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1. 发明公开

EP2778130A4 NANO-SILICON/CARBON COMPOSITE MATERIAL AND PREPARATION METHOD THEREFOR 有权转让
标题翻译：纳米硅/炭复合材料及其制造方法
公开(公告)号：EP2778130A4
公开(公告)日：2015-07-29
申请号：EP12848316
申请日：2012-11-09
申请人： GEN RES INST NONFERROUS METALS
发明人： LU SHIGANG , YANG JUANYU , WANG XINGMING , DING HAIYANG , GAO ZHEFENG
IPC分类号： C01B31/36 , B82Y30/00 , C25B1/00 , H01M4/04 , H01M4/1393 , H01M4/1395 , H01M4/36 , H01M4/38 , H01M4/48 , H01M4/58 , H01M4/587 , H01M10/052
CPC分类号： H01M4/364 , B82Y30/00 , C01B32/956 , C25B1/006 , H01M4/0438 , H01M4/1393 , H01M4/1395 , H01M4/386 , H01M4/483 , H01M4/58 , H01M4/587 , H01M10/052

2. 发明公开

EP2778130A1 NANO-SILICON/CARBON COMPOSITE MATERIAL AND PREPARATION METHOD THEREFOR 有权转让
标题翻译： NERSO-SILIUM - / KOHLENSTOFFVERBUNDMATERIAL UND HERSTELLUNGSVERFAHRENDAFÜR
公开(公告)号：EP2778130A1
公开(公告)日：2014-09-17
申请号：EP12848316.1
申请日：2012-11-09
申请人： General Research Institute For Nonferrous Metals
发明人： LU, Shigang , YANG, Juanyu , WANG, Xingming , DING, Haiyang , GAO, Zhefeng
IPC分类号： C01B31/36 , H01M4/36
CPC分类号： H01M4/364 , B82Y30/00 , C01B32/956 , C25B1/006 , H01M4/0438 , H01M4/1393 , H01M4/1395 , H01M4/386 , H01M4/483 , H01M4/58 , H01M4/587 , H01M10/052
摘要： The invention relates to a nano silicon-carbon composite negative material for lithium ion batteries and a preparation method thereof. A porous electrode composed of silica and carbon is taken as a raw material, and a nano silicon-carbon composite material of carbon-loaded nano silicon is formed by a molten salt electrolysis method in a manner of silica in-situ electrochemical reduction. Silicon and carbon of the material are connected by nano silicon carbide, and are metallurgical-grade combination, so that the electrochemical cycle stability of the nano silicon-carbon composite material is improved. The preparation method of the nano silicon-carbon composite material provided by the invention comprises the following steps: compounding a porous block composed of carbon and silica powder with a conductive cathode collector as a cathode; using graphite or an inert anode as an anode, and putting the cathode and anode into CaCl 2 electrolyte or mixed salt melt electrolyte containing CaCl 2 to form an electrolytic cell; applying voltage between the cathode and the anode; controlling the electrolytic voltage, the electrolytic current density and the electrolytic quantity, so that silica in the porous block is deoxidized into nano silicon by electrolytic reduction, and the nano silicon-carbon composite material for lithium ion batteries is prepared at the cathode.
摘要翻译：本发明涉及一种用于锂离子电池的纳米硅碳复合负极材料及其制备方法。将由二氧化硅和碳组成的多孔电极作为原料，以二氧化硅原位电化学还原的方式通过熔融盐电解法形成含碳纳米硅的纳米硅 - 碳复合材料。材料的硅和碳通过纳米碳化硅连接，并且是冶金级组合，从而提高纳米硅 - 碳复合材料的电化学循环稳定性。本发明提供的纳米硅 - 碳复合材料的制备方法包括以下步骤：将由碳和二氧化硅粉末组成的多孔块与导电阴极集电体作为阴极复合; 使用石墨或惰性阳极作为阳极，并将阴极和阳极放入含CaCl 2的电解质或含有CaCl 2的混合盐熔融电解质中以形成电解槽; 在阴极和阳极之间施加电压; 控制电解电压，电解电流密度和电解量，使多孔块中的二氧化硅通过电解还原脱氧成纳米硅，并在阴极制备用于锂离子电池的纳米硅 - 碳复合材料。

3. 发明授权

EP2343403B1 ELECTROCHEMICAL METHOD FOR MANUFACTURING ONE OR MORE OF SILICON NANOWIRE AND SILICON NANOTUBE 有权转让
标题翻译：电化学方法制造一个或多个硅纳米线和硅纳米管
公开(公告)号：EP2343403B1
公开(公告)日：2018-04-25
申请号：EP09824414.8
申请日：2009-11-05
申请人： China Automotive Battery Research Institute Co, Ltd.
发明人： LU, Shigang , YANG, Juanyu , ZHANG, Xiangjun , KAN, Surong
IPC分类号： C25B1/00 , C01B33/021 , C30B9/14 , C30B29/06 , C30B29/60
CPC分类号： C25B1/006 , C01B33/021 , C30B9/14 , C30B29/06 , C30B29/60 , Y10S977/762 , Y10S977/814 , Y10S977/899
摘要： The present invention provides an electrochemical method for producing Si nanopowder, Si nanowires and/or Si nanotubes directly from compound SiX or a mixture containing compound SiX, wherein the method comprises: the compound SiX or the mixture containing compound SiX is used as cathode and immersed in an electrolyte comprising a metal compound molten salt, a cathodic potential is applied to electrolyse, and then one or more of Si nanopowder, Si nanowires and Si nanotubes are formed on the cathode electrode. The method of the present invention has advantages as follows: 1) shorter production processing, 2) inexpensive equipment, 3) convenient operation, 4) reduction of contaminants, 5) easily available feed materials, and 6) easy to achieve continuous production. It inaugurates a new field of using electrochemical method for producing one-dimensional Si nanomaterial, and offers a new way of producing Si nanopowder, Si nanowires and Si nanotubes.

