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1. 发明公开

EP2791107A1 MALONIC ACID DI-SALTS AND A METHOD FOR PREPARING MALONYL DIHALIDES 有权转让
标题翻译：丙二酸二乙酯二盐及其制造方法MALONYLDIHALOGENIDEN
公开(公告)号：EP2791107A1
公开(公告)日：2014-10-22
申请号：EP12808629.5
申请日：2012-12-13
申请人： E. I. Du Pont de Nemours and Company
发明人： ZHANG, Wenming , ANNIS, Gary, David
IPC分类号： C07C257/06 , C07D487/04 , C07C57/34 , C07C51/60 , C07C57/72
CPC分类号： C07D471/04 , C07C51/60 , C07C55/36 , C07C57/34 , C07C57/36 , C07D213/55 , C07C57/72
摘要： A compound of Formula 2 is disclosed wherein R1, MA and MB are as defined in the disclosure. Also disclosed is a method for preparing a compound of Formula 1 wherein R1 and X are as defined in the disclosure comprising contacting a compound of Formula 2 with a halogenating agent. Also disclosed is a method for preparing a compound of Formula 4 wherein R1, R3 and R4 are as defined in the disclosure, comprising reacting a compound of Formula 5 wherein R3 and R4 are as defined in the disclosure with a compound of Formula 1, with a compound of Formula 1, the process of preparing the compound of Formula 4 includes the step of preparing the compound of Formula 1 from the compound of Formula 2 by the method disclosed above. Also disclosed is compound that is methyl 3,5-dichlorobenzeneethanimidate methyl 3,5-dichlorobenzeneethanimidate or ethyl 3,5-dichlorobenzeneethanimidate or salts thereof.

2. 发明授权

EP2176244B1 Method for preparing 5-haloalkyl-4,5-dihydroisoxazole derivatives 有权转让
标题翻译：一种用于5 - 卤代烷基-4,5-二氢异恶唑衍生物的制备方法
公开(公告)号：EP2176244B1
公开(公告)日：2016-06-01
申请号：EP08797091.9
申请日：2008-08-04
申请人： E. I. du Pont de Nemours and Company
发明人： ANNIS, Gary, David , SMITH, Brenton, Todd
IPC分类号： C07D261/04 , C07D413/10 , C07D413/12 , C07D417/12 , C07C49/235
CPC分类号： C07D261/04 , C07C45/65 , C07C45/68 , C07C45/72 , C07C49/813 , C07C49/83 , C07C49/835 , C07C49/84 , C07C65/38 , C07C69/007 , C07C201/12 , C07C205/45 , C07D413/10 , C07D413/12 , C07D417/12

3. 发明授权

EP2162440B1 PROCESS FOR PREPARING 2-AMINO-5-CYANOBENZOIC ACID DERIVATIVES 有权
公开(公告)号：EP2162440B1
公开(公告)日：2012-02-22
申请号：EP08780919.0
申请日：2008-06-23
申请人： E. I. Du Pont de Nemours and Company
发明人： ANNIS, Gary, David
IPC分类号： C07D231/14 , C07D401/04 , C07C253/14 , C07C255/58 , C07F15/04
CPC分类号： C07D401/04 , C07C253/14 , C07D231/14 , C07F15/04 , C07C255/58
摘要： Disclosed is a method for preparing a compound of Formula 1 comprising (1) contacting a compound of Formula 2, with (2) at least one alkali metal cyanide and (3) at least one compound of Formula (4); wherein R1 is NHR3 or OR4; R2 is CH3 or Cl; R3 is H, C1-C4 alkyl, cyclopropyl, cyclopropylcyclopropyl, cyclopropylmethyl or methylcyclopropyl; R4 is H or C1-C4 alkyl; and X is Br, Cl or I. Also disclosed is a method for preparing a compound of Formula (4 )comprising contacting a mixture of (i) at least one compound of Formula (9 )and (ii) at least one metal reducing agent with (iii) dichlorobis(triphenylphosphine)nickel, and further disclosed is a method for removing nickel impurities from a mixture thereof with compounds of Formula (1 )comprising contacting the mixture with oxygen in the presence of an aqueous cyanide solution, and additionally disclosed is a method for preparing a compound of Formula (5); wherein R5, R6, R7 and Z are as defined in the disclosure, using a compound of Formula (1,) characterized by preparing the compound of Formula (1) by the method disclosed above.

