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    • 1. 发明公开
    • VERFAHREN ZUM TROCKNEN EINES NASSMATERIALS
    • EP2140217A1
    • 2010-01-06
    • EP08714794.8
    • 2008-04-01
    • Lehmann, Markus
    • BRAENDLI, Mark
    • F26B3/20F26B7/00F26B9/08F26B25/00
    • F26B25/006F26B3/205F26B7/00F26B9/085F26B2200/18
    • The invention relates to a method for drying a wet material (4) which comprises a liquid Fd to be distilled, using a gas-tight container system (1) that is resistant to excess and/or negative pressure. Said container system comprises a drying container (2) containing the wet material (4) whose temperature can be adjusted, a condenser (3) for condensing the liquid Fd, which has turned to vapor and whose temperature can be adjusted, to give the condensation product (5), and a vapor chamber (6) connecting the drying container (2) and the condenser (3). The aim of the invention is to make sure that the vapor in the vapor chamber (6) is free of foreign gas except for a tolerated remainder. To achieve this aim, the pressure in the vapor chamber (6) is monitored and controlled in such a manner that drying and distillation are always carried out in a range close to the saturation vapor pressure of the liquid Fd to be distilled. For this purpose, the pressure and the temperature in the vapor chamber (6) have to be continuously determined. If the pressure is too high, it is reduced in such a manner that especially foreign gas is removed.
    • 包含待蒸馏的液体Fd的湿材料的干燥方法使用耐过剩和/或负压的气密容器系统和连接干燥容器和冷凝器的干燥容器,冷凝器和蒸气室。 温度可调的干燥容器包含湿材料。 液体Fd在温度可调的蒸气室中转变为蒸汽。 冷凝器冷凝蒸气以产生冷凝产物。 监测和控制蒸气室中的压力,使得干燥和蒸馏总是在接近待蒸馏的液体Fd的饱和蒸汽压的范围内进行。 连续测定蒸气室中的压力和温度。 如果压力超过该范围的上限,则压力以这样的方式减少,特别是除去外来气体。