4. 发明授权

EP2778130B1 NANO-SILICON/CARBON COMPOSITE MATERIAL AND PREPARATION METHOD THEREFOR 有权转让
标题翻译：纳米硅/碳复合材料及其制备方法
公开(公告)号：EP2778130B1
公开(公告)日：2017-10-11
申请号：EP12848316.1
申请日：2012-11-09
申请人： China Automotive Battery Research Institute Co, Ltd.
发明人： LU, Shigang , YANG, Juanyu , WANG, Xingming , DING, Haiyang , GAO, Zhefeng
IPC分类号： H01M4/36 , C25B1/00 , H01M4/04 , H01M4/38 , H01M4/48 , H01M4/58 , H01M4/587 , B82Y30/00 , H01M4/1393 , H01M4/1395 , H01M10/052
CPC分类号： H01M4/364 , B82Y30/00 , C01B32/956 , C25B1/006 , H01M4/0438 , H01M4/1393 , H01M4/1395 , H01M4/386 , H01M4/483 , H01M4/58 , H01M4/587 , H01M10/052

5. 发明公开

EP2343403A4 ELECTROCHEMICAL METHOD FOR MANUFACTURING ONE OR MORE OF SILICON NANOPOWDER, SILICON NANOWIRE AND SILICON NANOTUBE 有权转让
标题翻译：电化学过程用于生产一种或更多的硅纳米粉，硅纳米线和硅纳米管
公开(公告)号：EP2343403A4
公开(公告)日：2016-06-08
申请号：EP09824414
申请日：2009-11-05
申请人： GEN RES INST FOR NONFERROUS METALS BEIJNG
发明人： LU SHIGANG , YANG JUANYU , ZHANG XIANGJUN , KAN SURONG
IPC分类号： C30B29/06 , C01B33/023 , C25B1/00 , C30B29/60
CPC分类号： C25B1/006 , C01B33/021 , C30B9/14 , C30B29/06 , C30B29/60 , Y10S977/762 , Y10S977/814 , Y10S977/899
摘要： The present invention provides an electrochemical method for producing Si nanopowder, Si nanowires and/or Si nanotubes directly from compound SiX or a mixture containing compound SiX, wherein the method comprises: the compound SiX or the mixture containing compound SiX is used as cathode and immersed in an electrolyte comprising a metal compound molten salt, a cathodic potential is applied to electrolyse, and then one or more of Si nanopowder, Si nanowires and Si nanotubes are formed on the cathode electrode. The method of the present invention has advantages as follows: 1) shorter production processing, 2) inexpensive equipment, 3) convenient operation, 4) reduction of contaminants, 5) easily available feed materials, and 6) easy to achieve continuous production. It inaugurates a new field of using electrochemical method for producing one-dimensional Si nanomaterial, and offers a new way of producing Si nanopowder, Si nanowires and Si nanotubes.

6. 发明公开

EP2343403A1 ELECTROCHEMICAL METHOD FOR MANUFACTURING ONE OR MORE OF SILICON NANOPOWDER, SILICON NANOWIRE AND SILICON NANOTUBE 有权转让
标题翻译：电化学过程用于生产一种或更多的硅纳米粉，硅纳米线和硅纳米管
公开(公告)号：EP2343403A1
公开(公告)日：2011-07-13
申请号：EP09824414.8
申请日：2009-11-05
申请人： General Research Institute For Nonferrous Metals, Beijng
发明人： LU, Shigang , YANG, Juanyu , ZHANG, Xiangjun , KAN, Surong
IPC分类号： C30B29/06 , C30B29/60 , C25B1/00 , C01B33/023
CPC分类号： C25B1/006 , C01B33/021 , C30B9/14 , C30B29/06 , C30B29/60 , Y10S977/762 , Y10S977/814 , Y10S977/899
摘要： The present invention provides an electrochemical method for producing Si nanopowder, Si nanowires and/or Si nanotubes directly from compound SiX or a mixture containing compound SiX, wherein the method comprises: the compound SiX or the mixture containing compound SiX is used as cathode and immersed in an electrolyte comprising a metal compound molten salt, a cathodic potential is applied to electrolyse, and then one or more of Si nanopowder, Si nanowires and Si nanotubes are formed on the cathode electrode. The method of the present invention has advantages as follows: 1) shorter production processing, 2) inexpensive equipment, 3) convenient operation, 4) reduction of contaminants, 5) easily available feed materials, and 6) easy to achieve continuous production. It inaugurates a new field of using electrochemical method for producing one-dimensional Si nanomaterial, and offers a new way of producing Si nanopowder, Si nanowires and Si nanotubes.
摘要翻译：对本发明的电化学方法提供了一种生产硅纳米粉末，Si纳米线和/或Si，从化合物的SiX或含有化合物的SiX的混合物直接纳米管，worin该方法包括：化合物的SiX或含有化合物的SiX的混合物用作阴极，并浸入在电解质包含金属化合物的熔融盐，在阴极电位被施加到电解，然后一个或更多的Si纳米粉末，Si纳米线和Si纳米管上的阴极电极上形成。本发明的方法具有以下优点：1）更短的生产加工，2）廉价的设备，3）方便手术，4）减少污染物的，5）容易获得的进料，以及6）容易实现连续生产。它开创采用电化学的制造方法的一维的Si纳米材料的一个新的领域，并提供产硅纳米粉末，Si纳米线和Si纳米管的新方法。

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