilling the heater effluent in a flash distillation column under a specific condition so as to remove lighter fractions and recovering heavy fraction from the column bottom as the intermediate pitch. The process for the preparation of the intermediate pitch is simple and economical and allows continuous production without fluctuation of quality of the intermediate pitch. The intermediate pitch is also suitable for the production of higher density carbon products.
摘要翻译：迄今尚未成功制备具有令人满意的煤或石油来源重油的高性能碳纤维。我们现在可以成功制备出优良的中纬节距，可以制备抗拉强度高于300Kg / mm2，杨氏模量为50吨/平方毫米的高性能碳纤维。中间沥青可以通过在特定条件下在管状加热器中加热煤或石油来源的重油，然后在特定条件下将闪蒸蒸馏塔中的加热器流出物闪蒸，以除去较轻馏分并重新沉积从柱底部的分数作为中间间距。制备中间沥青的方法简单经济，可连续生产，而不会造成中间沥青质量的波动。中间沥青也适用于生产高密度碳产品。

2. 发明授权

EP1490455B1 A PROCESS FOR OBTAINING HIGH PURITY PHENANTHRENE AND A SYSTEM THEREOF 有权
标题翻译：一种获得高纯度菲及其装置
公开(公告)号：EP1490455B1
公开(公告)日：2007-07-25
申请号：EP02714411.2
申请日：2002-03-27
申请人： Council of Scientific and Industrial Research;an Indian Reg. body incorporated under Reg. of Societies Act (Act XXI of 1860)
发明人： TIWARI,Kaushal,Kishore , RAO,Sukuru,Ramakrishna Central Fuel Research Inst. , THAKUR,Sanjay,Kumar Central Fuel Research Inst. , BANERJI, Somnath Central Fuel Research Institute
IPC分类号： C10C1/08 , C07C15/30 , B01D3/14 , C07C7/04
CPC分类号： C10C1/08 , B01D3/14 , B01D3/322 , C07C7/04 , C07C15/30
摘要： The present invention relates to a system and a process for obtaining phenanthrene of about 95 % purity fromcoal tar distilled fraction containing crude phenanthrene by performing fractional distillation at a reduced pressure of 50 mm mercury and at a temperature range of 160-180 °C to obtain first distilled fraction containing acenaphthene and fluorene; a second distillate fraction at a temperature range of 200-230 °C containing phenanthrene, anthracene and traces of carbazole; followed by re-distilling the second distillate fraction at a temperature range of 210-224 °C to finally obtain pure phenanthrene and a residue which is again used for the recovery of residual phenanthrene by re-distillation at a temperature range of 210-224 °C.

3. 发明授权

EP0198471B1 Method of purifying the starting material for use in the production of carbon products 失效
标题翻译：净化用于生产碳产品的起始材料的方法
公开(公告)号：EP0198471B1
公开(公告)日：1989-11-23
申请号：EP86105174.6
申请日：1986-04-15
申请人： MARUZEN PETROCHEMICAL CO., LTD.
发明人： Tsuchitani, Masatoshi , Naito, Sakae
IPC分类号： C10C1/18
CPC分类号： C10C1/08 , C10C1/18

4. 发明公开

EP1490455A1 A PROCESS FOR OBTAINING HIGH PURITY PHENANTHRENE AND A SYSTEM THEREOF 有权
标题翻译：一种获得高纯度菲及其装置
公开(公告)号：EP1490455A1
公开(公告)日：2004-12-29
申请号：EP02714411.2
申请日：2002-03-27
申请人： Council of Scientific and Industrial Research;an Indian Reg. body incorporated under Reg. of Societies Act (Act XXI of 1860)
发明人： TIWARI,Kaushal,KishoreCentral Fuel Research Inst. , RAO,Sukuru,RamakrishnaCentral Fuel Research Inst. , THAKUR,Sanjay,KumarCentral Fuel Research Inst. , BANERJI, SomnathCentral Fuel Research Institute
IPC分类号： C10C1/08 , C07C15/30 , B01D3/14 , C07C7/04
CPC分类号： C10C1/08 , B01D3/14 , B01D3/322 , C07C7/04 , C07C15/30
摘要： The present invention relates to a system and a process for obtaining phenanthrene of about 95 % purity fromcoal tar distilled fraction containing crude phenanthrene by performing fractional distillation at a reduced pressure of 50 mm mercury and at a temperature range of 160-180 °C to obtain first distilled fraction containing acenaphthene and fluorene; a second distillate fraction at a temperature range of 200-230 °C containing phenanthrene, anthracene and traces of carbazole; followed by re-distilling the second distillate fraction at a temperature range of 210-224 °C to finally obtain pure phenanthrene and a residue which is again used for the recovery of residual phenanthrene by re-distillation at a temperature range of 210-224 °C.