4. 发明公开

EP1888536A1 METHOD FOR PREPARING SUBSTITUTED PYRIMIDINES 有权
标题翻译：用于生产取代嘧啶
公开(公告)号：EP1888536A1
公开(公告)日：2008-02-20
申请号：EP06759727.8
申请日：2006-05-12
申请人： E. I. DU PONT DE NEMOURS AND COMPANY
发明人： ANNIS, Gary, David
IPC分类号： C07D239/30 , C07D239/36 , C07D239/42
CPC分类号： C07D239/42 , C07D239/30 , C07D239/36
摘要： Disclosed a method for preparing a ester (Formula I) wherein R1 is cyclopropyl, 4-chlorophenyl or 4-bromophenyl; and R2 is C1-C14 alkyl; comprising contacting acetal (Formula II) with a persulfate oxidant in the presence of a strong sulfur- or phosphorus-containing mineral acid and an oxidation resistant solvent.

5. 发明公开

EP1373210A1 HETEROCYCLIC DIAMIDE INVERTEBRATE PEST CONTROL AGENTS 有权
标题翻译：杂环二酰胺进行战斗脊椎动物害虫
公开(公告)号：EP1373210A1
公开(公告)日：2004-01-02
申请号：EP02723322.0
申请日：2002-02-28
申请人： E. I. du Pont de Nemours and Company
发明人： ANNIS, Gary, David , FINKELSTEIN, Bruce, Lawrence
IPC分类号： C07D213/82 , C07D231/40 , C07D333/38 , C07D403/12 , C07D401/14 , C07D409/12 , C07D409/14 , C07D401/12 , C07D213/81 , C07D413/12
CPC分类号： C07D213/82 , A01N43/10 , A01N43/40 , A01N43/54 , A01N43/56 , A01N43/80 , C07D231/40 , C07D333/38 , C07D401/12 , C07D401/14 , C07D405/12 , C07D409/12 , C07D409/14 , C07D413/12 , C07D413/14
摘要： This invention provides compounds of Formula (I), N-oxides and suitable salts thereof, wherein A and B are independently O or S; each J is independently a phenyl ring, a naphthyl ring system, a 5- or 6-membered heteroaromatic ring or an aromatic 8-, 9- or 10-membered fused heterobicyclic ring system wherein each ring or ring system is optionally substituted with 1 to 4 R5; K is, together with the two contiguous linking carbon atoms, a 5- or 6-membered heteroaromatic ring optionally substituted with 1 to 3 R?4; and R1 R2, R3, R4, R5¿ and n are as defined in the disclosure. Also disclosed are methods for controlling an invertebrate pest comprising contacting the invertebrate pest or its environment with a biologically effective amount of a compound of Formula (I), an N-oxide thereof or a suitable salt of the compound (e.g., as a composition described herein). This invention also pertains to a composition for controlling an invertebrate pest comprising a biologically effective amount of a compound of Formula (I), an N-oxide thereof or a suitable salt of the compound and at least one additional component selected from the group consisting of surfactants, solid diluents and liquid diluents.

6. 发明公开

EP2260016A2 METHOD FOR PREPARING 3-TRIFLUOROMETHYL CHALCONES 有权转让
标题翻译：用于生产3-三氟甲基查尔
公开(公告)号：EP2260016A2
公开(公告)日：2010-12-15
申请号：EP09730611.2
申请日：2009-04-08
申请人： E. I. du Pont de Nemours and Company
发明人： ANNIS, Gary, David
IPC分类号： C07C45/68 , C07D261/04 , C07C45/74 , C07C49/80 , C07C25/13
CPC分类号： C07D261/04 , C07C17/35 , C07C25/13 , C07C45/455 , C07C45/70 , C07C49/80 , C07C49/813 , C07C67/343 , C07C205/45 , C07C209/74 , C07C231/12 , C07C231/14 , C07C235/84 , C07D213/40 , C07D231/12 , C07D231/14 , C07D231/16 , C07D249/08 , C07D249/10 , C07D277/28 , C07C69/94 , C07C69/76 , C07C211/56
摘要： Disclosed is a method for preparing a compound of formula (2) from compounds of formula (5) and (6), wherein Z and Y are defined herein and X denotes I. Also disclosed are novel compounds of formula (2).

