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1. 发明公开

EP1954728A1 VERFAHREN ZUR HERSTELLUNG VON HOCHREAKTIVEN ISOBUTENHOMO- ODER -COPOLYMEREN AUS TECHNISCHEN C4-KOHLENWASSERSTOFFSTRÖMEN MITTELS PROTONENSAURER KATALYSATORKOMPLEXE 审中-公开
标题翻译：工艺用于生产技术C4烃流高活性异丁烯均聚物或共聚物BY质子酸催化剂络合物
公开(公告)号：EP1954728A1
公开(公告)日：2008-08-13
申请号：EP06819482.8
申请日：2006-11-15
申请人： BASF SE
发明人： HANEFELD, Phillip , BÖHM, Volker , SIGL, Marcus , CHALLAND, Nina , RÖPER, Michael , WALTER, Hans-Michael
IPC分类号： C08F10/10 , C08F4/52
CPC分类号： C08F10/10 , C08F110/10 , C08F4/52 , C08F2500/04
摘要： The invention relates to the production of highly reactive isobutylene homo- or copolymers with Mn = 500 to 1,000,000 by polymerizing isobutylene from technical flows of C4-hydrocarbon having a isobutylene content ranging from 1 to 90 % by weight in liquid phase in the presence of a dissolved, dispersed or supported catalyst complex by using, as a catalyst complex, a Bronsted acid compound (I) [H+]k Yk- Lx (I) Yk- weakly coordinating k-valent anion, which contains at least one carbon-containing grouping; L represents neutral solvent molecules, and; x = 0.

2. 发明授权

EP2282986B1 VERFAHREN ZUR HERSTELLUNG VON AROMATISCHEN UND HETEROAROMATISCHEN CARBONSÄUREN, CARBONSÄUREESTERN UND CARBONSÄUREAMIDEN 有权
标题翻译：用于生产芳族和杂芳族羧酸，羧酸和羧酸酯的酰胺
公开(公告)号：EP2282986B1
公开(公告)日：2017-04-19
申请号：EP09753852.4
申请日：2009-05-25
申请人： BASF SE
发明人： CHALLAND, Nina , ALTENHOFF, Ansgar, Gereon , SCHMIDT-LEITHOFF, Joachim , WISSEL-STOLL, Kathrin , RACK, Michael , RHEINHEIMER, Joachim
IPC分类号： C07C51/10 , C07C67/36 , C07C231/00 , C07C231/02 , C07C63/04 , C07C69/76 , C07C235/84 , C07C231/10
CPC分类号： C07C231/10 , C07C51/10 , C07C67/36 , C07C63/04 , C07C69/76 , C07C235/84