5. 发明授权

EP0465434B1 Distilled, fractional and rectified coal tar oil for ecologically impregnating wood 失效
$Distilled, fractional and rectified coal tar oil for ecologically impregnating wood$
标题翻译：蒸馏，分馏和纠正煤焦油为生态木浸渍。
公开(公告)号：EP0465434B1
公开(公告)日：1995-09-20
申请号：EP91830209.2
申请日：1991-05-20
申请人： MARGARITELLI - S.P.A.
发明人： Margaritelli, Giuseppe
IPC分类号： B27K3/46 , C10C1/08
CPC分类号： B27K3/46 , C10C1/08

6. 发明公开

EP0198471A3 Method of purifying the starting material for use in the production of carbon products 失效
标题翻译：净化用于生产碳产品的起始材料的方法
公开(公告)号：EP0198471A3
公开(公告)日：1987-05-27
申请号：EP86105174
申请日：1986-04-15
申请人： MARUZEN PETROCHEMICAL CO., LTD.
发明人： Tsuchitani, Masatoshi , Naito, Sakae
IPC分类号： C10C01/18
CPC分类号： C10C1/08 , C10C1/18
摘要： The unwanted components from coal tars should be removed at a certain stage of the process for producing homogeneous spinning pitches which are suitable for use in the production of high-performance carbon fibers from coal tars. The unwanted components can be eliminated from coal tars in a very efficient manner by the following procedures: subjecting the coal tars to distillation or flash distillation so as to separate a heavy component having a boiling point higher than a predetermined temperature, dissolving the heavy component in a monocyclic aromatic hydrocarbon solvent, and subjecting the solution to'filtration or centrifugation.

7. 发明公开

EP0465434A1 Distilled, fractional and rectified coal tar oil for ecologically impregnating wood 失效
$Distilled, fractional and rectified coal tar oil for ecologically impregnating wood$
标题翻译： Destilliertes，fraktioniertes und rektifiziertesSteinkohlenteerölzurökologischenHolzimprägnierung。
公开(公告)号：EP0465434A1
公开(公告)日：1992-01-08
申请号：EP91830209.2
申请日：1991-05-20
申请人： MARGARITELLI - S.P.A.
发明人： Margaritelli, Giuseppe
IPC分类号： B27K3/46 , C10C1/08
CPC分类号： B27K3/46 , C10C1/08
摘要： The present invention regards a distilled, fractional and rectified coal tar oil for the ecological impregnation of wood characterized by the fact that it is the product of column rectification of naphthalene oil carried out at a temperature ranging from between 230xc and 330xC.
摘要翻译：本发明涉及一种用于生态浸渍木材的蒸馏，分馏和精馏的焦油油，其特征在于它是在230℃至330℃之间的温度范围内进行萘油的柱精馏的产物。

8. 发明授权

EP0243509B1 Process for the preparation of a mesophase pitch for preparing carbon fibres 失效
标题翻译：制备用于制备碳纤维的MESOPHASE PITCH的方法
公开(公告)号：EP0243509B1
公开(公告)日：1990-08-08
申请号：EP86104841.1
申请日：1986-04-09
申请人： MARUZEN PETROCHEMICAL CO., LTD.
发明人： Tsuchitani, Masatoshi , Nakajima, Ryoichi
IPC分类号： C10C3/06 , C10C1/16 , D01F9/14
CPC分类号： C10C1/08 , C10C1/16 , C10C1/19 , C10C3/002 , C10C3/06 , D01F9/145

9. 发明公开

EP0198471A2 Method of purifying the starting material for use in the production of carbon products 失效
标题翻译：一种用于纯化中使用的起始原料的煤产品的制造方法。
公开(公告)号：EP0198471A2
公开(公告)日：1986-10-22
申请号：EP86105174.6
申请日：1986-04-15
申请人： MARUZEN PETROCHEMICAL CO., LTD.
发明人： Tsuchitani, Masatoshi , Naito, Sakae
IPC分类号： C10C1/18
CPC分类号： C10C1/08 , C10C1/18
摘要： The unwanted components from coal tars should be removed at a certain stage of the process for producing homogeneous spinning pitches which are suitable for use in the production of high-performance carbon fibers from coal tars. The unwanted components can be eliminated from coal tars in a very efficient manner by the following procedures: subjecting the coal tars to distillation or flash distillation so as to separate a heavy component having a boiling point higher than a predetermined temperature, dissolving the heavy component in a monocyclic aromatic hydrocarbon solvent, and subjecting the solution to'filtration or centrifugation.

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