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1. 发明公开

EP1836146A1 VERFAHREN ZUR HERSTELLUNG VON PROPEN AUS PROPAN 有权
公开(公告)号：EP1836146A1
公开(公告)日：2007-09-26
申请号：EP06700188.3
申请日：2006-01-04
申请人： BASF AKTIENGESELLSCHAFT
发明人： CRONE, Sven , MACHHAMMER, Otto , SCHINDLER, Götz-Peter , BORGMEIER, Frieder
IPC分类号： C07C5/327 , C07C7/11 , C07C7/04
CPC分类号： C07C5/3337 , C07C7/11 , C07C11/06
摘要： A) A feed stream containing propane is prepared, B) the feed stream containing propane, optionally steam and optionally an oxygen-containing gas stream are fed to a dehydrogenation zone and propane undergoes a dehydrogenation to give propene, whereby a product gas stream b is obtained containing propane, propene, methane, ethane, ethene, carbon monoxide, carbon dioxide, steam, optionally hydrogen and optionally oxygen, C) the product gas stream b is cooled, optionally compressed and steam separated off by condensation, to give a product gas stream c stripped of steam, D) the product gas stream c is brought into contact with a selective inert absorption agent which selectively absorbs propene in a first absorption zone, to give an essentially propane-charged absorption agent stream d1 and a gas stream d2 containing propane, methane, ethane, ethene, carbon monoxide, carbon dioxide and hydrogen, E) the absorption agent stream d1 is optionally depressurised in a first desorption zone, to give an essentially propene-charged absorption agent stream e1 and a gas stream e2, containing propene, said gas stream e2 being recycled into the first absorption zone and F) a propene-containing gas stream f1 is released from the essentially propene-charged absorption agent stream d1 and e1 in at least one second desorption zone by depressurization, heating and/or stripping of the absorption agent stream d1 and e1 with recycling of the selective absorption agent.
摘要翻译： A）制备含有丙烷的进料流，B）将含有丙烷，任选的蒸汽和任选的含氧气流的进料流进料至脱氢区，并将丙烷脱氢生成丙烯，由此产物气流b为得到含有丙烷，丙烯，甲烷，乙烷，乙烯，一氧化碳，二氧化碳，蒸汽，任选的氢气和任选的氧气，C）将产物气流b冷却，任选压缩并通过冷凝分离出蒸汽，得到产物气体 d）将产物气流c与选择性吸收剂接触，所述选择性惰性吸收剂选择性吸收第一吸收区中的丙烯，得到基本上丙烷加入的吸收剂流d1和含有丙烷，甲烷，乙烷，乙烯，一氧化碳，二氧化碳和氢气，E）吸收剂料流d1任选地在第一解吸区中减压至g 基本上丙烯的吸收剂流e1和含丙烯的气流e2，所述气流e2被再循环到第一吸收区中，并且F）含丙烯的气流f1从基本上带丙烯的吸收剂释放在至少一个第二解吸区中通过吸收剂流d1和e1的减压，加热和/或汽提以及选择性吸收剂的再循环来产生流d1和e1。

2. 发明公开

EP1615870A2 VERFAHREN DER HETEROGEN KATALYSIERTEN PARTIELLEN DIREKTEN OXIDATION VON PROPAN UND/ODER ISO-BUTAN ZU ACRYLSÄURE UND/ODER METHACRYLSÄURE 有权
标题翻译：过程用于丙烯酸和/或甲基丙烯酸丙烷和/或异丁烷非均相催化部分直接氧化
公开(公告)号：EP1615870A2
公开(公告)日：2006-01-18
申请号：EP04726111.0
申请日：2004-04-07
申请人： BASF Aktiengesellschaft
发明人： MACHHAMMER, Otto , CRONE, Sven , BORGMEIER, Frieder , MÜLLER-ENGEL, Klaus, Joachim , ADAMI, Christoph , DIEFENBACHER, Armin
IPC分类号： C07C57/05
CPC分类号： C07C51/215 , C07C57/04
摘要： Disclosed is a method for the heterogeneously catalyzed partial direct oxidation of propane and/or isobutane. According to said method, target product is separated from the product gas mixture obtained in the reaction stage in a reprocessing stage, the remaining product gas mixture is divided into two partial quantities having the same composition, one partial quantity is redirected into the reaction stage while the other partial quantity is discharged, and both the reaction stage and the reprocessing stage are operated at an increased pressure.

