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1. 发明授权

EP1169119B1 ROHRBÜNDELREAKTOR, INSBESONDERE FÜR KATALYTISCHE GASPHASENREAKTIONEN 有权
标题翻译：管式反应器，尤其气相催化反应的
公开(公告)号：EP1169119B1
公开(公告)日：2003-10-15
申请号：EP00926738.6
申请日：2000-03-15
申请人： BASF AKTIENGESELLSCHAFT
发明人： OLBERT, Gerhard , CORR, Franz , REUTER, Peter , WAMBACH, Ludwig , HAMMON, Ulrich
IPC分类号： B01J8/06 , B01J19/24 , B01J19/00
CPC分类号： C07C45/35 , B01J8/067 , B01J19/0013 , B01J19/2425 , B01J2208/00212 , B01J2208/00221 , B01J2208/00256 , B01J2219/00094 , B01J2219/00103 , C07C45/38 , C07C47/22 , C07C47/127
摘要： The invention relates to a multi-tube fixed-bed reactor and to the use of a reactor of this type for carrying out catalytic gas phase reactions, especially for carrying out exothermic or endothermic catalytic gas phase reactions such as producing phthalic anhydride (PSA), acrylic acid (AA), methacrylic acid (MAA), acrolein, maleic anhydride (MSA), glyoxal, phosgene, hydrogen cyanide or vinyl formamide (VFA). According to the invention, in the case of larger reactors where a considerable reaction heat is produced or required and must be dissipated as a result of the numerous reaction tubes (17), the ratio of tube distribution t to tube outer diameter da is made dependant on the reactor diameter or the tube bundle diameter dRBa. If the outer diameter of the reaction tube bundle (18) is more than 4 metres, a ratio of tube distribution t to tube outer diameter da of at least 1.3 is preferred.

2. 发明公开

EP1169119A2 ROHRBÜNDELREAKTOR, INSBESONDERE FÜR KATALYTISCHE GASPHASENREAKTIONEN 有权
标题翻译：管式反应器，尤其气相催化反应的
公开(公告)号：EP1169119A2
公开(公告)日：2002-01-09
申请号：EP00926738.6
申请日：2000-03-15
申请人： BASF AKTIENGESELLSCHAFT
发明人： OLBERT, Gerhard , CORR, Franz , REUTER, Peter , WAMBACH, Ludwig , HAMMON, Ulrich
IPC分类号： B01J8/00
CPC分类号： C07C45/35 , B01J8/067 , B01J19/0013 , B01J19/2425 , B01J2208/00212 , B01J2208/00221 , B01J2208/00256 , B01J2219/00094 , B01J2219/00103 , C07C45/38 , C07C47/22 , C07C47/127
摘要： The invention relates to a multi-tube fixed-bed reactor and to the use of a reactor of this type for carrying out catalytic gas phase reactions, especially for carrying out exothermic or endothermic catalytic gas phase reactions such as producing phthalic anhydride (PSA), acrylic acid (AA), methacrylic acid (MAA), acrolein, maleic anhydride (MSA), glyoxal, phosgene, hydrogen cyanide or vinyl formamide (VFA). According to the invention, in the case of larger reactors where a considerable reaction heat is produced or required and must be dissipated as a result of the numerous reaction tubes (17), the ratio of tube distribution t to tube outer diameter da is made dependant on the reactor diameter or the tube bundle diameter dRBa. If the outer diameter of the reaction tube bundle (18) is more than 4 metres, a ratio of tube distribution t to tube outer diameter da of at least 1.3 is preferred.

3. 发明授权

EP1064246B1 VERFAHREN ZUR HERSTELLUNG VON CARBONYLVERBINDUNGEN 有权
标题翻译：用于生产羰基
公开(公告)号：EP1064246B1
公开(公告)日：2004-06-23
申请号：EP99939843.1
申请日：1999-02-25
申请人： BASF AKTIENGESELLSCHAFT
发明人： DEMUTH, Dirk , FETZER, Thomas , PRATSCH, Volker , WENDRICH, Thomas , MENIG, Helmuth , WAMBACH, Ludwig , HARTH, Klaus
IPC分类号： C07C45/38 , C07C45/39 , C07C47/127 , C07C47/04
CPC分类号： C07C45/39 , C07C45/38 , C07C47/04 , C07C47/127

4. 发明公开

EP1064246A1 VERFAHREN ZUR HERSTELLUNG VON CARBONYLVERBINDUNGEN 有权
标题翻译：用于生产羰基
公开(公告)号：EP1064246A1
公开(公告)日：2001-01-03
申请号：EP99939843.1
申请日：1999-02-25
申请人： BASF AKTIENGESELLSCHAFT
发明人： DEMUTH, Dirk , FETZER, Thomas , PRATSCH, Volker , WENDRICH, Thomas , MENIG, Helmuth , WAMBACH, Ludwig , HARTH, Klaus
IPC分类号： C07C45/38 , C07C45/39 , C07C47/127 , C07C47/04
CPC分类号： C07C45/39 , C07C45/38 , C07C47/04 , C07C47/127
摘要： The invention relates to a method for producing carbonyl compounds of formula (I), wherein R1 is a hydrogen atom or an alkyl radical with 1 to 3 C-atoms and R2 is a hydrogen atom, a C¿2?-C4-alkenyl radical which can be unsubstituted or substituted one to three times with C1-C3-alkyl or a radical of formula (II), wherein R?3¿ is a hydrogen atom or an oxygen atom together with R4, R4 is the radical OR6 or an oxygen atom together with R3, R5 is a hydrogen atom, an alkyl radical with 1 to 8 C-atoms, a C¿2?-C4-alkenyl radical which can be unsubstituted or substituted one to three times with C1-C3-alkyl or a cyclohexyl or cyclopentyl radical and R?6¿ is an alkyl radical with 1 to 4 C-atoms, a cyclohexyl or cyclopentyl radical or a radical of formula -CH¿2?-CHO or -CH2-CH2-O-CH2-CHO by gas phase oxidation of methanol or alcohols of formula (III), wherein R?1 and R5¿ have the meaning given above and R7 is a hydrogen atom or a radical OR?8 and R8¿ is a hydrogen atom, an alkyl radical with 1 to 4 C-atoms, a cyclohexyl or cyclopentyl radical or a radical of formula -CH¿2?-CH2-OH or -CH2-CH2-O-CH2-OH with an oxygen-containing gas in the presence of catalysts containing copper and/or silver and optionally, a phosphor compound which is volatile in the reaction conditions, the quantity of phosphor (calculated as P) being up to 20 ppm in relation to the quantity in weight of alcohol used. The inventive method is characterised in that it uses a catalyst system consisting of one catalyst which is essentially phosphor-free and at least one catalyst containing phosphor-containing copper and/or silver.

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