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1. 发明公开

EP1234810A1 PROCESS FOR THE PRODUCTION OF HALOGENOFLUOROCARBONS 有权
标题翻译： VERFAHREN ZUR HERSTELLUNG VON HALOGENFLUORKOHLENSTOFF-VERBINDUNGEN
公开(公告)号：EP1234810A1
公开(公告)日：2002-08-28
申请号：EP00976339.2
申请日：2000-11-20
申请人： Daikin Industries, Ltd.
发明人： TAKUBO, Seiji , SHIBATA, Noriaki , NAKADA, Tatsuo , SHIBANUMA, Takashi
IPC分类号： C07C17/20 , C07C19/08 , C07C21/18
CPC分类号： C07C17/208 , C07C17/206
摘要： The present invention provides a process for preparing a fluorine-containing halogenated hydrocarbon compound by fluorinating, in a reaction field where an antimony halide compound represented by the general formula:

SbCl p F 5-p (I)

wherein p is a value within a range from 0 to 2, and hydrogen fluoride and a halogenated hydrocarbon compound as a raw material exist, the halogenated hydrocarbon compound in a molar ratio of the antimony halide compound to hydrogen fluoride within a range from 40/60 to 90/10. According to this process, a fluorine-containing halogenated hydrocarbon compound (HFC), which is important as a substitute compound of CFC or HCFC, can be prepared economically advantageously with good selectivity while suppressing a corrosive action of a reaction vessel.
摘要翻译：本发明提供一种通过在反应领域中氟化制备含氟卤代烃化合物的方法，其中通式为SbClpF5-p表示的卤化锑化合物其中p为0至2的范围内的值，以及存在氟化氢和作为原料的卤代烃化合物，卤化锑化合物与氟化氢的摩尔比在40/60〜90/10的范围内的卤代烃化合物。根据该方法，作为CFC或HCFC的替代化合物，重要的含氟卤代烃化合物（HFC）可以在抑制反应容器的腐蚀作用的同时，以良好的选择性经济地制备。

2. 发明公开

EP0716065A1 PROCESS FOR PRODUCING HEXAFLUOROCYCLOBUTENE AND PROCESS FOR PRODUCING HEXAFLUOROCYCLOBUTANE 失效
标题翻译：生产六氟环丁烯的方法和生产六氟环戊烷的方法
公开(公告)号：EP0716065A1
公开(公告)日：1996-06-12
申请号：EP94923068.4
申请日：1994-08-03
申请人： DAIKIN INDUSTRIES, LTD.
发明人： NAKADA, Tatsuo , AOYAMA, Hirokazu , YAMAMOTO, Akinori
IPC分类号： C07C23/06 , C07C17/23 , C07C17/354 , B01J21/08 , B01J23/26 , B01J23/74 , B01J23/86 , B01J27/138 , B01J23/44 , B01J23/46
CPC分类号： C07C23/06 , B01J23/464 , C07C17/23 , C07C17/281 , C07C17/354
摘要： Manufacturing method for hexafluorocyclobutene in which 1,2-dichlorohexafluorocyclobutane is dechlorinated using hydrogen in the presence of a metal oxide and/or silicon oxide catalyst. Manufacturing method for (Z)-1,2,3,3,4,4-hexafluorocyclobutane which carries out the hydrogen-adding reaction (hydrogen reduction) of the raw material, 1,2-dichlorohexafluorocyclobutane, in the presence of a rhodium catalyst, or which carries out vapor-phase hydrogen reduction of hexafluorocyclobutene in the presence of a palladium catalyst.
Using this manufacturing method, hexafluorocyclobutene can easily be derived in a single step with high selectivity from 1,2-dichlorohexafluorocyclobutane which can be obtained readily and at a low cost. This method also produces a high yield of (Z)-1,2,3,3,4,4-hexafluorocyclobutane.
摘要翻译：六氟环丁烯的制造方法，其中在金属氧化物和/或氧化硅催化剂存在下使用氢气使1,2-二氯六氟环丁烷脱氯。在铑催化剂存在下，对原料1,2-二氯六氟环丁烷进行加氢反应（氢还原）的（Z）-1,2,3,3,4,4-六氟环丁烷的制造方法或者在钯催化剂存在下进行六氟环丁烯的气相氢还原。采用这种制造方法，六氟环丁烯可容易地以低成本容易地从1,2-二氯六氟环丁烷高选择性地一步得到。该方法也产生（Z）-1,2,3,3,4,4-六氟环丁烷的高收率。

