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1. 发明公开

EP0122797A1 Process for producing granular, water-swellable crosslinked acrylic copolymer, and its use 失效
标题翻译：一种用于制备颗粒剂，水可溶胀的交联的丙烯酸共聚物和其使用过程中。
公开(公告)号：EP0122797A1
公开(公告)日：1984-10-24
申请号：EP84302554.5
申请日：1984-04-13
申请人： MITSUI PETROCHEMICAL INDUSTRIES, LTD.
发明人： Honda, Narimichi , Wakumoto, Hiroshi , Nakano, Takayuki , Ueki, Hiromi , Hiratsuka, Jyunzo
IPC分类号： C08F220/54 , A01G1/00
CPC分类号： C08F220/54 , A01G24/00 , A01G24/35
摘要： A process for producing a granular, water-swellable crosslinked acrylic copolymer, which comprises copolymerizing in an aqueous medium in the presence of a radical polymerization initiator a monomeric mixture comprising (a) at least one acrylic amide monomer selected from the group consisting of acrylamide, methacrylamide and N-methyl substitution products of these amides and (b) at least one acrylic crosslinkable comonomer selected from the group consisting of N,N'-alkylene- or arylene-bis-acrylamides, N,N'-alkylene- bismethacrylamides, alkylenebisacrylates, alkylene-bismethacrylates, alkylene glycolbisacrylates, polyalkylene glycol-bisacrylates, alkylene glycol-bismethacrylates and polyalkylene glycol-bismethacrylates, the proportion of the comonomer (b) being 0.01 to 5 moles per 100 moles of the acrylic amide monomer (a), and forming a granular copolymer; and (i) drying the resulting granular copolymer at a temperature of 105 to 150°C, or(ii) heat-treating the resulting granular copolymer in the presence of moisture under substantially sealed conditions at a temperature of 100 to 160°C; and a method of hydroponically growing a plant, which comprises growing the plant in artificial soil composed of a granular, water-swellable crosslinked acrylic copolymer.
摘要翻译：一种用于生产颗粒状，水可溶胀的交联丙烯酸共聚物，其包含在wässrige介质中，在自由基聚合引发剂的存在下共聚合过程的单体混合物，其包含选自丙烯酰胺的选自（a）至少一种丙烯酸酰胺单体，选自的N，N'-亚烷基 - 或亚芳基 - 双 - 丙烯酰胺，N选定甲基丙烯酰胺和合成的酰胺和（b）至少一种丙烯酸类交联性共聚单体的N-甲基取代产物，N'- alkylenebismethacrylamides，alkylenebisacrylates，alkylenebismethacrylates ，亚烷基glycolbisacrylates，聚亚烷基glycolbisacrylates，亚烷基二醇和bismethacrylates聚亚烷基二醇bismethacrylates，（b）是每100个摩尔的丙烯酰胺单体（a），并且形成粒状共聚物的0点01分至5摩尔的共聚单体的比例; 及（i）干燥所述颗粒在105至150℃的温度下得到的共聚物，或者（ii）热处理在100〜160℃的温度下在潮湿的基本上密封的条件下在存在所得到的粒状共聚物; 和水耕的方法生长的植物，其包括生长在粒状，水可溶胀的交联丙烯酸共聚物组成的人造土壤植物。

2. 发明授权

EP0122797B1 Process for producing granular, water-swellable crosslinked acrylic copolymer, and its use 失效
标题翻译：生产水溶性交联丙烯酸共聚物的方法及其用途
公开(公告)号：EP0122797B1
公开(公告)日：1987-07-15
申请号：EP84302554.5
申请日：1984-04-13
申请人： MITSUI PETROCHEMICAL INDUSTRIES, LTD.
发明人： Honda, Narimichi , Wakumoto, Hiroshi , Nakano, Takayuki , Ueki, Hiromi , Hiratsuka, Jyunzo
IPC分类号： C08F220/54 , A01G1/00
CPC分类号： C08F220/54 , A01G24/00 , A01G24/35
摘要： A process for producing a granular, water-swellable crosslinked acrylic copolymer, which comprises copolymerizing in an aqueous medium in the presence of a radical polymerization initiator a monomeric mixture comprising (a) at least one acrylic amide monomer selected from the group consisting of acrylamide, methacrylamide and N-methyl substitution products of these amides and (b) at least one acrylic crosslinkable comonomer selected from the group consisting of N,N min -alkylene- or arylene-bis-acrylamides, N,N min -alkylenebismethacrylamides, alkylenebisacrylates, alkylenebismethacrylates, alkylene glycolbisacrylates, polyalkylene glycol-bisacrylates, alkylene glycol-bismethacrylates and polyalkylene glycol-bismethacrylates, the proportion of the comonomer (b) being 0.01 to 5 moles per 100 moles of the acrylic amide monomer (a), and forming a granular copolymer; and (i) drying the resulting granular copolymer at a temperature of 105 to 150 DEG C, or (ii) heat-treating the resulting granular copolymer in the presence of moisture under substantially sealed conditions at a temperature of 100 to 160 DEG C; and a method of hydroponically growing a plant, which comprises growing the plant in artificial soil composed of a granular, water-swellable crosslinked acrylic copolymer.

3. 发明授权

EP0122797B2 Process for producing granular, water-swellable crosslinked acrylic copolymer, and its use 失效
标题翻译：一种用于制备颗粒剂，水可溶胀的交联的丙烯酸共聚物和其使用过程中。
公开(公告)号：EP0122797B2
公开(公告)日：1994-05-18
申请号：EP84302554.5
申请日：1984-04-13
申请人： MITSUI PETROCHEMICAL INDUSTRIES, LTD.
发明人： Honda, Narimichi , Wakumoto, Hiroshi , Nakano, Takayuki , Ueki, Hiromi , Hiratsuka, Jyunzo
IPC分类号： C08F220/54 , A01G1/00
CPC分类号： C08F220/54 , A01G24/00 , A01G24/35
摘要： A process for producing a granular, water-swellable crosslinked acrylic copolymer, which comprises copolymerizing in an aqueous medium in the presence of a radical polymerization initiator a monomeric mixture comprising (a) at least one acrylic amide monomer selected from the group consisting of acrylamide, methacrylamide and N-methyl substitution products of these amides and (b) at least one acrylic crosslinkable comonomer selected from the group consisting of N,N min -alkylene- or arylene-bis-acrylamides, N,N min -alkylenebismethacrylamides, alkylenebisacrylates, alkylenebismethacrylates, alkylene glycolbisacrylates, polyalkylene glycol-bisacrylates, alkylene glycol-bismethacrylates and polyalkylene glycol-bismethacrylates, the proportion of the comonomer (b) being 0.01 to 5 moles per 100 moles of the acrylic amide monomer (a), and forming a granular copolymer; and (i) drying the resulting granular copolymer at a temperature of 105 to 150 DEG C, or (ii) heat-treating the resulting granular copolymer in the presence of moisture under substantially sealed conditions at a temperature of 100 to 160 DEG C; and a method of hydroponically growing a plant, which comprises growing the plant in artificial soil composed of a granular, water-swellable crosslinked acrylic copolymer.

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