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1. 发明授权

EP1620494B1 VERFAHREN ZUR VAKUUMERZEUGUNG BEI DER HERSTELLUNG VON POLYMEREN 有权
标题翻译：过程在聚合物中生产真空PRODUCING
公开(公告)号：EP1620494B1
公开(公告)日：2008-07-30
申请号：EP04724560.0
申请日：2004-03-31
申请人： Lurgi Zimmer GmbH
发明人： KÄMPF, Rudolf
IPC分类号： C08G85/00
CPC分类号： F04F5/54 , B01J3/006 , B01J2219/00006 , B01J2219/00162 , C08G63/785 , C08G64/205 , C08G65/4093 , C08G75/23 , C08G79/04
摘要： The invention relates to a method for the production of polymers by means of melt-phase polycondensation in at least one reaction step under vacuum. The vapor produced is drawn off by at least one steam jet vacuum pump with a downstream injection condenser from the reaction step. In order to improve the method, the steam jet vacuum pump is driven with alkylene carbonate in vapor form and liquid alkylene carbonate is supplied to the injection condenser as coolant.

2. 发明授权

EP1768775B1 VERFAHREN UND VORRICHTUNG ZUR ABSATZWEISEN HERSTELLUNG VON POLYMEREN DURCH SCHMELZEKONDENSATION 有权
标题翻译：方法和装置通过熔融缩聚物贸易形式生产
公开(公告)号：EP1768775B1
公开(公告)日：2008-01-23
申请号：EP05772235.7
申请日：2005-07-02
申请人： Lurgi Zimmer GmbH
发明人： KÄMPF, Rudolf
IPC分类号： B01J19/18 , C08G63/78
CPC分类号： B01J19/20 , B01J19/18 , B01J2219/00006 , B01J2219/00777 , B01J2219/00779 , C08G63/785 , C08G64/205
摘要： Disclosed are a method and a device for gradually producing high-molecular polyphosphonates, polysulfones, polyarylates, polyamides, polyarylene ethers, or polyetherketones by melt-condensing a monomer compound carrying hydroxyl groups, carboxyl groups, anhydride groups, phosphoric acid groups, phosphono groups, phosphonate groups, phosphino groups, phosphinate groups, carbonyl groups, sulfonyl groups, sulfonate groups, siloxane groups, or amino groups on its own or along with at least one diphenol, dialcohol, diamine, or a dicarbonate component. According to the invention, a) esterification or reesterification and precondensation are performed in an intermittently operated first reactor (1) in the presence of an esterification catalyst or reesterification catalyst; b) polycondensation is then optionally performed in an intermittently operated intermediate reactor (6) by optionally adding one or several additional monomers, another catalyst, and additives until a predetermined polycondensation level or viscosity level has been attained; and finally c) condensation is continued in an intermittently operated final reactor (12) until the desired polycondensation level or viscosity level has been reached; and d) branching molecules comprising more than two functional groups are optionally added prior to or during esterification or re-esterification, prior to or during polycondensation optionally performed in the intermediate reactor, or prior to or during polycondensation performed in the final reactor. The dwell time in the reactors ranges between 5 minutes and 15 hours while the temperature is set to 180 to 300 °C in reactors (1) and (6) and to 240 to 400 °C in reactor (12), the pressure being continuously or gradually lowered from 2000 to 100 mbar in reactors (1) and (6) and to 100 to 0.01 mbar in reactor (12) by sucking off the vapors produced during condensation.

3. 发明公开

EP1871821A1 VERFAHREN UND VORRICHTUNG ZUR VAKUUMERZEUGUNG UND ABSCHEIDUNG VON FLÜCHTIGEN VERBINDUNGEN BEI POLYKONDENSATIONSREAKTIONEN 审中-公开
标题翻译：方法和装置真空产生和缩聚挥发性化合物的分离
公开(公告)号：EP1871821A1
公开(公告)日：2008-01-02
申请号：EP06707283.5
申请日：2006-02-27
申请人： Lurgi Zimmer GmbH
发明人： KÄMPF, Rudolf
IPC分类号： C08G64/30 , C08G63/78 , B01J3/00
CPC分类号： C08G69/28 , B01D53/1487 , B01D53/1493 , B01J3/006 , B01J2219/00162 , B01J2219/00247 , C08G63/785 , C08G64/205 , F04F5/54
摘要： The invention relates to a method for generating a vacuum and for separating volatile compounds during esterfication, transesterfication and/or polycondensation reactions. One or several jets of steam comprising a spray condenser, which is arranged up or downstream, are connected to the suction side of a reactor which is to be evacuated and phenol or steam containing phenol is used as propellant steam at a pressure of 0.5 hPa to approximately 1.5 MPa and liquid phenol or a liquid containing phenol is used as a spraying agent.

