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1. 发明公开

EP2963090A1 Method of manufacturing an anticorrosive pigment, the anticorrosive pigment and its application 审中-公开
标题翻译：一种用于生产耐腐蚀颜料，抗腐蚀颜料及其使用方法
公开(公告)号：EP2963090A1
公开(公告)日：2016-01-06
申请号：EP14460113.5
申请日：2014-12-17
申请人： Instytut Elektrotechniki
发明人： Szymanski, Wojciech , Halama, Agnieszka , Pasciak, Grzegorz
IPC分类号： C09D5/08 , C01B25/18 , C09C1/00
CPC分类号： C09D5/084 , C01P2004/61 , C09C1/0003
摘要： The subject of this invention is a method of manufacturing an anticorrosive pigment, the anticorrosive pigment itself and its application, especially in organic protective coatings.
The essence of the method, according to the invention, consists in that the reagents zinc phosphate tetrahydrate Zn 3 (PO 4 ) 2 ·4H 2 O in the amount of 110.0 g, heptamolybdate tetrahydrate (NH 4 ) 6 Mo 7 O 24 ·4H 2 O in the amount of 40.6 g - 70 g, calcium oxide CaO in the amount of 30.1 g - 54.0 g, boric acid H 3 BO 3 in the amount of 100.0 g and sodium carbonate Na 2 CO 3 in the amount of 15.3 g - 50.1 g are thoroughly mixed and calcined at a temperature from 1000 °C to 1100 °C for 0.5 h to 1 h until a glass phase is formed, upon which the obtained melt containing zinc oxide ZnO in the amount of 58.6 g, phosphoric oxide P 2 O 5 in the amount of 34.1 g, molybdenum oxide MoO 3 in the amount of 33.1g - 57.1 g, calcium oxide CaO in the amount of 30.1 g-54.0 g, boric oxide B 2 O 3 in the amount of 56.3 g and sodium oxide Na 2 O in the amount of 8.89 g - 29.3 g, are grinded, advantageously to the grain size below 5 µm.
The essence of the anticorrosive pigment, according to the invention consists in that it has a form of a powdered melt containing zinc oxide ZnO in the amount of 58.6 g, phosphoric oxide P 2 O 5 in the amount of 34.1 g, molybdenum oxide MoO 3 in the amount of 33.1g - 57.1 g, calcium oxide CaO in the amount of 30.1 g - 54.0 g, boric oxide B 2 O 3 in the amount of 56.3 g and sodium oxide Na 2 O in the amount of 8.9 g-29.3 g, advantageously with the grain size below 5 µm.
Use of a powdered melt, which is added in the amount from 10.1 g to 52.6 g into 1000 g of paint as an active pigment, enhancing corrosion resistivity of coatings made from solvent and water soluble epoxy paints, and solvent and water soluble polyvinyl, acryl and alkyd epoxy paints.
摘要翻译：本发明的主题是制造防腐蚀颜料，所述防腐蚀颜料本身和它的应用的方法，在爱情特别是有机保护涂层。该方法的本质，根据本发明，besteht，DASS死试剂磷酸锌四水合物的Zn 3（PO 4）2·4H 2 O在110.0克，七钼酸铵四水合物的量（NH 4）6 Mo 7 O 24·4H 2 O中40.6克量 - 70克，氧化钙的CaO 30.1克量 - 54.0克，硼酸H 3 BO 3在100.0克和碳酸钠的Na 2 CO 3的量在15.3克量 - 50.1克充分混合和在1000℃〜1100℃的温度下反应0.5小时至1小时，直到玻璃相煅烧形成，在其上所获得的熔体含有氧化锌的ZnO在58.6克量，磷酸氧化物 P 2 O 5在34.1克，氧化钼的MoO 3中33.1克的量的量 - 57.1克，氧化钙中的CaO 30.1 G-54.0克，氧化硼B 2 O 3的量在56.3克量和氧化钠的Na在8.89克量2 O - 3.29克，被研磨，有利地小于5微米的粒径。所述防腐蚀颜料的本质，雅丁发明besteht DASS它具有粉末熔融在34.1克量的含有氧化锌的ZnO在58.6克，磷酸氧化物P 2 O 5的量的形式，氧化钼的MoO 3 在33.1克的量 - 57.1克，氧化钙中的CaO 30.1克量 - 54.0克，氧化硼B 2 O 3中的56.3克和氧化钠的Na 2 O的量在8.9 G-29.3克量，有利地与在5微米以下的粒径。粉末熔融，在所有这是在添加量由10.1克至52.6克入1000克漆作为活性颜料，增强从溶剂和水溶性环氧涂料，溶剂和水溶性聚乙烯醇制备的涂层的抗腐蚀性的用途，丙烯酸和醇酸环氧漆。

