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1. 发明授权

EP2860158B1 METAL-CONTAINING SILICOALUMINOPHOSPHATE MOLECULAR SIEVE HAVING THE RHO FRAMEWORK STRUCTURE AND PROCESS FOR ITS PREPARATION 有权
标题翻译：具有RHO骨架结构的含金属的硅铝磷酸盐分子筛及其制备方法
公开(公告)号：EP2860158B1
公开(公告)日：2017-08-02
申请号：EP12878414.7
申请日：2012-06-08
申请人： Dalian Institute Of Chemical Physics, Chinese Academy of Sciences
发明人： TIAN, Peng , SU, Xiong , LIU, Zhongmin , FAN, Dong , ZHANG, Ying , YANG, Yue
IPC分类号： C01B39/54 , B01J20/18 , B01J20/30 , B01J29/85 , C07C45/32
CPC分类号： C01B39/54 , B01J20/18 , B01J20/3078 , B01J29/85 , B01J37/082

2. 发明公开

EP2860158A1 METAL SILICOALUMINOPHOSPHATE MOLECULAR SIEVE HAVING RHO SKELETON STRUCTURE AND PREPARATION PROCESS THEREFOR 有权
标题翻译：金属化学硅酸盐微生物 - 麦芽糖酵母
公开(公告)号：EP2860158A1
公开(公告)日：2015-04-15
申请号：EP12878414.7
申请日：2012-06-08
申请人： Dalian Institute Of Chemical Physics, Chinese Academy of Sciences
发明人： TIAN, Peng , SU, Xiong , LIU, Zhongmin , FAN, Dong , ZHANG, Ying , YANG, Yue
IPC分类号： C01B39/54
CPC分类号： C01B39/54 , B01J20/18 , B01J20/3078 , B01J29/85 , B01J37/082
摘要： The present invention relates to a metal silicoaluminophosphate molecular sieve MeAPSO with a RHO framework structure and a preparation method thereof. The metal silicoaluminophosphate molecular sieve is characterized in that: the metal atoms are at least one of vanadium, copper, molybdenum, zirconium, cobalt, manganese, magnesium, iron, nickel and zinc. The chemical composition of said metal silicoaluminophosphate molecular sieve in anhydrous state is expressed as: mR•nMe•(SixAlyPz)O 2 , where R represents template existed in molecular sieve micropores, m is the molar number of said template per one molar of (SixAlyPz)O 2 , m=0.1∼0.5; Me represents metal atom entering into said metal silicoaluminophosphate molecular sieve framework, n is the molar number of Me per one molar of (SixAlyPz)O 2 , n=0.001∼0.30. Said metal silicoaluminophosphate molecular sieve has ion exchange performance and adsorption performance. The catalyst prepared from said metal silicoaluminophosphate molecular sieve can be applicable to multiple hydrocarbon reactions, such as catalytic cracking, reforming, polymerization, alkylation, transalkylation, isomerization, dehydrogenation, hydrogenation and the like.
摘要翻译：本发明涉及具有RHO骨架结构的金属硅铝磷酸盐分子筛MeAPSO及其制备方法。金属硅铝磷酸盐分子筛的特征在于：金属原子是钒，铜，钼，锆，钴，锰，镁，铁，镍和锌中的至少一种。所述金属硅铝磷酸盐分子筛的无水状态的化学成分表示为：mR¢nMe¢（SixAlyPz）O 2，其中R表示模板存在于分子筛微孔中，m是每一摩尔的所述模板的摩尔数（SixAlyPz）O 2，m = 0.1〜0.5; Me表示进入所述金属硅铝磷酸盐分子筛框架的金属原子，n是每摩尔（SixAlyPz）O 2的Me的摩尔数，n = 0.001 / 0.30。所述金属硅铝磷酸盐分子筛具有离子交换性能和吸附性能。由所述金属硅铝磷酸盐分子筛制备的催化剂可适用于多个烃反应，如催化裂化，重整，聚合，烷基化，烷基转移，异构化，脱氢，氢化等。