3. 发明公开

EP2282986A1 VERFAHREN ZUR HERSTELLUNG VON AROMATISCHEN UND HETEROAROMATISCHEN CARBONSÄUREN, CARBONSÄUREESTERN UND CARBONSÄUREAMIDEN 有权
标题翻译：用于生产芳族和杂芳族羧酸，羧酸和羧酸酯的酰胺
公开(公告)号：EP2282986A1
公开(公告)日：2011-02-16
申请号：EP09753852.4
申请日：2009-05-25
申请人： BASF SE
发明人： CHALLAND, Nina , ALTENHOFF, Ansgar, Gereon , SCHMIDT-LEITHOFF, Joachim , WISSEL-STOLL, Kathrin , RACK, Michael , RHEINHEIMER, Joachim
IPC分类号： C07C51/10 , C07C67/36 , C07C231/00 , C07C231/02 , C07C63/04 , C07C69/76 , C07C235/84
CPC分类号： C07C231/10 , C07C51/10 , C07C67/36 , C07C63/04 , C07C69/76 , C07C235/84
摘要： Method for producing aromatic and heteroaromatic carboxylic acids, carboxylic acid esters and carboxylic acid amides through the reacting of aromatic or heteroaromatic halogenides R-X
n , where n = a whole number from 1 to 6, R = a substituted or unsubstituted, aromatic or heteroaromatic radical and X = a chlorine, bromine or iodine atom; with carbon monoxide and water, ammonia, alcohols or amines in the presence of bases and nonvalent or bivalent palladium compounds and bidentate diphosphanes or complexes of nonvalent or bivalent palladium with bidentate diphosphanes, in which bidentate diphosphanes are used (R
1- )(R
2- )P-Y-P(-R
3 )(-R
4 ), with R
1 to R
4 =, unsubstituted aryl radicals or aryl radicals that are substituted with at least one radical having a positive resonance effect or a positive inductive effect, or unsubstituted or substituted cycloalkyl radicals; and Y = hydrocarbon groups with a total of 2 to 20 carbon atoms, wherein at least one of the carbon atoms carried only one or no hydrogen atom as a substituent; excepting the reaction of 4-bromo-3-difluoromethyl-1 -methylpyrazol with 2-(3,4,5-trifluoorphenyl)aniline and carbon monoxide to form N-[2-(3,4,5-Trifluorophenyl)phenyl]-3- difluoromethyl-1 -methylpyrazol-4-carboxylic acid amide.
摘要翻译：过程用于制备芳族和杂芳族羧酸，羧酸酯和羧酰胺通过芳族或杂芳族卤化物R-Xn中的反应，其中n =整数1〜6，R = substituiertem奥德unsubstituiertem和芳族或杂芳族基团和X =氯，溴或碘原子，与一氧化碳和水，氨，在碱和零价或二价钯化合物和双齿diphosphanes或零价或二价钯与二齿diphosphanes的络合物的存在下的醇或cardamines，其中使用了二齿diphosphanes（R1 - ）的（R 2）p-Y-P（-R 3）（ - R 4），其中R 1至R 4 =芳基unsubstituiertem自由基或芳基用至少一个基团表现出正的共振效应substituiertem 或正感应效应，或unsubstituiertem或substituiertem环烷基，和Y =烃基含总共2至20个碳原子，其中至少部分的碳原子中的一个仅携带一个或没有水合罗根原子作为取代基; 除了4-溴-3-二氟甲基-1-甲基吡的反应与2-（3,4,5-三氟苯基）苯胺和一氧化碳，得到N- [2-（3,4,5-三氟苯基）苯基] -3-二氟甲基-1-甲基吡唑-4-甲酰胺。

4. 发明授权

EP2632909B1 VERFAHREN ZUR HERSTELLUNG VON 1,4-BISHYDROXYETHYL-PIPERAZIN 有权
标题翻译：用于生产1,4-二羟基乙基哌嗪
公开(公告)号：EP2632909B1
公开(公告)日：2015-02-25
申请号：EP11776413.4
申请日：2011-10-26
申请人： BASF SE
发明人： WIGBERS, Christof Wilhelm , CHALLAND, Nina , MELDER, Johann-Peter , RHEUDE, Udo , DOSTALEK, Roman
IPC分类号： C07D295/088
CPC分类号： C07D295/088

5. 发明授权

EP2164831B1 VERFAHREN ZUR HERSTELLUNG N-SUBSTITUIERTER (3-DIHALOMETHYL-1-METHYL-PYRAZOL-4-YL)CARBOXAMIDE 有权
标题翻译： METHOD FOR PRODUCING N-取代的（3-二卤代-1-甲基吡唑-4-基）羧酰胺
公开(公告)号：EP2164831B1
公开(公告)日：2013-07-17
申请号：EP08760299.1
申请日：2008-05-30
申请人： BASF SE
发明人： ZIERKE, Thomas , RHEINHEIMER, Joachim , RACK, Michael , SMIDT, Sebastian Peer , ALTENHOFF, Ansgar Gereon , SCHMIDT-LEITHOFF, Joachim , CHALLAND, Nina
IPC分类号： C07D231/14
CPC分类号： C07D231/14