2. 发明公开

EP2960302A1 Method of synthesis of hybrid compounds of polyaniline and application of hybrid compounds of polyaniline 审中-公开
标题翻译：过程聚苯胺和聚苯胺的杂化化合物的应用的杂化化合物的合成
公开(公告)号：EP2960302A1
公开(公告)日：2015-12-30
申请号：EP14460112.7
申请日：2014-12-17
申请人： Instytut Elektrotechniki
发明人： Szymanski, Wojciech , Halama, Agnieszka , Madalinski, Jacek , Pasciak, Grzegorz
IPC分类号： C09D5/08 , C09D163/00 , C08G73/02
CPC分类号： C09D163/00 , C08G73/0266 , C08K5/55 , C08K13/02 , C09D5/086 , C09D7/62
摘要： The subject of this invention is a method of synthesis of of hybrid compounds of polyaniline and application of hybrid compounds of polyaniline.
The method consists in that to an ice water cooled acid solution, selected from the group of orthophosphoric acids of a concentration of 0.1 - 6 M, or hydrochloric, hydrofluoric, nitric and sulfuric acid of a concentration 0.1 - 8 M, containing an oxidizer in a form of dissolved ammonium persulfate (NH 4 ) 2 S 2 O 8 in the amount of 10.0 - 20.0 g and 5.0 - 20.0 g of ammonium heptamolybdate tetrahydrate (NH 4 ) 6 Mo 7 O 24 x 4 H 2 O), 5.11 g of aniline is added, whereby the cooled solution is stirred for at least 1 hour, and then left for at least 4 hours at an ambient temperature, and after sedimentation the dark-green precipitate of polyaniline heptarilolybdate is filtered, thoroughly rinsed with distilled water until the filtrate is colorless and finally dried at 378 K for at least 8 hours. Application consists in that the polyaniline heptamolybdates, added in the amount of 0.1 to 5 mass %, play a role of inhibitors, enhancing corrosion resistance of coatings made from epoxy resins, water soluble polyvinyl, acryl and alkyd epoxy paints, and paints dissolved in two-component solvents.
摘要翻译：本发明的主题是聚苯胺和聚苯胺的杂化化合物的应用的杂化的化合物的合成方法。该方法besteht DASS到冰水冷却酸溶液，从该组的浓度为0.1的正磷酸选自 - -6 M，或盐酸，氢氟酸，硝酸和硫酸的浓度0.1 - -8 M，在氧化剂的含溶解过硫酸铵的形式（NH 4）2 S 2 O 8在10.0量 - 20.0 g且5.0 - 20.0四水合七钼酸铵的（NH 4）6 Mo 7 O 24×4 H 2 O），5.11克苯胺加入，由此冷却的溶液搅拌至少1小时，然后在环境温度下静置至少4小时，和聚苯胺heptarilolybdate的暗绿色沉淀过滤沉淀后，用蒸馏水彻底冲洗，直到滤液是无色的，最后在378的温度下干燥至少8小时。在DASS死聚苯胺heptamolybdates应用besteht，添加在0.1〜5质量％，起到抑制剂的作用，增强从环氧树脂，水溶性聚乙烯醇，丙烯酸树脂和醇酸环氧涂料制备的涂层的耐腐蚀性，并在两个溶于涂料 -component溶剂。

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