3. 发明公开

EP2930148A1 SAPO-34 ZEOLITE HAVING DIGLYCOLAMINE AS TEMPLATING AGENT AND SYNTHESIS METHOD FOR THE ZEOLITE 有权
标题翻译： SAPO-34-ZEOLITH MIT DIGLYCOLAMIN ALS TEMPLAT UND VERFAHREN ZUR HERSTELLUNG DES ZEOLITHS
公开(公告)号：EP2930148A1
公开(公告)日：2015-10-14
申请号：EP12890022.2
申请日：2012-12-10
申请人： Dalian Institute Of Chemical Physics, Chinese Academy of Sciences
发明人： WANG, Dehua , TIAN, Peng , LIU, Zhongmin , FAN, Dong , ZHANG, Ying , SU, Xiong
IPC分类号： C01B39/54
CPC分类号： C01B39/54 , B01J20/18 , B01J20/3071 , B01J20/3078 , B01J29/85 , B01J35/023 , B01J37/04 , B01J37/06 , B01J37/08 , C01B37/08
摘要： The present invention provides a SAPO-34 molecular sieve, whose chemical composition in the anhydrous state is expressed as: mDGA·(Si x Al y P z )O 2 ; wherein DGA is diglycolamine, distributing in the cages and pores of said molecular sieve; m is the molar number of the template agent diglycolamine per one mole of (Si x Al y P z )O 2 , and m is from 0.03 to 0.25; x, y, z respectively represents the molar number of Si, Al, P, and x is from 0.01 to 0.30, and y is from 0.40 to 0.60, and z is from 0.25 to 0.49, and x + y + z =1. Said SAPO-34 molecular sieve can be used as an acid-catalyzed reaction catalyst, such as a methanol to olefins reaction catalyst. The present invention also concerns the application of said SAPO-34 molecular sieve in adsorption separation of CH 4 and CO 2 .
摘要翻译：本发明提供SAPO-34分子筛，其无水状态的化学组成表示为：mDGA·（Si x Al y P z）O 2; 其中DGA是二甘醇胺，分布在所述分子筛的笼和孔中; m是每摩尔（Si x Al y P z）O 2的模板剂二甘醇胺的摩尔数，m为0.03至0.25; x，y，z分别表示Si，Al，P的摩尔数，x为0.01〜0.30，y为0.40〜0.60，z为0.25〜0.49，x + y + z = 1。所述SAPO-34分子筛可用作酸催化的反应催化剂，如甲醇 - 烯烃反应催化剂。本发明还涉及所述SAPO-34分子筛在CH 4和CO 2的吸附分离中的应用。

4. 发明公开

EP2902362A1 SAPO-34 MOLECULAR SIEVE AND SYNTHESIS METHOD THEREOF 有权
标题翻译： SAPO-34分子筛和合成方法THEREFOR
公开(公告)号：EP2902362A1
公开(公告)日：2015-08-05
申请号：EP12885586.3
申请日：2012-09-26
申请人： Dalian Institute Of Chemical Physics, Chinese Academy of Sciences
发明人： FAN, Dong , TIAN, Peng , LIU, Zhongmin , SU, Xiong , ZHANG, Ying , YANG, Yue
IPC分类号： C01B39/54 , C01B37/08
CPC分类号： C01B39/54 , B01J29/85 , B01J37/0018 , B01J37/009 , B01J37/08 , B01J2231/763 , C01B37/08
摘要： The present invention concerns a SAPO-34 molecular sieve and method for preparing the same, whose chemical composition in the anhydrous state is expressed as: mDIPA·(Si x Al y P z )O 2 , wherein, DIPA is diisopropylamine existing in cages and pore channels of said molecular sieve, wherein m is the molar number of diisopropylamine per one mole of (SixAlyPz)O 2 , and m is from 0.03 to 0.25; x, y, z respectively represents the molar number of Si, Al, P, and x is from 0.01 to 0.30, and y is from 0.40 to 0.60, and z is from 0.25 to 0.49, and x + y + z =1. The SAPO-34 molecular sieve can be used as catalysts for acid-catalyzed reaction or oxygenate to olefins reaction.