3. 发明授权

EP1234810B1 PROCESS FOR THE PRODUCTION OF HALOGENOFLUOROCARBONS 有权
标题翻译：用于生产卤素FLUOR碳化合物
公开(公告)号：EP1234810B1
公开(公告)日：2007-01-10
申请号：EP00976339.2
申请日：2000-11-20
申请人： DAIKIN INDUSTRIES, LTD.
发明人： TAKUBO, Seiji , SHIBATA, Noriaki , NAKADA, Tatsuo , SHIBANUMA, Takashi
IPC分类号： C07C17/20 , C07C19/08 , C07C21/18
CPC分类号： C07C17/208 , C07C17/206
摘要： A process for the production of halogenofluorocarbons by fluorinating a halogenated hydrocarbon in a reaction system containing an antimony halide of the general formula: SbClpF5-p [wherein p is 0 to 2], hydrogen fluoride, and the halogenated hydrocarbon serving as the starting material with the molar ratio of the antimony halide to hydrogen fluoride being set in the range of 40/60 to 90/10. According to this process, halogenofluorocarbons (HFC) important as the substitute for CFC or HCFC can be highly selectively and economically produced with decreased corrosion of the reactor.

4. 发明公开

EP0581961A1 PROCESS FOR PRODUCING HALOGENATED BUTENE AND BUTANE 失效
标题翻译： VERFAHREN ZUR HERSTELLUNG VON HALOGENIERTEM BUTEN UND BUTAN。
公开(公告)号：EP0581961A1
公开(公告)日：1994-02-09
申请号：EP93901537.6
申请日：1993-01-12
申请人： DAIKIN INDUSTRIES, LTD.
发明人： NAKADA, Tatsuo , AOYAMA, Hirokazu , KOYAMA, Satoshi
IPC分类号： C07C17/04 , C07C19/08 , C07C21/18 , B01J27/12
CPC分类号： C07C17/21 , C07C21/18
摘要： A process for industrially producing at least one halogen compound selected from the group consisting of 1,1,1,4,4,4-hexafluoro-2,3-dichlorobutane, 1,1,1,4,4,4-hexafluoro-2-chloro-2-butene, 1,1,1,2,4,4,4-hepta-fluoro-2-butene and 1,1,1,2,2,4,4,4-octafluorobutane by the vapor-phase reaction of 1,1,2,3,4,4-hexachloro-1,3-butadiene with hydrogen fluoride in the presence of a fluorination catalyst.
摘要翻译：一种工业生产至少一种选自1,1,1,4,4,4-六氟-2,3-二氯丁烷，1,1,1,4,4,4-六氟-2- 2-氯-2-丁烯，1,1,1,2,4,4,4-七氟-2-丁烯和1,1,1,2,2,4,4,4-八氟丁烷由蒸气在氟化催化剂存在下，1,1,2,3,4,4-六氯-1,3-丁二烯与氟化氢的相反应。

5. 发明授权

EP0581961B1 PROCESS FOR PRODUCING HALOGENATED BUTENE AND BUTANE 失效
标题翻译：用于生产卤化丁烯和丁烷
公开(公告)号：EP0581961B1
公开(公告)日：1996-09-18
申请号：EP93901537.6
申请日：1993-01-12
申请人： DAIKIN INDUSTRIES, LTD.
发明人： NAKADA, Tatsuo , AOYAMA, Hirokazu , KOYAMA, Satoshi
IPC分类号： C07C17/04 , C07C19/08 , C07C21/18 , B01J27/12
CPC分类号： C07C17/21 , C07C21/18
摘要： A process for industrially producing at least one halogen compound selected from the group consisting of 1,1,1,4,4,4-hexafluoro-2,3-dichlorobutane, 1,1,1,4,4,4-hexafluoro-2-chloro-2-butene, 1,1,1,2,4,4,4-hepta-fluoro-2-butene and 1,1,1,2,2,4,4,4,-octafluorobutane by the vapor-phase reaction of 1,1,2,3,4,4-hexachloro-1,3-butadiene with hydrogen fluoride in the presence of a fluorination catalyst.

