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1. 发明授权

EP2784063B1 METHOD FOR PRODUCING BETA-MERCAPTOCARBOXYLIC ACID 有权
公开(公告)号：EP2784063B1
公开(公告)日：2018-09-19
申请号：EP12852172.1
申请日：2012-11-20
申请人： Mitsui Chemicals, Inc.
发明人： FURUYA, Masayuki , OGAWA, Tatsuya , NISHIMURA, Takeshi
IPC分类号： C07C319/04 , C07C319/28 , C07C321/04 , C07C321/14 , C07C323/52 , C07C319/06 , C07C319/24
CPC分类号： C07C319/04 , C07C319/24 , C07C319/28 , C07C323/52
摘要： A process for preparing ²-mercaptocarboxylic acid of the present invention is provided with Step a for reacting a compound represented by a formula: X 1 2 S (X 1 represents hydrogen, Na or K) or a compound represented by a formula: X 2 SH (X 2 represents Na or K), alkali hydroxide represented by a formula: X 3 OH (X 3 represents Na or K), and unsaturated carboxylic acid represented by the following General Formula (1) to obtain a reaction solution including a compound represented by the following General Formula (2) and a compound represented by the following General Formula (3), Step b for neutralizing the reaction solution obtained in Step a with an acid to obtain a reaction solution including ²-mercaptocarboxylic acid represented by the following General Formula (4) and a compound represented by the following General Formula (5), Step c for distillation-refining the reaction solution obtained in Step b to obtain the ²-mercaptocarboxylic acid represented by General Formula (4), and Step d for returning a distillation residue including the compound represented by General Formula (5) in Step c to Step a.

2. 发明公开

EP2426210A1 PROCESS FOR PRODUCTION OF 3-MERCAPTOPROPIONIC ACID OR SALT THEREOF 审中-公开
标题翻译： VERFAHREN ZUR HERSTELLUNG VON 3-MERCAPTOPROPIONSÄUREODER EINEM SALZ DARAUS
公开(公告)号：EP2426210A1
公开(公告)日：2012-03-07
申请号：EP10769529.8
申请日：2010-04-30
申请人： Mitsui Chemicals, Inc.
发明人： ARAKI, Tadashi , FURUYA, Masayuki , HAYASHI, Hidetoshi
IPC分类号： C12P11/00 , C12N15/09
CPC分类号： C12P11/00 , C08G75/28 , C12Y305/01004 , C12Y402/01084
摘要： The present invention provides is a method for producing 3-mercaptopropionic acid from 3-mercaptopropionamide or a salt thereof with the use of an amidase. The method enables the production of 3-mercaptopropionic acid on an industrial scale through an enzymatic reaction.
摘要翻译：本发明提供了使用酰胺酶从3-巯基丙酰胺或其盐生产3-巯基丙酸的方法。该方法能够通过酶反应在工业规模生产3-巯基丙酸。

3. 发明公开

EP4001974A1 POLYTHIOL COMPOSITION AND APPLICATION THEREOF 审中-实审转让
公开(公告)号：EP4001974A1
公开(公告)日：2022-05-25
申请号：EP20839843.8
申请日：2020-07-14
申请人： Mitsui Chemicals, Inc.
发明人： NISHIMURA, Takeshi , FURUYA, Masayuki , SUESUGI, Kouji
IPC分类号： G02B1/04 , C08G18/38
摘要： A polythiol composition includes a polythiol compound (A) including at least one of 4,8-dimercaptomethyl-1,11-dimercapto-3,6,9-trithiaundecane, 4,7-dimercaptomethyl-1,11-dimercapto-3,6,9-trithiaundecane, or 5,7-dimercaptomethyl-1,11-dimercapto-3,6,9-trithiaundecane, and a polythiol compound (B) that is 4-mercaptomethyl-1,8-dimercapto-3,6-dithiaoctane.

4. 发明公开

EP2784064A1 METHOD FOR PRODUCING BETA-MERCAPTOCARBOXYLIC ACID 有权
标题翻译： PROCESS FOR BETA巯基的制备
公开(公告)号：EP2784064A1
公开(公告)日：2014-10-01
申请号：EP12852300.8
申请日：2012-11-20
申请人： Mitsui Chemicals, Inc.
发明人： FURUYA, Masayuki , OGAWA, Tatsuya , NISHIMURA, Takeshi
IPC分类号： C07C319/04 , C07C319/28 , C07C323/52 , C07B61/00
CPC分类号： C07C319/04 , C07C319/28 , C07C323/52
摘要： There is provided a process for preparing β-mercaptocarboxylic acid represented by the following General Formula (3) comprising step of reacting hydrogen sulfide, alkali hydroxide represented by a formula: XOH (X represents Na or K), and unsaturated carboxylic acid represented by the following General Formula (1) under atmospheric pressure to obtain a reaction solution including a compound represented by the following General Formula (2) and step of neutralizing the reaction solution in an acid. An amount of the alkali hydroxide is equal to or greater than total moles of the unsaturated carboxylic acid and the hydrogen sulfide.