7. 发明公开

EP2162440A2 PROCESS FOR PREPARING 2-AMINO-5-CYANOBENZOIC ACID DERIVATIVES 有权
标题翻译：制备2-氨基-5-氰基苯甲酸衍生物的方法
公开(公告)号：EP2162440A2
公开(公告)日：2010-03-17
申请号：EP08780919.0
申请日：2008-06-23
申请人： E. I. Du Pont de Nemours and Company
发明人： ANNIS, Gary, David
IPC分类号： C07D231/14 , C07D401/04 , C07C253/14 , C07C255/58 , C07F15/04
CPC分类号： C07D401/04 , C07C253/14 , C07D231/14 , C07F15/04 , C07C255/58
摘要： Disclosed is a method for preparing a compound of Formula 1 comprising (1) contacting a compound of Formula 2, with (2) at least one alkali metal cyanide and (3) at least one compound of Formula (4); wherein R1 is NHR3 or OR4; R2 is CH3 or Cl; R3 is H, C1-C4 alkyl, cyclopropyl, cyclopropylcyclopropyl, cyclopropylmethyl or methylcyclopropyl; R4 is H or C1-C4 alkyl; and X is Br, Cl or I. Also disclosed is a method for preparing a compound of Formula (4 )comprising contacting a mixture of (i) at least one compound of Formula (9 )and (ii) at least one metal reducing agent with (iii) dichlorobis(triphenylphosphine)nickel, and further disclosed is a method for removing nickel impurities from a mixture thereof with compounds of Formula (1 )comprising contacting the mixture with oxygen in the presence of an aqueous cyanide solution, and additionally disclosed is a method for preparing a compound of Formula (5); wherein R5, R6, R7 and Z are as defined in the disclosure, using a compound of Formula (1,) characterized by preparing the compound of Formula (1) by the method disclosed above.
摘要翻译：公开了用于制备式1化合物的方法，其包括（1）使式2的化合物与（2）至少一种碱金属氰化物和（3）至少一种式（4）的化合物接触; 其中R1是NHR3或OR4; R2是CH3或Cl; R3是H，C1-C4烷基，环丙基，环丙基环丙基，环丙基甲基或甲基环丙基; R4是H或C1-C4烷基; 还公开了制备式（4）化合物的方法，其包括使（i）至少一种式（9）化合物和（ii）至少一种金属还原剂与（iii）二氯双（三苯基膦）镍反应，并进一步公开了一种从式（1）化合物的混合物中除去镍杂质的方法，该方法包括在氰化物水溶液存在下使混合物与氧气接触，制备式（5）化合物的方法; 其中R5，R6，R7和Z如本发明中所定义，使用式（1）化合物，其特征在于通过上述公开的方法制备式（1）化合物。

8. 发明公开

EP2094644A2 PROCESS FOR PREPARING 2-AMINO-5-CYANOBENZOIC ACID DERIVATIVES 审中-公开
标题翻译：制备2-氨基-5-氰基苯甲酸衍生物的方法
公开(公告)号：EP2094644A2
公开(公告)日：2009-09-02
申请号：EP07867794.5
申请日：2007-12-18
申请人： E. I. Du Pont de Nemours and Company
发明人： ANNIS, Gary, David , BRUENING, Joerg , CURRIE, Martin, James , DUMAS, Donald, Joseph , SHAPIRO, Rafael
IPC分类号： C07C231/12 , C07C253/14 , C07C233/65 , C07C255/58 , C07D401/04
CPC分类号： C07C253/14 , C07C231/12 , C07C233/65 , C07C255/58
摘要： Disclosed is a method for preparing a compound of Formula (1) comprising contacting a compound of Formula (2) with a metal cyanide reagent, a copper (I) salt reagent, an iodide salt reagent and at least one compound of Formula (3): wherein R1 is NHR3 or OR4; R2 is CH3 or Cl; R3 is H, C1-C4 alkyl, cyclopropyl, cyclopropylcyclopropyl, cyclopropylmethyl or methylcyclopropyl; R4 is H or C1-C4 alkyl; Y is Br or Cl; X is NR13 or O; n is 0 or 1; and R5, R6, R7, R8, R9, R10, R11, R12 and R13 are as defined in the disclosure. Also disclosed is a method for preparing a compound of Formula (2) wherein Y is Br and R1 is NHR3 comprising introducing a gas containing bromine into a liquid containing a compound of Formula (4), and further disclosed is a method for preparing a compound of Formula (5) wherein R14, R15, R16 and Z are as defined in the disclosure using a compound of Formula (1) characterized by preparing the compound of Formula (1) by the method disclosed above.
摘要翻译：公开了用于制备式（1）化合物的方法，其包括使式（2）化合物与金属氰化物试剂，铜（I）盐试剂，碘化物盐试剂和至少一种式（3）化合物接触，：其中R1是NHR3或OR4; R2是CH3或Cl; R3是H，C1-C4烷基，环丙基，环丙基环丙基，环丙基甲基或甲基环丙基; R4是H或C1-C4烷基; Y是Br或Cl; X是NR 13或O; n是0或1; 和R5，R6，R7，R8，R9，R10，R11，R12和R13如本发明中所定义。还公开了用于制备其中Y为Br且R 1为NHR 3的式（2）化合物的方法，其包括将含溴气体引入含有式（4）化合物的液体中，并且还公开了制备化合物（5）的化合物，其中R 14，R 15，R 16和Z如本公开中所定义，使用式（1）化合物，其特征在于通过上述公开的方法制备式（1）化合物。