6. 发明公开

EP0703207A1 PROCESS FOR PRODUCING 1,1,1,3,3-PENTAFLUOROPROPANE AND/OR 1,1,3,3,3-PENTAFLUOROPROPENE 失效
标题翻译：生产1,1,1,3,3-五氟丙烷和/或1,1,3,3,3-五氟丙烯的方法
公开(公告)号：EP0703207A1
公开(公告)日：1996-03-27
申请号：EP94916420.6
申请日：1994-05-30
申请人： DAIKIN INDUSTRIES, LTD.
发明人： YAMAMOTO, Akinori , SEKI, Eiji , AOYAMA, Hirokazu , NAKADA, Tatsuo
IPC分类号： C07C19/08 , C07C21/18 , C07C17/00 , B01J23/26 , B01J23/42 , B01J23/44 , B01J23/46 , B01J23/74 , B01J23/78 , B01J23/86
CPC分类号： C07C19/08 , C07C17/00 , C07C17/23 , C07C17/354 , C07C21/18
摘要： A process for producing 1,1,1,3,3-pentafluoropropane by reducing 1,1,1,3,3,3-pentafluoropropene with hydrogen in the presence of a palladium catalyst in vapor phase at 40 to 300 °C. A process for producing 1,1,1,3,3-pentafluoropropane and/or 1,1,3,3,3-pentafluoropropene by hydrogenating 2-chloro-1,1,3,3,3-pentafluoropropene in the presence of a catalyst comprising at least one member selected from palladium, platinum and rhodium at a temperature of particularly 30 to 450 °C. A process for producing 1,1,3,3,3-pentafluoropropene by dechlorinating 1,1,1,3,3-pentafluoro-2,3-dichloropropane with hydrogen in the presence of a metal oxide catalyst. These processes can provide 1,1,1,3,3-pentafluoropropane and/or 1,1,3,3,3-pentafluoropropene in high yields.
摘要翻译：一种通过在钯催化剂存在下在40-300℃下在气相中用氢气还原1,1,1,3,3,3-五氟丙烯制备1,1,1,3,3-五氟丙烷的方法。一种生产1,1,1,3,3-五氟丙烷和/或1,1,3,3,3-五氟丙烯的方法，该方法是通过在2-氯-1,1,3,3,3-五氟丙烯存在下氢化2-氯-1,1,3,3,3-五氟丙烯包含选自钯，铂和铑中的至少一种的催化剂，在特别是30至450℃的温度下进行。通过在金属氧化物催化剂存在下用氢气脱氯1,1,1,3,3-五氟-2,3-二氯丙烷生产1,1,3,3,3-五氟丙烯的方法。这些方法可以以高收率提供1,1,1,3,3-五氟丙烷和/或1,1,3,3,3-五氟丙烯。