5. 发明公开

EP3988602A1 USE CONDITION SETTING METHOD FOR POLYMERIZATION CATALYST, POLYMERIZATION CONDITION SETTING METHOD, AND METHOD FOR PRODUCING OPTICAL MATERIAL 审中-实审转让
公开(公告)号：EP3988602A1
公开(公告)日：2022-04-27
申请号：EP20826102.4
申请日：2020-06-18
申请人： Mitsui Chemicals, Inc.
发明人： FURUYA, Masayuki , NISHIMURA, Takeshi
IPC分类号： C08G85/00 , C08F2/00
摘要： A method for setting conditions for use of a polymerization catalyst of the present invention includes a physical property acquiring step S10 of acquiring a physical property value derived from remaining functional groups after maintaining a temperature of a composition including a polymerization-reactive compound and a predetermined amount of a polymerization catalyst, a remaining functional group ratio calculating step S20 of calculating a remaining functional group ratio from the physical property value, a reaction rate constant calculating step S30 of calculating a reaction rate constant based on a reaction rate equation from the remaining functional group ratio, a fitting step S40 of calculating an activation energy and a frequency factor from the reaction rate constant using an Arrhenius plot, a polymerization catalyst selecting step S50 of determining whether or not the activation energy satisfies a predetermined condition for the polymerization catalyst, an approximation equation setting step S60 of setting an approximation equation from the frequency factor, and a catalyst addition range setting step S70 of setting an addition range with respect to the polymerization-reactive compound.

6. 发明公开

EP3960731A1 THIOL-CONTAINING COMPOSITION FOR OPTICAL MATERIAL AND POLYMERIZABLE COMPOSITION FOR OPTICAL MATERIAL 审中-公开
公开(公告)号：EP3960731A1
公开(公告)日：2022-03-02
申请号：EP20795100.5
申请日：2020-04-24
申请人： Mitsui Chemicals, Inc.
发明人： NISHIMURA, Takeshi , FURUYA, Masayuki , KUMA, Shigetoshi
IPC分类号： C07C323/52 , G02B1/04 , C08G18/38 , C08G18/72
摘要： The thiol-containing composition for an optical material of the present invention includes a compound (A) represented by General Formula (a), and a compound (B) composed of at least one selected from a compound (b2-1) represented by General Formula (b2-1), a compound (b3-1) represented by General Formula (b3-1), a compound (b3-2) represented by General Formula (b3-2), and a compound (b4-2) represented by General Formula (b4-2), in which, in high-performance liquid chromatography measurement, the total peak area ratio of the compound included in the compound (B) is 0.1% to 60.0% with respect to the peak area 100 of the compound (A).

7. 发明授权

EP2918577B1 METHOD FOR OBTAINING A PURIFIED ALDEHYDE COMPOUND 有权
公开(公告)号：EP2918577B1
公开(公告)日：2018-07-25
申请号：EP13853532.3
申请日：2013-11-08
申请人： Mitsui Chemicals, Inc.
发明人： KAKINUMA, Naoyuki , FURUYA, Masayuki , SAKATA, Michiharu , TOKUNAGA, Koichi , KUMA, Shigetoshi
IPC分类号： C07C253/34 , B01J25/00 , B01J31/24 , C07C209/26 , C07C209/48 , C07C211/19 , C07C253/30 , C07C255/47 , C07C263/10 , C07C265/14 , C07B61/00
CPC分类号： C07C263/10 , B01J31/24 , C07B63/00 , C07C209/26 , C07C211/19 , C07C253/30 , C07C253/34 , C07C255/47 , C07C265/14 , C07C2602/42
摘要： The purification method of an aldehyde compound of the present invention includes a step of neutralizing a reaction solution containing an aldehyde compound by adding water and a base compound to the reaction solution, and a step of distilling the neutralized reaction solution, in which the reaction solution is obtained by reacting a compound represented by the following Formula (a1) or (a2) with hydrogen and carbon monoxide in the presence of a metal compound of groups 8 to 10 and a phosphorus compound, the phosphorus compound is represented by Formula (R 1 O) 3 P, and the base compound is at least one kind selected from among carbonate and hydrogen carbonate of metals of group I on the periodic table and carbonate and hydrogen carbonate of metals of group II on the periodic table.