6. 发明公开

EP2164831A1 VERFAHREN ZUR HERSTELLUNG N-SUBSTITUIERTER (3-DIHALOMETHYL-1-METHYL-PYRAZOL-4-YL)CARBOXAMIDE 有权
标题翻译： METHOD FOR PRODUCING N-取代的（3-二卤代-1-甲基吡唑-4-基）羧酰胺
公开(公告)号：EP2164831A1
公开(公告)日：2010-03-24
申请号：EP08760299.1
申请日：2008-05-30
申请人： BASF SE
发明人： ZIERKE, Thomas , RHEINHEIMER, Joachim , RACK, Michael , SMIDT, Sebastian Peer , ALTENHOFF, Ansgar Gereon , SCHMIDT-LEITHOFF, Joachim , CHALLAND, Nina
IPC分类号： C07D231/14
CPC分类号： C07D231/14
摘要： The present invention relates to a method for the production of n-substituted (3-dihalomethyl-1-methyl-pyrazole-4-YL) carboxamides of the formula (I), wherein R1 stands for optionally substituted phenyl or C3-C7-cycloalkyl, R1a stands for hydrogen or fluorine, or R1a together with R1 stands for optionally substituted C3-C5-alkyandiyl or C5-C7-cycloalkandiyl, R2 stands for C1-C6-alkyl, C2-C6-alkenyl, C2-C6-alkinyl or C1-C4-alkoxy-C1-C2-alkyl, X stands for F or Cl, and n stands for 0, 1, 2, or 3, said method comprising A) providing a compound of the formula (II), wherein X stands for F or Cl, Y for Cl or Br, and R2 has one of the above-mentioned meanings, and B) the reaction of a compound of the formula (II) with carbon monoxide and a compound of the formula (III), wherein R1, R1a and n have one of the above-mentioned meanings; in the presence of a palladium catalyst; the intermediate products used for the production according to the inventive method; and methods for the production thereof.

7. 发明公开

EP2858978A1 VERFAHREN ZUR HERSTELLUNG VON PIPERAZIN 审中-公开
标题翻译：用于生产哌
公开(公告)号：EP2858978A1
公开(公告)日：2015-04-15
申请号：EP13725699.6
申请日：2013-05-29
申请人： BASF SE
发明人： BOU CHEDID, Roland , MELDER, Johann-Peter , ABEL, Ulrich , DOSTALEK, Roman , CHALLAND, Nina , STEIN, Bernd , JÖDECKE, Michael
IPC分类号： C07D295/023 , C07C211/10 , C07C211/14
CPC分类号： C07D295/023 , C07C209/16 , C07C211/13 , C07C211/10 , C07C211/14
摘要： Method for preparing piperazine of formula I by reacting diethanolamine (DEOA) of formula II with ammonia in the presence of hydrogen and a metal-containing supported catalyst. Before the catalyst is reduced with hydrogen, the catalytically active mass of the catalyst contains oxygen-containing aluminum, copper, nickel and cobalt compounds and 0.2 to 5.0 wt.% oxygen-containing tin compounds calculated as SnO, and the reaction is carried out in the liquid phase at an absolute pressure ranging from 160 to 220 bar, at a temperature ranging from 180 to 220°C, ammonia is used at a molar ratio ranging from 5 to 25 in relation to the DEOA used in the process, the method being carried out in the presence of 0.2 to 9.0 wt.% hydrogen relative to the total amount of DEOA and ammonia used in the process.

8. 发明公开

EP2632909A1 VERFAHREN ZUR HERSTELLUNG VON 1,4-BISHYDROXYETHYL-PIPERAZIN 有权
标题翻译：用于生产1,4-二羟基乙基哌嗪
公开(公告)号：EP2632909A1
公开(公告)日：2013-09-04
申请号：EP11776413.4
申请日：2011-10-26
申请人： BASF SE
发明人： WIGBERS, Christof Wilhelm , CHALLAND, Nina , MELDER, Johann-Peter , RHEUDE, Udo , DOSTALEK, Roman
IPC分类号： C07D295/088
CPC分类号： C07D295/088
摘要： A process for preparing 1,4-bishydroxyethylpiperazine (BHEPIP) of the formula I, characterized in that diethanolamine (DEOA) of the formula II is converted in a reactor at a temperature in the range from 130 to 300°C in the presence of a copper-containing, chromium-free heterogeneous catalyst in the liquid phase.