5. 发明授权

EP2660203B1 METHOD FOR SYNTHESIZING SAPO MOLECULAR SIEVE BY SOLVOTHERMAL METHOD 失效
公开(公告)号：EP2660203B1
公开(公告)日：2018-08-22
申请号：EP11852524.5
申请日：2011-06-24
申请人： Dalian Institute Of Chemical Physics, Chinese Academy of Sciences
发明人： TIAN, Peng , LIU, Zhongmin , ZHANG, Ying , FAN, Dong , SU, Xiong
IPC分类号： C01B39/54 , C01B37/08 , B01J29/85
CPC分类号： B01J29/85 , C01B37/08 , C01B39/54 , C07C1/20 , C07C2529/85 , Y02P30/42
摘要： A solvothermal synthesis process of the SAPO molecular sieves and catalysts prepared thereby are provided. The synthesis process comprises the following steps: a) an organic amine, an aluminum source, a phosphorus source, a silicon source, and water are mixed in a molar ratio of 6-30 : 1 : 0.5-5 : 0.01-1.0 : 0.1-15, to obtain an initial mixture for preparing the SAPO molecular sieves, wherein the molar ratio of water to the organic amine is less than 2.0; b) the initial mixture obtained in the step a) is maintained at 30-60 °C and aged with stirring for not more than 24 hours, to obtain an initial gel; c) the initial gel obtain in the step b) is crystallized at 150-250 °C for 0.5-15 days. The SAPO molecular sieves prepared thereby are used, after being calcined at 400 - 700 °C in air, as catalysts for acid-catalyzed reactions or for conversion reactions of oxygen-containing compounds to olefins.

6. 发明授权

EP2930148B1 SAPO-34 ZEOLITE HAVING DIGLYCOLAMINE AS TEMPLATING AGENT AND SYNTHESIS METHOD FOR THE ZEOLITE 有权
标题翻译：以二元醇为模板剂的SAPO-34沸石及其沸石的合成方法
公开(公告)号：EP2930148B1
公开(公告)日：2017-07-05
申请号：EP12890022.2
申请日：2012-12-10
申请人： Dalian Institute Of Chemical Physics, Chinese Academy of Sciences
发明人： WANG, Dehua , TIAN, Peng , LIU, Zhongmin , FAN, Dong , ZHANG, Ying , SU, Xiong
IPC分类号： C01B39/54 , C01B37/08 , B01J20/18 , B01J20/30 , B01J29/85 , C07C1/20
CPC分类号： C01B39/54 , B01J20/18 , B01J20/3071 , B01J20/3078 , B01J29/85 , B01J35/023 , B01J37/04 , B01J37/06 , B01J37/08 , C01B37/08

7. 发明公开

EP3827898A1 CATALYST FOR PREPARING ETHYLBENZENE FROM ETHANOL AND BENZENE, PREPARATION THEREFOR AND USE THEREOF 审中-公开
公开(公告)号：EP3827898A1
公开(公告)日：2021-06-02
申请号：EP18927322.0
申请日：2018-07-27
申请人： Dalian Institute of Chemical Physics, Chinese Academy of Sciences
发明人： SU, Xiong , YANG, Xiaoli , HUANG, Yanqiang , ZHANG, Tao
IPC分类号： B01J29/40 , C07C15/073 , C07C2/86
摘要： Disclosed is a catalyst for producing ethylbenzene in one-step by vapor phase alkylation reaction of ethanol and benzene. The catalyst has the following features for the reaction: high alkylation reaction activity, high selectivity of ethylbenzene in an alkylation product, high hydrothermal stability and stable catalytic performance. The catalyst comprises a mesoporous-microporou composite TNU-9 molecular sieve and the silicon to aluminum molar ratio, SiO 2 /Al 2 O 3 , of the meso-microporous composite TNU-9 molecular sieve ranges from 50 to 200.

8. 发明授权

EP2902107B1 SAPO-34 MOLECULAR SIEVES AND SYNTHESIS METHOD THEREOF 有权
标题翻译： SAPO-34分子筛及其合成方法
公开(公告)号：EP2902107B1
公开(公告)日：2017-08-09
申请号：EP12885573.1
申请日：2012-09-26
申请人： Dalian Institute Of Chemical Physics, Chinese Academy of Sciences
发明人： TIAN, Peng , LIU, Zhongmin , FAN, Dong , SU, Xiong , ZHANG, Ying , YANG, Yue
IPC分类号： C01B39/54 , C01B37/08
CPC分类号： B01J29/85 , B01J29/84 , B01J37/0018 , B01J37/009 , B01J37/08 , B01J2231/763 , C01B37/08 , C01B39/54 , C07C1/20 , C07C7/13 , C07C2529/85 , C07C11/02 , C07C9/08