3. 发明公开

EP1546074A1 VERFAHREN ZUR HERSTELLUNG VON WENIGSTENS EINEM PARTIELLEN OXIDATIONS- UND/ODER AMMOXIDATIONSPRODUKT DES PROPYLENS 有权
标题翻译：工艺用于生产至少一个部分氧化和/或丙烯氨氧化
公开(公告)号：EP1546074A1
公开(公告)日：2005-06-29
申请号：EP03798911.8
申请日：2003-09-18
申请人： BASF AKTIENGESELLSCHAFT
发明人： HECHLER, Claus , SCHINDLER, Götz-Peter , PETZOLDT, Jochen , ADAMI, Christoph , MACHHAMMER, Otto , MÜLLER-ENGEL, Klaus, Joachim , MARTAN, Hans
IPC分类号： C07C7/05 , C07C51/25 , C07C45/35 , C07C255/08 , C07C253/24 , C07D301/10 , C07C5/48 , C07C5/32 , C07C11/06
CPC分类号： C07C51/215 , B01J23/002 , B01J23/8877 , C07C51/252 , C07C253/24 , Y02P20/52 , C07C57/04 , C07C255/08
摘要： Disclosed is a method for producing at least one partial propylene oxidation and/or ammoxidation product, according to which the propylene is produced from raw propane by means of dehydration and is subjected to a heterogeneously catalyzed partial gas phase oxidation and/or partial gas phase ammoxidation in the presence of unreacted propane as a component of a gas mixture 2 having a total C4 hydrocarbon content of = 3 percent by volume.

4. 发明授权

EP1015411B1 VERFAHREN ZUR FRAKTIONIERTEN KONDENSATION EINES ACRYLSÄURE ODER METHACRYLSÄURE ENTHALTENDEN HEISSEN GASGEMISCHES MIT EINEM HOHEN ANTEIL NICHT KONDENSIERBARER KOMPONENTEN 有权
标题翻译：分凝丙烯酸或甲基丙烯酸的方法CONTAINING HOT气体混合物与高百分比的非冷凝组分
公开(公告)号：EP1015411B1
公开(公告)日：2003-06-11
申请号：EP98950022.8
申请日：1998-09-10
申请人： BASF AKTIENGESELLSCHAFT
发明人： ECK, Bernd , MACHHAMMER, Otto , PROLL, Theo , SCHLIEPHAKE, Volker , THIEL, Joachim , BRÖLLOS, Klaus
IPC分类号： C07C57/07
CPC分类号： B01D5/003 , C07C51/44 , C07C57/04
摘要： The invention relates to a method for the fractional condensation of a gas mixture which contains at least one other condensable constituent in addition to acrylic acid or methacrylic acid and which also has a high proportion of one or several non-condensable constituents. According to said method, the gas mixture is passed through a column with separation-efficient baffles and the condensable constituents are condensed out by cooling.

5. 发明公开

EP1109774A1 VERFAHREN ZUR HERSTELLUNG VON ACROLEIN UND/ODER ACRYLSÄURE AUS PROPAN 审中-公开
标题翻译： VERFAHREN ZUR HERSTELLUNG VON ACROLEIN UND / ODERACRYLSÄUREAUS PROPAN
公开(公告)号：EP1109774A1
公开(公告)日：2001-06-27
申请号：EP99941557.3
申请日：1999-08-10
申请人： BASF AKTIENGESELLSCHAFT
发明人： MACHHAMMER, Otto , TENTEN, Andreas , JACHOW, Harald , HAUPT, Susanne , ARNOLD, Heiko , UNVERRICHT, Signe
IPC分类号： C07C57/05 , C07C45/35 , C07C5/333
CPC分类号： C07C51/215 , C07C45/33 , C07C45/35 , C07C51/252 , C07C47/22 , C07C57/04
摘要： A method for producing acrolein and/or acrylic acid from propane, whereby the propane undergoes partial homogeneous and/or heterogeneous catalysed oxydehydrogenation in a first reaction step with molecular oxygen to form propane. The product gas mixture formed in the first reaction step is used to produce acrolein and/or acrylic acid by means of gas-phase catalytic propane oxidation. The method is characterised in that the molecular oxygen which is required in the first reaction area and is different from the recycled oxygen gas is added to the initial reaction gas mixture of the first reaction area as modified air containing nitrogen with the proviso that the nitrogen content of the modified air is lower than and the oxygen content of the modified air is greater than the corresponding air contents. The invention is further characterised in that at least one part of the molecular nitrogen contained in the flow of residual gas is separated from the residual gas flow before the residual gas flow is returned to the first reaction area.
摘要翻译：由丙烷生产丙烯醛和/或丙烯酸的方法，其中丙烷在第一反应步骤中与分子氧进行部分均相和/或多相催化氧化脱氢生成丙烷。在第一反应步骤中形成的产物气体混合物用于通过气相催化丙烷氧化生产丙烯醛和/或丙烯酸。该方法的特征在于，将第一反应区域所需的与再循环氧气不同的分子氧作为含有氮的改质空气添加到第一反应区域的初始反应气体混合物中，其条件是氮含量的改性空气的氧含量低于并且改性空气的氧含量大于相应的空气含量。本发明的特征还在于，在残余气流返回到第一反应区之前，残留气体流中所含的至少一部分分子氮与残余气流分离。