9. 发明公开

EP1147096A1 HERBICIDAL OXADIAZOLIDINES 审中-公开
标题翻译：除草剂奥沙利嗪
公开(公告)号：EP1147096A1
公开(公告)日：2001-10-24
申请号：EP00913237.4
申请日：2000-01-20
申请人： E. I. du Pont de Nemours and Company
发明人： ANNIS, Gary, David , CHIANG, George, Chih-Shu , FORNEY, David, Raymond , PATEL, Kanu, Maganbhai , RORER, Morris, Padgett , SMITH, William, Francis, III , STEVENSON, Thomas, Martin , SUN, King-Mo , TSENG, Chi-Ping
IPC分类号： C07D271/07 , C07D413/04 , C07D413/06 , C07D413/12 , C07D413/14 , C07D417/04 , C07D417/06 , C07F9/653 , C07F7/10 , A01N47/38 , C07C271/06 , A01N57/24 , A01N55/10
CPC分类号： C07D271/07 , A01N47/38 , C07C271/66 , C07D271/08 , C07D271/10 , C07D413/04 , C07D413/06 , C07D413/12 , C07D417/04 , C07D417/06 , C07F7/0812 , C07F9/65318
摘要： Compounds of Formula (1) and processes for their preparation, their N-oxides and agriculturally suitable salts, are disclosed which are useful for controlling undesired vegetation wherein Q, X?1, X2, X3, R1, R2, R6 and R7¿ are as defined in the disclosure. Also disclosed are novel intermediates of Formula (5), Formula (8) and Formula (20) wherein R27 is -(CR6R7)q-Q; R6, R7, q, Q, X?1 and X2¿ are as defined in the disclosure. Also disclosed are compositions containing the compounds of Formula (1) and a method for controlling undesired vegetation which involves contacting the vegetation or its environment with an effective amount of a compound of Formula (1).
摘要翻译：公开了式（1）化合物及其制备方法，其N-氧化物和农业上合适的盐，其可用于防治不需要的植物，其中Q 1，X 1，X 2，X 3，R 1，R 2，R 6和R 7' 如在本公开中所定义的。还公开了式（5），式（8）和式（20）的新颖中间体，其中R 27为 - （CR 6 R 7）q -Q; R 6，R 7，q，Q，X 1和X 2如本发明中所定义。还公开了含有式（1）化合物的组合物和控制不期望植物的方法，该方法包括使植物或其环境与有效量的式（1）化合物接触。

10. 发明授权

EP2260016B1 METHOD FOR PREPARING 3-TRIFLUOROMETHYL CHALCONES 有权转让
标题翻译：用于生产3-三氟甲基查尔
公开(公告)号：EP2260016B1
公开(公告)日：2015-09-02
申请号：EP09730611.2
申请日：2009-04-08
申请人： E. I. du Pont de Nemours and Company
发明人： ANNIS, Gary, David
IPC分类号： C07C45/68 , C07D261/04 , C07C45/74 , C07C49/80 , C07C25/13 , C07C67/343 , C07C205/45 , C07C209/74 , C07D249/08 , C07D249/10 , C07C231/12 , C07D277/28 , C07D213/40 , C07C17/35 , C07C45/45 , C07C45/70
CPC分类号： C07D261/04 , C07C17/35 , C07C25/13 , C07C45/455 , C07C45/70 , C07C49/80 , C07C49/813 , C07C67/343 , C07C205/45 , C07C209/74 , C07C231/12 , C07C231/14 , C07C235/84 , C07D213/40 , C07D231/12 , C07D231/14 , C07D231/16 , C07D249/08 , C07D249/10 , C07D277/28 , C07C69/94 , C07C69/76 , C07C211/56
摘要： Disclosed is a method for preparing a compound of formula (2) from compounds of formula (5) and (6), wherein Z and Y are defined herein and X denotes I. Also disclosed are novel compounds of formula (2).

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