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1. 发明公开

EP2966107A1 BLOCK COPOLYMER AND PRODUCTION METHOD FOR SAME 审中-公开
标题翻译： BLOCKCOPOLYMER UND HERSTELLUNGSVERFAHRENDAFÜR
公开(公告)号：EP2966107A1
公开(公告)日：2016-01-13
申请号：EP14759952.6
申请日：2014-03-05
申请人： Toray Industries, Inc.
发明人： ICHINOSE, Keiko , YOKOE, Makito , YAMAMOTO, Daisuke , YAMAUCHI, Koji , YAMASHITA, Kohei
IPC分类号： C08G63/688 , C08G64/18 , C08G65/26 , C08G69/14 , C08G75/00 , C08G75/06 , C08G81/00
CPC分类号： C08G81/00 , C08G69/14 , C08G69/42 , C08G69/48 , C08G75/14 , C08G2261/126 , C08G2650/40 , C08L71/00 , C08L81/02
摘要： A block comprised of a copolymer is obtained by ring-opening polymerization of a cyclic polyarylene sulfide, so that a block copolymer is produced to have a maximum peak molecular weight measured by size exclusion chromatography (SEC) in a range of not less than 2,000 and less than 2,000,000 and have a unimodal molecular weight distribution in this range.
摘要翻译：通过环状聚芳硫醚的开环聚合获得共聚物的嵌段，从而制得嵌段共聚物，其具有通过尺寸排阻色谱法（SEC）测定的最大峰分子量在2000以上的范围内，小于200万，在此范围内具有单峰分子量分布。

2. 发明公开

EP2065410A1 PROCESS FOR PRODUCTION OF THERMOPLASTIC COPOLYMER 审中-公开
标题翻译： VERFAHREN ZUR HERSTELLUNG VON热塑性共聚物
公开(公告)号：EP2065410A1
公开(公告)日：2009-06-03
申请号：EP07807192.5
申请日：2007-09-13
申请人： Toray Industries, Inc.
发明人： YAMAMOTO, Daisuke , SUDO, Ken , TAKAMURA, Hajime , YAMASHITA, Taro , YAMAUCHI, Koji , MATSUMOTO, Hideki , UTAZAKI, Kenichi
IPC分类号： C08F220/12 , C08F8/48 , C08F220/04
CPC分类号： C08F220/14 , C08F8/44 , C08F8/48 , C08F220/06 , C08F2800/20 , C08F2810/20 , C08F2810/30 , C08F2220/1825 , C08F265/06
摘要： A process for continuously producing a thermoplastic copolymer, in which a copolymer (A) containing unsaturated carboxylic acid alkyl ester units and unsaturated carboxylic acid units is produced and in succession heat-treated to perform intramolecular cyclization reaction by dehydration and/or dealcoholization reaction, for producing a thermoplastic copolymer (B) containing glutaric anhydride units and the unsaturated carboxylic acid alkyl ester units. The obtained copolymer is excellent in heat resistance and colorless transparency and very small in foreign matter content.
摘要翻译：一种连续制造热塑性共聚物的方法，其中制备含有不饱和羧酸烷基酯单元和不饱和羧酸单元的共聚物（A），并连续热处理以通过脱水和/或脱醇反应进行分子内环化反应，用于制备含有戊二酸酐单元和不饱和羧酸烷基酯单元的热塑性共聚物（B）。所得共聚物的耐热性和无色透明性优异，异物含量非常小。

3. 发明公开

EP1496067A8 THERMOPLASTIC POLYMER, PROCESS FOR PRODUCING THE SAME, AND MOLDED ARTICLE 审中-公开
标题翻译：热塑性聚合物，其生产方法和成型制品
公开(公告)号：EP1496067A8
公开(公告)日：2005-09-21
申请号：EP03712911.1
申请日：2003-03-25
申请人： TORAY INDUSTRIES, INC.
发明人： MATSUMOTO, Hideki , TANAKA, Akiko , YAMAMOTO, Daisuke , SATO, Daisuke , YAMANAKA, Toru
IPC分类号： C08F8/48 , G02B1/04
CPC分类号： G02B1/041 , C08F8/48 , G02B1/04 , C08L101/06 , C08L33/00 , C08F220/14
摘要： A thermoplastic polymer containing glutaric anhydride units of the following general formula (1) and having an absorbance at awavelength of 280 nm of at most 0.5 (the absorbance is a value of the polymer film having a thickness of 100 µm, measured with a UV-visible spectrophotometer) and a glass transition temperature of not lower than 130°C has high-level colorless transparency and good heat resistance, moldability and dwell stability. wherein R 1 and R 2 are the same or different and each represents a hydrogen atom or an alkyl group having from 1 to 5 carbon atoms.
摘要翻译：一种热塑性聚合物，其含有下述通式（1）所示的戊二酸酐单元，波长280nm处的吸光度为0.5以下（吸光度为100μm厚的聚合物膜的值，用UV- 可见分光光度计）且玻璃化转变温度不低于130℃具有高水平的无色透明度和良好的耐热性，成型性和保压稳定性。其中R1和R2相同或不同，并且各自表示氢原子或具有1至5个碳原子的烷基。