9. 发明公开

EP2902107A1 SAPO-34 MOLECULAR SIEVES AND SYNTHESIS METHOD THEREOF 有权
标题翻译： SAPO-34 MOLEKULARSIEBE UND SYNTHESEVERFAHRENDAFÜR
公开(公告)号：EP2902107A1
公开(公告)日：2015-08-05
申请号：EP12885573.1
申请日：2012-09-26
申请人： Dalian Institute Of Chemical Physics, Chinese Academy of Sciences
发明人： TIAN, Peng , LIU, Zhongmin , FAN, Dong , SU, Xiong , ZHANG, Ying , YANG, Yue
IPC分类号： B01J29/85 , B01J29/84 , C01B37/08
CPC分类号： B01J29/85 , B01J29/84 , B01J37/0018 , B01J37/009 , B01J37/08 , B01J2231/763 , C01B37/08 , C01B39/54 , C07C1/20 , C07C7/13 , C07C2529/85 , C07C11/02 , C07C9/08
摘要： The present invention concerns a SAPO-34 molecular sieve and method for preparing the same, whose chemical composition in the anhydrous state is expressed as: mSDA·(Si x Al y P z )O 2 , wherein m is from 0.08 to 0.3, and x is from 0.01 to 0.60, and y is from 0.2 to 0.60, and z is from 0.2 to 0.60, and x + y + z =1. There is the template agent SDA in micropores of the molecular sieve. SDA is organic amine with the structural formula as (CH 3 ) 2 NRN(CH 3 ) 2 , wherein R is saturated straight-chain or branch-chain alkylene group with the number of carbon atoms at a range from 2 to 5. There is a slight Si enrichment phenomenon on the crystal surface of the molecular sieve crystal, and the ratio of the surface Si content to the bulk Si content of the crystal ranges from 1.50 to 1.01. Said SAPO-34 molecular sieve after calcined at a temperature range from 400 to 700 °C in air can be used as a gas adsorbent and catalysts for acid-catalyzed reaction or oxygenate to olefin reaction.
摘要翻译：本发明涉及一种SAPO-34分子筛及其制备方法，其无水状态的化学成分表示为：mSDA·（Si x Al y P z）O 2，其中m为0.08〜0.3，以及 x为0.01〜0.60，y为0.2〜0.60，z为0.2〜0.60，x + y + z = 1。在分子筛的微孔中存在模板剂SDA。 SDA是结构式为（CH 3）2 NRN（CH 3）2的有机胺，其中R是碳原子数为2〜5的饱和直链或支链亚烷基。存在在分子筛晶体的晶体表面上存在轻微的Si富集现象，并且表面Si含量与晶体的Si含量之比在1.50至1.01之间。在空气中在400-700℃的温度范围煅烧后的所述SAPO-34分子筛可用作气体吸附剂和用于酸催化反应或含氧化合物与烯烃反应的催化剂。

10. 发明公开

EP2660203A1 METHOD FOR SYNTHESIZING SAPO MOLECULAR SIEVE BY SOLVOTHERMAL METHOD AND CATALYST PREPARED THEREBY 失效
标题翻译：法合成SAPO分子七个由SOLVOTHERMISCHES过程，并在这个过程中制得的催化剂
公开(公告)号：EP2660203A1
公开(公告)日：2013-11-06
申请号：EP11852524.5
申请日：2011-06-24
申请人： Dalian Institute Of Chemical Physics, Chinese Academy of Sciences
发明人： TIAN, Peng , LIU, Zhongmin , ZHANG, Ying , FAN, Dong , SU, Xiong
IPC分类号： C01B39/54 , C01B37/08 , B01J29/85
CPC分类号： B01J29/85 , C01B37/08 , C01B39/54 , C07C1/20 , C07C2529/85 , Y02P30/42
摘要： A solvothermal synthesis process of the SAPO molecular sieves and catalysts prepared thereby are provided. The synthesis process comprises the following steps: a) an organic amine, an aluminum source, a phosphorus source, a silicon source, and water are mixed in a molar ratio of 6-30 : 1 : 0.5-5 : 0.01-1.0 : 0.1-15, to obtain an initial mixture for preparing the SAPO molecular sieves, wherein the molar ratio of water to the organic amine is less than 2.0; b) the initial mixture obtained in the step a) is maintained at 30-60 °C and aged with stirring for not more than 24 hours, to obtain an initial gel; c) the initial gel obtain in the step b) is crystallized at 150-250 °C for 0.5-15 days. The SAPO molecular sieves prepared thereby are used, after being calcined at 400 - 700 °C in air, as catalysts for acid-catalyzed reactions or for conversion reactions of oxygen-containing compounds to olefins.

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