8. 发明公开

EP2784063A1 METHOD FOR PRODUCING BETA-MERCAPTOCARBOXYLIC ACID 有权
标题翻译：生产β-巯基羧酸的方法
公开(公告)号：EP2784063A1
公开(公告)日：2014-10-01
申请号：EP12852172.1
申请日：2012-11-20
申请人： Mitsui Chemicals, Inc.
发明人： FURUYA, Masayuki , OGAWA, Tatsuya , NISHIMURA, Takeshi
IPC分类号： C07C319/04 , C07C319/28 , C07C321/04 , C07C321/14
CPC分类号： C07C319/04 , C07C319/24 , C07C319/28 , C07C323/52
摘要： A process for preparing β-mercaptocarboxylic acid of the present invention is provided with Step a for reacting a compound represented by a formula: X 1 2 S (X 1 represents hydrogen, Na or K) or a compound represented by a formula: X 2 SH (X 2 represents Na or K), alkali hydroxide represented by a formula: X 3 OH (X 3 represents Na or K), and unsaturated carboxylic acid represented by the following General Formula (1) to obtain a reaction solution including a compound represented by the following General Formula (2) and a compound represented by the following General Formula (3), Step b for neutralizing the reaction solution obtained in Step a with an acid to obtain a reaction solution including β-mercaptocarboxylic acid represented by the following General Formula (4) and a compound represented by the following General Formula (5), Step c for distillation-refining the reaction solution obtained in Step b to obtain the β-mercaptocarboxylic acid represented by General Formula (4), and Step d for returning a distillation residue including the compound represented by General Formula (5) in Step c to Step a.
摘要翻译：本发明的β-巯基羧酸的制备方法包括步骤a：使式X12S（X1代表氢，Na或K）所代表的化合物或式X2X代表的化合物（X2代表Na或（2）表示的化合物和下述通式（2）表示的化合物的反应溶液，式（X）表示的碱金属氢氧化物，X3OH表示的碱金属氢氧化物（X3表示Na或K）（3）所示的化合物，工序b，用酸中和工序a中得到的反应液，得到含有下述通式（4）所示的β-巯基羧酸和下述通式（5）所示的步骤c，对通过步骤b得到的反应溶液进行蒸馏精制，得到通式（4）所示的β-巯基羧酸，工序df 或将包含步骤c中由通式（5）表示的化合物的蒸馏残余物返回至步骤a。

9. 发明公开

EP2708527A1 ALDEHYDE COMPOUND PRODUCTION METHOD 有权
标题翻译：一种用于生产醛
公开(公告)号：EP2708527A1
公开(公告)日：2014-03-19
申请号：EP12782970.3
申请日：2012-05-07
申请人： Mitsui Chemicals, Inc.
发明人： KUMA, Shigetoshi , SAKATA, Michiharu , TOKUNAGA, Kouichi , SHIMAKAWA, Chitoshi , KAKINUMA, Naoyuki , FURUYA, Masayuki , TANAKA, Mamoru
IPC分类号： C07C45/49 , C07C47/347 , C07C209/26 , C07C209/48 , C07C211/19 , C07C253/30 , C07C255/47 , C07C263/10 , C07C265/14 , C07B61/00
CPC分类号： C07C253/30 , C07C45/29 , C07C45/49 , C07C209/26 , C07C209/48 , C07C209/52 , C07C263/10 , C07C2602/42 , C07C211/19 , C07C265/14 , C07C255/47 , C07C47/347
摘要： A process for producing an aldehyde compound of the invention comprising: reacting a compound represented by the following formula (a1) or (a2) with a hydrogen and a carbon monoxide in a presence of a compound containing a metal belonging to Groups 8 to 10 and a phosphorous compound so as to satisfy the following conditions (1) and (2) to synthesize an aldehyde compound;
wherein the condition (1) is that a content of a metal included in the compound containing a metal belonging to Groups 8 to 10 is 0.01 ppmmol to 300 ppmmol with respect to 1 mol of the compound represented by the formula (a1) or (a2), and
wherein the condition (2) is that a molar ratio represented by the phosphorous compound (mol)/ the metal (mol) is 100 or more;

10. 发明公开

EP3778655A1 METHOD FOR SETTING POLYMERIZATION CONDITIONS AND METHOD FOR PRODUCING OPTICAL MATERIAL 审中-公开
公开(公告)号：EP3778655A1
公开(公告)日：2021-02-17
申请号：EP18912105.6
申请日：2018-06-06
申请人： Mitsui Chemicals, Inc.
发明人： FURUYA, Masayuki , NISHIMURA, Takeshi , ITO, Shinsuke , OGAWA, Tatsuya
IPC分类号： C08F2/00
摘要： The method for setting polymerization condition of the present invention includes a physical property acquiring step S10 of, when heating a composition including a polymerization-reactive compound and a polymerization catalyst and/or a polymerization initiator and retaining heat at a predetermined temperature, acquiring a physical property value a derived from a functional group before heating of the polymerization-reactive compound and a physical property value b derived from a remaining functional group after maintaining a temperature for a predetermined time; a remaining functional group ratio calculating step S20 of calculating a remaining functional group ratio from the physical property value a and the physical property value b; a reaction rate coefficient calculating step S30 of calculating a reaction rate coefficient from the remaining functional group ratio on the basis of a reaction rate equation; and a polymerization temperature calculating step S40 of calculating a polymerization temperature on the basis of the reaction rate coefficient and conditions below.

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