7. 发明授权

EP0703207B1 PROCESS FOR PRODUCING 1,1,1,3,3-PENTAFLUOROPROPANE AND/OR 1,1,3,3,3-PENTAFLUOROPROPENE 失效
标题翻译：用于生产1,1,1,3,3-五氟丙烷和/或1,1,3,3,3-五氟丙烯
公开(公告)号：EP0703207B1
公开(公告)日：2000-01-26
申请号：EP94916420.6
申请日：1994-05-30
申请人： DAIKIN INDUSTRIES, LTD.
发明人： YAMAMOTO, Akinori , SEKI, Eiji , AOYAMA, Hirokazu , NAKADA, Tatsuo
IPC分类号： C07C19/08 , C07C21/18 , C07C17/00 , B01J23/26 , B01J23/42 , B01J23/44 , B01J23/46 , B01J23/74 , B01J23/78 , B01J23/86
CPC分类号： C07C19/08 , C07C17/00 , C07C17/23 , C07C17/354 , C07C21/18
摘要： A process for producing 1,1,1,3,3-pentafluoropropane by reducing 1,1,1,3,3,3-pentafluoropropene with hydrogen in the presence of a palladium catalyst in vapor phase at 40 to 300 °C. A process for producing 1,1,1,3,3-pentafluoropropane and/or 1,1,3,3,3-pentafluoropropene by hydrogenating 2-chloro-1,1,3,3,3-pentafluoropropene in the presence of a catalyst comprising at least one member selected from palladium, platinum and rhodium at a temperature of particularly 30 to 450 °C. A process for producing 1,1,3,3,3-pentafluoropropene by dechlorinating 1,1,1,3,3-pentafluoro-2,3-dichloropropane with hydrogen in the presence of a metal oxide catalyst. These processes can provide 1,1,1,3,3-pentafluoropropane and/or 1,1,3,3,3-pentafluoropropene in high yields.

8. 发明授权

EP0716065B1 PROCESS FOR PRODUCING HEXAFLUOROCYCLOBUTENE AND PROCESS FOR PRODUCING HEXAFLUOROCYCLOBUTANE 失效
标题翻译：生产六氟环丁烯的方法和生产六氟环戊烷的方法
公开(公告)号：EP0716065B1
公开(公告)日：1999-07-14
申请号：EP94923068.4
申请日：1994-08-03
申请人： DAIKIN INDUSTRIES, LTD.
发明人： NAKADA, Tatsuo , AOYAMA, Hirokazu , YAMAMOTO, Akinori
IPC分类号： C07C23/06 , C07C17/23 , C07C17/354 , B01J21/08 , B01J23/26 , B01J23/74 , B01J23/86 , B01J27/138 , B01J23/44 , B01J23/46 , C07C17/281
CPC分类号： C07C23/06 , B01J23/464 , C07C17/23 , C07C17/281 , C07C17/354
摘要： A process for producing hexafluorocyclobutene by dechlorinating 1,2-dichlorohexafluorocyclobutane with hydrogen in the presence of a metal oxide and/or silicon oxide catalyst. A process for producing (Z)-1,2,3,3,4,4-hexafluorocyclobutane either by reducing hexafluorocyclobutene with hydrogen in a vapor phase in the presence of a palladium catalyst or by hydrogenating (reducing with hydrogen) 1,2-dichlorohexafluorocyclobutane in the presence of a rhodium catalyst. An inexpensively available 1,2-dichlorohexafluorocyclobutane can readily be converted into hexafluorocyclobutene in one step at an excellent selectivity. Further it is possible to produce (Z)-1,2,3,3,4,4-hexafluorocyclobutane in a high yield.
摘要翻译：一种在金属氧化物和/或氧化硅催化剂存在下用1,2-二氯六氟环丁烷与氢气脱氯生产六氟环丁烯的方法。一种生产（Z）-1,2,3,3,4,4-六氟环丁烷的方法，其通过在钯催化剂存在下用气相中的氢气还原六氟环丁烯或通过氢化（用氢还原）二氯六氟环丁烷在铑催化剂存在下反应。廉价可得的1,2-二氯六氟环丁烷可以容易地以极好的选择性一步转化成六氟环丁烯。此外，可以以高收率生产（Z）-1,2,3,3,4,4-六氟环丁烷。