9. 发明公开

EP2139837A1 VERFAHREN ZUR HERSTELLUNG VON AMEISENSÄURE 审中-公开
标题翻译： VERFAHREN ZUR HERSTELLUNG VONAMEISENSÄURE
公开(公告)号：EP2139837A1
公开(公告)日：2010-01-06
申请号：EP08717979.2
申请日：2008-03-18
申请人： BASF SE
发明人： CHALLAND, Nina , SAVA, Xavier , RÖPER, Michael
IPC分类号： C07C51/00 , C07C51/02 , C07C53/06 , C07C53/02
CPC分类号： C07C51/00 , B01J31/0202 , B01J31/0237 , B01J31/0271 , B01J31/2404 , B01J2231/625 , B01J2531/821 , C07C51/02 , C07C53/06 , C07C53/02
摘要： The invention relates to a method for producing formic acid by generating the corresponding ammonium formate by means of catalytic hydrogenation of carbon dioxide with hydrogen on a catalyst comprising a metal of groups 8 through 10 of the periodic system, in the presence of a primary, secondary, and/or tertiary amine, and by cleaving the ammonium formate by heating it in formic acid and the amine, characterized in that the primary, secondary, or tertiary amine is selected from the amines of formula I or the mixtures thereof, R1 through R3 being identical or different and being hydrogen, linear or branched alkyl radicals having 1 to 18 carbon atoms, cycloaliphatic radicals having 5 to 7 carbon atoms, aryl radicals and/or aryl alkyl radicals, at least one of the radicals R1 to R3 carrying a hydroxyl group, and that said hydrogenation is performed in a solvent having a boiling point of ≥105°C at normal pressure, and that the formic acid is obtained in the hydrogenation reaction mixture comprising the high-boiling solvent by thermal cleavage of the ammonium formate and distillation of the formic acid.
摘要翻译：本发明涉及一种生产甲酸的方法，该方法通过在含有周期系统第8-10族金属的催化剂上，用二氧化碳用氢催化氢化，在伯，仲，和/或叔胺，并且通过在甲酸和胺中将甲酸铵加热裂解甲酸铵，其特征在于伯胺，仲胺或叔胺选自式I的胺或其混合物，R1至R3 相同或不同并且是氢，具有1至18个碳原子的直链或支链烷基，具有5至7个碳原子的环脂族基团，芳基和/或芳基烷基，至少一个基团R 1至R 3携带羟基并且所述氢化在常压下在沸点≥105℃的溶剂中进行，并且甲酸在氢化反应混合物中获得 e通过甲酸铵的热裂解和甲酸的蒸馏包含高沸点溶剂。

10. 发明公开

EP1954727A1 VERFAHREN ZUR HERSTELLUNG VON HOCHREAKTIVEN ISOBUTENHOMO- ODER -COPOLYMEREN MITTELS BORHALTIGER KATALYSATORKOMPLEXE 审中-公开
标题翻译：用于生产高活性异丁烯均聚物或含硼BY催化剂络合物共聚物
公开(公告)号：EP1954727A1
公开(公告)日：2008-08-13
申请号：EP06807816.1
申请日：2006-11-15
申请人： BASF SE
发明人： HANEFELD, Phillip , BÖHM, Volker , SIGL, Marcus , CHALLAND, Nina , RÖPER, Michael , WALTER, Hans-Michael , VOIT, Brigitte , KUEHN, Fritz, Elmar , HIJAZI, Ahmed , NARAYANAN, Radha, Krishnan
IPC分类号： C08F10/10 , C07F5/02 , C08F4/52
CPC分类号： C07F5/027 , C08F10/10 , C08F110/10 , C08F4/52 , C08F2500/04
摘要： The invention relates to the production of highly reactive isobutylene homo- or copolymers with Mn = 500 to 45,000 by polymerizing isobutylene in liquid phase in the presence of a dissolved, dispersed or supported boron-containing catalyst complex by using, as a catalyst complex, a Bronsted compound (I) [H+]m+1 [R1R2R3B-(-Am+-BR5R6-)n-R4](m+1)- Lx (I), in which: R1 to R6 represent aliphatic, heterocyclic or aromatic fluorine-containing hydrocarbon radicals, which are independent of one another and which each have 1 to 18 carbon atoms or silyl groups containing C1 to C18 hydrocarbon radicals; A represents a bridge member that, via its nitrogen atoms forms bonds which are covalent to the boron atoms; L represents neutral solvent molecules; n = 0 or 1; m = 0 or 1, and; x ≥ 0.

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