4. 发明公开

EP3553048A1 METHOD FOR PRODUCING -CAPROLACTAM 有权
公开(公告)号：EP3553048A1
公开(公告)日：2019-10-16
申请号：EP17879609.0
申请日：2017-12-05
申请人： Toray Industries, Inc.
发明人： TSUKAMOTO, Daijiro , ITO, Masateru , YAMADA, Katsushige , AKAHIRA, Masato , YAMAMOTO, Daisuke , YAMAUCHI, Koji
IPC分类号： C07D201/08 , B01J23/648 , B01J23/847 , C07C255/19 , C07D223/10 , C07B61/00
摘要： The present invention is a method of producing ε-caprolactam through adipamide as an intermediate, and characteristically includes a lactamization step of reacting adipamide, formed from a material compound, with hydrogen and ammonia in the presence of a catalyst containing: a metal oxide mainly containing an oxide(s) of one or more metallic elements selected from the group consisting of metallic elements of group 5 and groups 7 to 14 in the 4th to 6th periods of the periodic table; and a metal and/or a metal compound having a hydrogenation ability. The method can increase the selectivity of ε-caprolactam.

5. 发明公开

EP3088443A1 POLYPHENYLENE SULPHIDE BLOCK COPOLYMER, METHOD FOR MANUFACTURING SAME, AND METHOD FOR MANUFACTURING POLYPHENYLENE SULPHIDE POROUS BODY 审中-公开
标题翻译：聚苯硫醚嵌段共聚物，其制造方法及聚苯硫醚多孔体的制造方法
公开(公告)号：EP3088443A1
公开(公告)日：2016-11-02
申请号：EP14873514.5
申请日：2014-12-24
申请人： Toray Industries, Inc.
发明人： YAMASHITA, Kohei , UNOHARA, Takeshi , TAKEUCHI, Kosaku , YAMAMOTO, Daisuke , YAMAUCHI, Koji
IPC分类号： C08G81/00 , C08G75/02 , C08J9/26
CPC分类号： C08G81/00 , C08G75/0204 , C08G75/0259 , C08G75/0286 , C08J9/26 , C08J2201/046 , C08J2381/02 , C08J2381/04
摘要： A heat-resistant, chemical-resistant polyphenylene sulfide block copolymer containing polyphenylene sulfide units and aromatic polyester units, wherein the polyphenylene sulfide units have a number average molecular weight in the range of 6,000 to 100,000. Provided is a novel polyphenylene sulfide block copolymer that overcomes the disadvantages of block copolymers including a low-molecular-weight polyphenylene sulfide segment and having poor heat resistance and chemical resistance.
摘要翻译：一种含有聚苯硫醚单元和芳香族聚酯单元的耐热耐化学性聚苯硫醚嵌段共聚物，其中聚苯硫醚单元的数均分子量范围为6,000至100,000。提供一种新型聚苯硫醚嵌段共聚物，其克服了包含低分子量聚苯硫醚链段的嵌段共聚物的缺点，并且耐热性和耐化学性差。

6. 发明公开

EP3202961A1 POLYPHENYLENE SULFIDE FIBER 审中-公开
标题翻译：聚苯硫醚纤维
公开(公告)号：EP3202961A1
公开(公告)日：2017-08-09
申请号：EP15847414.8
申请日：2015-09-24
申请人： Toray Industries, Inc.
发明人： KATSUTA, Hiroo , MITSUNAGA, Reo , YAMAMOTO, Daisuke , HORIUCHI, Shunsuke , FUNATSU, Yoshitsugu
IPC分类号： D01F6/76
CPC分类号： D01F6/765 , D02J1/22 , D02J13/00 , D02J13/005
摘要： Provided is a poly(phenylene sulfide) fiber which changes little in fiber structure and has excellent long-term heat resistance. Namely, a poly(phenylene sulfide) fiber having a degree of crystallization of 45.0% or higher, a content of movable amorphous components of 15.0% or less, and a weight-average molecular weight of 300,000 or less is provided.
摘要翻译：本发明提供一种纤维结构变化少，长期耐热性优异的聚苯硫醚纤维。即，提供结晶度为45.0％或更高，可移动的无定形组分含量为15.0％或更低，重均分子量为300,000或更低的聚（亚苯基硫醚）纤维。