4. 发明公开

EP1824587A1 REAKTOR ZUR BEHANDLUNG HOCHVISKOSER KUNSTSTOFFSCHMELZEN 有权
标题翻译：反应器的处理高度粘稠的塑料熔体
公开(公告)号：EP1824587A1
公开(公告)日：2007-08-29
申请号：EP05807857.7
申请日：2005-10-20
申请人： Lurgi Zimmer GmbH
发明人： KÄMPF, Rudolf , SCHULZE, Michael
IPC分类号： B01F7/10 , B01F15/06 , B01F15/00 , B01J19/18
CPC分类号： B01F15/068 , B01F7/10 , B01F15/00019 , B01J19/1887 , B01J2219/00094 , B01J2219/00166 , B01J2219/182
摘要： The invention relates to a reactor for the treatment of highly viscous plastic melts, comprising a horizontal, cylindrical container (2) with a vapour exhaust and chambers in the region of the melting bath, formed by the arrangement of panel walls, in which annular discs, fixed to a shaft (3) by spokes and serving as stirrer elements (4, 5) may be rotated, whereby, in the cavities of the annular discs (4, 5), two opposing scrapers (6, 7) are fixed to the inside of the container at an offset angle and run past at a small separation from the front faces of the annular discs and the sleeve of the shaft (3). According to the invention, the assembly and disassembly of the shaft and scraper is simplified by connection of the scraper to the inside of the container by means of a positive connection (13, 19).

5. 发明授权

EP1749042B1 VERFAHREN ZUR HERSTELLUNG VON ELASTOMEREN COPOLYESTERN 有权转让
标题翻译：用于生产弹性体共聚酯
公开(公告)号：EP1749042B1
公开(公告)日：2008-01-02
申请号：EP05715459.3
申请日：2005-02-23
申请人： Lurgi Zimmer GmbH
发明人： KÄMPF, Rudolf
IPC分类号： C08G63/78 , C08G63/672 , C07D307/08 , C08G65/20
CPC分类号： C08G63/78 , C08G63/672
摘要： The invention relates to a method for the continuous or discontinuous production of elastomeric copolyesters from polybutylene terephthalate (PBT) and polyoxytetramethylene glycol. According to said method, the tetrahydrofurane (THF) that occurs as a by-product during the production of polybutylene terephthalate from 1,4-butanediol is reacted after its rectification by means of a ring-opening polymerisation to form polyoxytetramethylene glycol, which condenses with the free or esterified carboxyl groups of the PBT to form a copolyester, whereby chain termination and deactivation of the catalyst take place by the addition of 1,4-butanediol, without the separation of the catalyst.

6. 发明授权

EP1824587B1 REAKTOR ZUR BEHANDLUNG HOCHVISKOSER KUNSTSTOFFSCHMELZEN 有权
公开(公告)号：EP1824587B1
公开(公告)日：2007-12-19
申请号：EP05807857.7
申请日：2005-10-20
申请人： Lurgi Zimmer GmbH
发明人： KÄMPF, Rudolf , SCHULZE, Michael
IPC分类号： B01F7/10 , B01F15/06 , B01F15/00 , B01J19/18
CPC分类号： B01F15/068 , B01F7/10 , B01F15/00019 , B01J19/1887 , B01J2219/00094 , B01J2219/00166 , B01J2219/182
摘要： The invention relates to a reactor for the treatment of highly viscous plastic melts, comprising a horizontal, cylindrical container (2) with a vapour exhaust and chambers in the region of the melting bath, formed by the arrangement of panel walls, in which annular discs, fixed to a shaft (3) by spokes and serving as stirrer elements (4, 5) may be rotated, whereby, in the cavities of the annular discs (4, 5), two opposing scrapers (6, 7) are fixed to the inside of the container at an offset angle and run past at a small separation from the front faces of the annular discs and the sleeve of the shaft (3). According to the invention, the assembly and disassembly of the shaft and scraper is simplified by connection of the scraper to the inside of the container by means of a positive connection (13, 19).
摘要翻译：用于处理高粘度塑料熔体的反应器本发明涉及一种用于处理高粘度塑料熔体的反应器，该反应器包括具有蒸汽排出装置的水平圆柱形容器（2）和在熔池区域中由腔壁布置形成的腔室，其中环形圆盘，通过辐条固定在轴（3）上并作为搅拌器元件（4,5）可以旋转，由此在环形盘（4,5）的空腔中，两个相对的刮板（6,7）固定到容器的内侧成偏斜角并且从环形盘的前表面和轴（3）的套筒以小间距行进。根据本发明，通过利用形状连接（13,19）将刮具连接到容器的内部来简化轴和刮板的组装和拆卸。

7. 发明公开

EP1869102A1 VERFAHREN ZUR AUFBEREITUNG VON KONDENSATEN AUS DER POLYKONDENSATION 审中-公开
标题翻译：一种用于处理冷凝液中缩聚
公开(公告)号：EP1869102A1
公开(公告)日：2007-12-26
申请号：EP06707287.6
申请日：2006-02-27
申请人： Lurgi Zimmer GmbH
发明人： KÄMPF, Rudolf , KARPF, Andreas , LINKE, Rainer , SCHMIDT, Oliver , SCHOLZ, Gerald
IPC分类号： C08G63/78 , C08G64/20 , C08G64/30 , B01J3/00
CPC分类号： C08G63/785 , B01D3/148 , C08G63/19
摘要： The invention relates to a method for treating vapours and condensates which arise during the production of polycondensates from bisphenols or high-value phenols by esterification and/or transesterification with alkyl or aryl esters of at least bivalent organic or inorganic acids. According to the invention, the treatment is carried out in a plurality of condensates and/or distillation columns which are connected in a step-by-step manner behind each other, each distillation column comprising a connected condensate. The dew point and the pressure in each condensate are adjusted such that in each step, monomers, oligomers or decomposition and transformation products are removed.

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