6. 发明公开

EP1833776A1 VERFAHREN ZUR HERSTELLUNG VON PROPEN AUS PROPAN 审中-公开
公开(公告)号：EP1833776A1
公开(公告)日：2007-09-19
申请号：EP05821810.8
申请日：2005-12-20
申请人： BASF AKTIENGESELLSCHAFT
发明人： MACHHAMMER, Otto , CRONE, Sven , SCHINDLER, Götz-Peter
IPC分类号： C07C5/333 , C07C11/06
CPC分类号： C07C5/3337 , C07C7/04 , C07C11/06
摘要： The invention relates to a method for the production of propene from propane comprising the steps: A) a feed gas stream containing propane is prepared, B) the feed gas stream containing propane a and an oxygen-containing gas stream are supplied to a dehydrogenation zone and propane is subjected to a non-oxidative catalytic autothermal dehydrogenation to give propene, whereby a product gas stream b containing propane, propene, methane, ethane, ethene, nitrogen, carbon monoxide, carbon dioxide, water vapour and hydrogen is obtained, C) the product gas stream b is cooled and water vapour separated off by condensation to give a product as stream c stripped of water vapour, D) non-condensable or low-boiling gas components are separated off by bringing the product gas stream c into contact with an inert absorption agent with subsequent desorption of the gases dissolved in the inert absorption agent, whereby a C3 hydrocarbon stream d1 and a waste-gas stream d2, containing methane, ethane, ethene, nitrogen, carbon monoxide, carbon dioxide and hydrogen are generated, E) the C3 hydrocarbon stream d1 is cooled and compressed, to give a liquid C3 hydrocarbon stream e1, F) the liquid C3 hydrocarbon stream e1 is fed to a first distillation zone and separated by distillation into a stream f1 containing propane and propene and a stream f2 containing ethane and ethene and G) the stream f1 is fed to a second distillation zone and separated by distillation into a product gas stream g1 of propene and a stream g2 of propane, whereby the stream g2 is at least partly recycled into the dehydrogenation zone.
摘要翻译：本发明涉及一种由丙烷生产丙烯的方法，其包括以下步骤：A）制备含有丙烷的进料气流，B）将含有丙烷a和含氧气流的进料气流供入脱氢区丙烷进行非氧化催化自热脱氢得到丙烯，由此得到含有丙烷，丙烯，甲烷，乙烷，乙烯，氮气，一氧化碳，二氧化碳，水蒸气和氢气的产物气流b，C）将产物气流b冷却并通过冷凝分离出水蒸汽，得到作为物流c的产物，汽提出水蒸气，D）通过使产物气流c与分离器接触，分离不可冷凝或低沸点气体组分惰性吸收剂，随后解吸溶解在惰性吸收剂中的气体，由此得到含有甲烷，乙烷，乙烯的C3烃物流d1和废气物流d2 产生一氧化碳，氮气，一氧化碳，二氧化碳和氢气，E）将C3烃物流d1冷却并压缩，得到液体C3烃物流e1，F）将液体C3烃物流e1进料到第一蒸馏区并通过蒸馏分离成含有丙烷和丙烯的料流f1和含有乙烷和乙烯的料流f2，和G）将料流f1供入第二蒸馏区并通过蒸馏分离成丙烯的产物气流g1和丙烷，由此将料流g2至少部分再循环到脱氢区中。

7. 发明授权

EP1537092B1 INTEGRIERTES VERFAHREN ZUR SYNTHESE VON PROPYLENOXID 有权
标题翻译：集成方法合成丙烯
公开(公告)号：EP1537092B1
公开(公告)日：2006-06-07
申请号：EP03790944.7
申请日：2003-08-29
申请人： BASF Aktiengesellschaft
发明人： BENDER, Michael , ZEHNER, Peter , MACHHAMMER, Otto , MÜLLER, Ulrich , HARTH, Klaus , SCHINDLER, Götz-Peter , JUNICKE, Henrik
IPC分类号： C07D301/12
CPC分类号： C07D301/12 , Y02P20/125 , Y02P20/582
摘要： The invention relates to an integrated method for synthesising propylene oxide, said method comprising at least the following steps: (i) dehydrogenation of propane to obtain a partial stream T (0), which contains at least propane, propene and hydrogen; (ii) separation of the partial stream T (0) to obtain at least one gaseous partial stream T (2) with a high hydrogen content and a partial stream T (1), which contains at least propene and propane; iii) hydrogen peroxide synthesis using the partial stream T (2), to produce a partial stream T (4) with a high hydrogen peroxide content and a gaseous partial stream T (6); (iv) separation of the partial stream T (1) to obtain at least one partial stream T (5) with a high propane content and at least one partial stream T (3) with a high propene content; (v) reaction of the partial stream(s) T (3) with partial stream T (4) to obtain propylene oxide.

