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1. 发明公开

EP3275835A1 ONLINE FURNACE DRYING METHOD FOR HEAT-INSULATION NATURAL GAS CATALYTIC OXIDIZING FURNACE 审中-公开
标题翻译：保温天然气催化氧化炉在线烘干方法
公开(公告)号：EP3275835A1
公开(公告)日：2018-01-31
申请号：EP16767645.1
申请日：2016-02-26
申请人： Wuhan Kaidi Engineering Technology Research Institute Co., Ltd.
发明人： CHEN, Yilong , ZHANG, Yanfeng , KUAI, Pingyu , TIAN, Wentang , WANG, Daxiang
IPC分类号： C01B3/38 , C01B31/18
CPC分类号： C01B3/40 , C01B3/386 , C01B32/40 , C01B2203/0261 , C01B2203/1017 , C01B2203/1082 , C01B2203/1241 , C01B2203/1614 , C01B2203/169
摘要： Disclosed is an online furnace drying method for a heat-insulation natural gas catalytic oxidizing furnace, comprising: (1) simultaneously introducing oxygen, natural gas and temperature-control gas capable of decreasing a reaction heating rate into a natural gas catalytic oxidizing furnace, controlling a molar ratio of the oxygen to the natural gas at (0.3-0.6): 1, and meanwhile, controlling a molar ratio of the temperature-control gas to raw material gas consisting of the oxygen and the natural gas at (0.1-7):(1.3-1.6); (2) preheating the mixed gas so as to gradually increase the temperature, and stopping the preheating until the temperature reaches an oxidation triggering temperature; and (3) gradually decreasing the molar ratio of the temperature-control gas to the raw material gas, allowing the reaction temperature to increase at a heating rate meeting the requirement of a designed furnace drying curve, and stopping the introduction of the temperature-control gas until the reaction temperature reaches a working temperature. The present invention solves the problem that the temperature rises excessively fast during the furnace heating process, prevents a heat-insulation fire-resisting material from being cracked due to shock heating, and protects the natural gas catalytic oxidizing furnace, so that the natural gas catalytic oxidizing furnace can be stably transitioned to a normal operation state.
摘要翻译：本发明公开了一种用于隔热天然气催化氧化炉的在线炉干燥方法，其包括：（1）同时将能够降低反应升温速率的氧气，天然气和温度控制气体引入天然气催化氧化炉，控制（0.3-0.6）:1的氧气与天然气的摩尔比，同时控制温度控制气体与氧气和天然气组成的原料气体在（0.1-7）的摩尔比，：（1.3-1.6）; （2）预热混合气体以逐渐升高温度，并停止预热直到温度达到氧化触发温度; （3）逐渐降低温度控制气体与原料气体的摩尔比，使反应温度以满足设计炉干燥曲线要求的升温速率升高，并停止引入温度控制气体直至反应温度达到工作温度。本发明解决了炉内加热过程中温度过快上升，防止隔热耐火材料因加热冲击而破裂，保护天然气催化氧化炉的问题，使天然气催化氧化炉可以稳定地转换到正常运行状态。

2. 发明公开

EP3309238A1 CHLORALKALI METHOD AND FISCHER-TROPSCH SYNTHESIS INTEGRATED UTILIZATION ADJUSTMENT PROCESS AND EQUIPMENT THEREFOR 审中-公开
标题翻译：氯代卡利法和费歇尔合成综合利用调整过程及其设备
公开(公告)号：EP3309238A1
公开(公告)日：2018-04-18
申请号：EP16806600.9
申请日：2016-04-15
申请人： Wuhan Kaidi Engineering Technology Research Institute Co., Ltd.
发明人： WANG, Daxiang , KUAI, Pingyu , LI, Meng , ZHANG, Yanfeng
IPC分类号： C10G2/00 , C01B3/52 , C01B3/04 , C10J3/00 , C10J3/84 , C10J3/48
CPC分类号： C10G2/34 , C01B3/04 , C01B3/52 , C10G2/00 , C10G2/35 , C10G2/50 , C10J3/00 , C10J3/48 , C10J3/84 , C10J2300/0916 , C10J2300/093 , C10J2300/0946 , C10J2300/1659 , C10K1/005 , C10K1/122 , C10K1/32 , C25B1/34 , C25B15/08 , Y02E50/32 , Y02E60/364
摘要： Provided are a chloralkali method and Fischer-Tropsch synthesis integrated utilization adjustment process and an equipment therefor. The process includes: 1) gasifying a gasification feedstock for the Fischer-Tropsch synthesis to obtain a crude synthesis gas with the main components being H 2 , CO and CO 2 ; 2) electrolyzing a saturated NaCl solution by using a conventional industrial chloralkali method to obtain a NaOH solution, Cl 2 and H 2 ; and 3) using the NaOH solution and H 2 prepared by the chloralkali method for removing CO 2 in the crude synthesis gas to obtain a pure synthesis gas and adjusting the molar ratio of carbon to hydrogen in the pure synthesis gas, respectively, so that the pure synthesis gas reaches the requirements for a feeding gas of the Fischer-Tropsch synthesis. The equipment includes a gasification apparatus, a chloralkali method electrolyzer, a gas-washing apparatus and a Fischer-Tropsch synthesis reactor. By organically combining the chloralkali method and the Fischer-Tropsch synthesis process, and using the hydrogen gas produced by the chloralkali method to adjust the composition of the pure synthesis gas, the treating amount of the water-gas shift process is reduced and the working procedure is simplified.
摘要翻译：提供了一种氯碱法和费托合成综合利用调整工艺及其设备。该方法包括：1）气化费 - 托合成的气化原料以获得主要组分为H 2，CO和CO 2的粗合成气; 2）采用常规工业氯碱法电解饱和NaCl溶液，得到NaOH溶液Cl2和H2; 3）采用NaOH溶液和氯碱法制备的H 2分别除去粗合成气中的CO 2，得到纯合成气，分别调整纯合成气中碳氢摩尔比，得到纯合成气气体达到费 - 托合成的进料气的要求。该设备包括气化装置，氯碱法电解槽，气体清洗装置和费 - 托合成反应器。通过将氯碱法和费 - 托合成法有机地结合起来，利用氯碱法生产的氢气调节纯合成气的组成，减少了水煤气变换工艺的处理量，工序被简化。

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