7. 发明公开

EP3150752A1 POLYPHENYLENE SULFIDE FIBERS, AND MANUFACTURING METHOD THEREFOR 审中-公开
标题翻译：多发性骨质疏松症
公开(公告)号：EP3150752A1
公开(公告)日：2017-04-05
申请号：EP15799260.3
申请日：2015-05-22
申请人： Toray Industries, Inc.
发明人： KATSUTA, Hiroo , MIHARA, Takaaki , YAMAMOTO, Daisuke , HORIUCHI, Shunsuke , FUNATSU, Yoshitsugu
IPC分类号： D01F6/96
CPC分类号： D01F6/765 , C08G75/0213 , C08G75/0254 , C08G75/0277 , D01D5/08 , D01D10/02 , D01F6/94 , D02J1/224
摘要： A poly(phenylene sulfide) fiber containing 1-10% by weight of a poly(phenylene sulfide) oligomer having a weight-average molecular weight of 5,000 or less, having a difference between a cold crystallization heat quantity (ΔHc) and a crystal melting heat quantity (ΔHm) during temperature rising in DSC, ΔHm-ΔHc, of 25 J/g or larger, and having an elongation of less than 40% and a strength of 3.0 cN/dtex or higher. The present invention provides a poly(phenylene sulfide) fiber which has high heat resistance and chemical resistance and which has high strength and, despite this, has excellent suitability for high-order processing, e.g., thermal shapability, because the amorphous parts thereof have high molecular movability.
摘要翻译：含有重量平均分子量为5,000以下的聚（苯硫醚）低聚物1-10重量％的聚苯硫醚纤维，其具有冷结晶热量（“Hc”）和结晶在DSC中升温时的熔融热量（“Hm”）为25J / g以上，伸长率小于40％，强度为3.0cN / dtex以上的“Hm-”Hc。本发明提供一种具有高耐热性和耐化学性并且具有高强度的聚苯硫醚纤维，尽管如此，它具有优异的适用于高级加工，例如热定形性，因为其非晶部分具有高的分子移动性。

8. 发明公开

EP3088470A1 POLYARYLENE SULFIDE RESIN COMPOSITION AND MOLDED ARTICLE COMPRISING SAME 审中-公开
标题翻译：多发性黄疸
公开(公告)号：EP3088470A1
公开(公告)日：2016-11-02
申请号：EP14874068.1
申请日：2014-12-19
申请人： Toray Industries, Inc.
发明人： ICHINOSE, Keiko , TAKAO, Hidenobu , YAMAMOTO, Daisuke , YAMAUCHI, Koji
IPC分类号： C08L81/02 , C08G75/06 , C08J3/20 , C08K5/098
CPC分类号： C08K5/098 , C08J5/18 , C08J2381/04 , C08L81/02
摘要： A polyarylene sulfide resin composition comprising a polyarylene sulfide (A) and an alkaline earth metal organic carboxylate (B) in an amount of 0.001 to 10 mol% based on the formula -(Ar-S)-, a repeating unit of polyarylene sulfide, wherein the polyarylene sulfide (A) has a weight average molecular weight of 10,000 or more and a weight reduction during heating that satisfies the following equation. ΔWr = W 1 − W 2 / W 1 × 100 ≤ 0.18 %
In the equation, ΔWr is a weight reduction ratio (%) determined by a thermogravimetric analysis performed in a non-oxidizing atmosphere under normal pressure at a temperature rise rate of 20°C/min from 50°C to any temperature equal to or higher than 330°C, wherein W 1 is a sample weight at 100°C, and W 2 is a sample weight at 330°C.
Provided is a polyarylene sulfide resin composition that contains a polyarylene sulfide produced in an economical and simple manner, has a lowered melt crystallization temperature and a retarded solidification rate, and generates little amount of gas at high temperatures.
摘要翻译：包含聚芳硫醚（A）和碱土金属有机羧酸酯（B）的聚芳硫醚树脂组合物，其量为式 - （Ar-S）为0.001〜10摩尔％，聚芳硫醚的重复单元，其中聚芳硫醚（A）的重均分子量为10,000以上，加热时的重量减少满足下式。 “Wr = W 1'W 2 / W 1×100‰0.18％在该方程式中，”Wr“是通过在非氧化性气氛中在常压下在温度下进行的热重分析测定的重量减少率（％）从50℃升至等于或高于330℃的任何温度的20℃/分钟的升温速率，其中W 1是100℃下的样品重量，W 2是在330℃下的样品重量。提供一种含有以经济，简单的方式制造的聚芳硫醚的聚芳硫醚树脂组合物，具有降低的熔融结晶温度和延迟固化速率，并且在高温下产生少量的气体。

9. 发明公开

EP4063345A1 METHOD FOR PRODUCING e-CAPROLACTAM 审中-实审
公开(公告)号：EP4063345A1
公开(公告)日：2022-09-28
申请号：EP20890793.1
申请日：2020-11-18
申请人： Toray Industries, Inc.
发明人： TSUKAMOTO, Daijiro , KAWAMURA, Kenji , YAMADA, Katsushige , AKAHIRA, Masato , YAMAMOTO, Daisuke
IPC分类号： C07C231/12 , C07C237/06 , C07D201/08
摘要： The present invention synthesizes ε-caprolactam from 5-cyanovaleramide with high yield by means of the steps (A) and (B) described below. (A) a step for obtaining 5-cyanovaleramide hydrogenation reaction mixture by causing 5-cyanovaleramide to react with hydrogen in an aqueous solvent in the presence of a hydrogenation catalyst (B) a step for obtaining ε-caprolactam by heating the 5-cyanovaleramide hydrogenation reaction mixture, which has been obtained in the step (A), to a temperature of from 180°C to 300°C in an aqueous solvent.

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