9. 发明授权

EP0703208B1 Method of producing 1,1,1,3,3-pentafluoropropane 失效
标题翻译：一种生产1,1,1,3,3-五氟丙烷的过程
公开(公告)号：EP0703208B1
公开(公告)日：1999-04-07
申请号：EP94916422.2
申请日：1994-05-30
申请人： DAIKIN INDUSTRIES, LTD.
发明人： YAMAMOTO, Akinori , SEKI, Eiji , AOYAMA, Hirokazu , TAKUBO, Seiji , NAKADA, Tatsuo
IPC分类号： C07C19/08 , C07C21/18 , C07C17/00 , C07C17/10 , C07C17/20 , B01J23/42 , B01J23/44 , B01J23/46 , B01J21/04 , B01J23/26 , B01J27/10
CPC分类号： C07C19/08 , B01J23/44 , C07C17/06 , C07C17/10 , C07C17/206 , C07C17/21 , C07C17/23 , C07C19/10 , C07C21/18
摘要： 1,1,1,3,3-pentafluoropropane is produced by hydrogenating 2,2,3-trichloro-1,1,1,3,3-pentafluoropropane with at least 4.5 times by equivalent as much hydrogen in the presence of a noble metal catalyst, particularly a palladium catalyst in vapor phase. The 1,1,1,3,3-pentafluoropropane is also produced by chlorofluorinating propane, propene, hexachloropropene, etc., in the presence of a metallic catalyst into 2,2,3-trichloro-1,1,1,3,3-pentafluoropropane and reducing the product with hydrogen in the presence of a noble metal catalyst. It is possible to produce 2,2,3-trichloro-1,1,1,3,3-pentafluoropropane and 1,1,1,3,3-pentafluoropropane efficiently and economically.

10. 发明公开

EP0703208A1 PROCESS FOR PRODUCING 1,1,1,3,3-PENTAFLUOROPROPANE, PROCESS FOR PRODUCING 2,2,3-TRICHLORO-1,1,1,3,3-PENTAFLUOROPROPANE, AND PROCESS FOR PRODUCING 2,2,3-TRICHLORO-1,1,1-TRIFLUOROPROPANE 失效
标题翻译：用于生产1,1,1,3,3-五氟丙烷，用于生产2,2,3-三氯1,1,1,3,3-五氟丙烷及其制造方法2,2,3 三氯1,1,1-三氟
公开(公告)号：EP0703208A1
公开(公告)日：1996-03-27
申请号：EP94916422.2
申请日：1994-05-30
申请人： DAIKIN INDUSTRIES, LTD.
发明人： YAMAMOTO, Akinori , SEKI, Eiji , AOYAMA, Hirokazu , TAKUBO, Seiji , NAKADA, Tatsuo
IPC分类号： C07C19/08 , C07C21/18 , C07C17/00 , C07C17/10 , C07C17/20 , B01J23/42 , B01J23/44 , B01J23/46 , B01J21/04 , B01J23/26 , B01J27/10
CPC分类号： C07C19/08 , B01J23/44 , C07C17/06 , C07C17/10 , C07C17/206 , C07C17/21 , C07C17/23 , C07C19/10 , C07C21/18
摘要： 1,1,1,3,3-pentafluoropropane is produced by hydrogenating 2,2,3-trichloro-1,1,1,3,3-pentafluoropropane with at least 4.5 times by equivalent as much hydrogen in the presence of a noble metal catalyst, particularly a palladium catalyst in vapor phase. The 1,1,1,3,3-pentafluoropropane is also produced by chlorofluorinating propane, propene, hexachloropropene, etc., in the presence of a metallic catalyst into 2,2,3-trichloro-1,1,1,3,3-pentafluoropropane and reducing the product with hydrogen in the presence of a noble metal catalyst. It is possible to produce 2,2,3-trichloro-1,1,1,3,3-pentafluoropropane and 1,1,1,3,3-pentafluoropropane efficiently and economically.
摘要翻译： 1,1,1,3,3-五氟丙烷是通过在贵金属存在下，通过氢化等效2,2,3-三氯-1,1,1,3,3-五氟丙烷与至少4.5倍之多氢产生金属催化剂，特别是在汽相钯催化剂。因此，1,1,1,3,3-五氟丙烷是由chlorofluorinating丙烷，丙烯，六氯丙烯，等等，在存在金属催化剂的成2,2,3-三氯1,1,1,3-产生 1,1,1,3,3-五氟丙烷和减少与氢的产物在贵金属催化剂的存在下进行。它可以产生2,2,3-三氯1,1,1,3,3-五氟丙烷和1,1,1,3,3-五氟丙烷有效和经济。

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