8. 发明公开

EP1613574A1 VERFAHREN ZUR HERSTELLUNG VON WENIGSTENS EINEM PARTIELLEN OXIDATIONS- UND/ODER AMMOXIDATIONSPRODUKT EINES KOHLENWASSERSTOFFS 审中-公开
标题翻译：工艺用于生产至少一个部分氧化和/或氨氧化烃
公开(公告)号：EP1613574A1
公开(公告)日：2006-01-11
申请号：EP04725618.5
申请日：2004-04-03
申请人： BASF Aktiengesellschaft
发明人： SCHINDLER, Götz-Peter , MACHHAMMER, Otto , MÜLLER-ENGEL, Klaus, Joachim , HECHLER, Claus , PETZOLDT, Jochen , ADAMI, Christoph , HARTH, Klaus
IPC分类号： C07C5/327 , C07C45/35 , C07C51/25 , C07C253/26
CPC分类号： B01J23/63 , B01J23/626 , C07C45/33 , C07C45/34 , C07C45/35 , C07C51/252 , C07C253/26 , Y02P20/52 , C07C47/22 , C07C57/04 , C07C255/08
摘要： The invention relates to a method for the production of at least one partial oxidation and/or ammoxidation product of a hydrocarbon, wherein at least one saturated hydrocarbon (K) that is heterogeneously catalyzed is partially dehydrogenated and the resulting product gas mixture (A) containing the partially dehydrogenated hydrocarbon is used as such or in modified form for the heterogeneously catalyzed, partial oxidation and/or ammoxidation of the partially dehydrogenated hydrocarbon contained in the product gas mixture (A), wherein at least one mechanical separation operation is conducted between the product gas mixture (A) and the heterogeneously catalyzed, partial oxidation and/or ammoxidation.

9. 发明授权

EP1105365B1 VERFAHREN ZUR HERSTELLUNG VON ACROLEIN UND/ODER ACRYLSÄURE AUS PROPAN 有权
标题翻译：用于生产丙烯醛和/或丙烯酸丙烷
公开(公告)号：EP1105365B1
公开(公告)日：2002-06-19
申请号：EP99940184.7
申请日：1999-08-10
申请人： BASF AKTIENGESELLSCHAFT
发明人： MACHHAMMER, Otto , TENTEN, Andreas , JACHOW, Harald , HAUPT, Susanne , ARNOLD, Heiko , UNVERRICHT, Signe
IPC分类号： C07C45/33 , C07C45/35 , C07C47/22 , C07C51/215 , C07C51/25 , C07C57/04
CPC分类号： C07C51/215 , C07C45/33 , C07C45/35 , C07C51/252 , C07C47/22 , C07C57/04

10. 发明授权

EP1015410B1 VERFAHREN ZUR HERSTELLUNG VON ACRYLSÄURE UND METHACRYLSÄURE 有权
标题翻译：用于生产丙烯酸和甲基丙烯酸
公开(公告)号：EP1015410B1
公开(公告)日：2002-04-03
申请号：EP98948948.9
申请日：1998-09-09
申请人： BASF AKTIENGESELLSCHAFT
发明人： ECK, Bernd , MACHHAMMER, Otto , PROLL, Theo , SCHLIEPHAKE, Volker , THIEL, Joachim , BRÖLLOS, Klaus
IPC分类号： C07C51/43
CPC分类号： C07C51/43 , C07C57/04
摘要： The invention relates to a method for producing acrylic acid and methacrylic acid by producing a gaseous product mixture which essentially has the composition of a reaction mixture of the catalytic gas phase oxidation of C3-/C4- alkanes, -alkenes, -alkanols or -alkanals or precursors thereof to form acrylic acid or methacrylic acid. The product is separated from the gaseous product mixture according to a method comprising the following steps: a) condensing the gaseous product mixture; b) crystallising the acrylic acid or methacrylic acid from the solution obtained in (a); c) separating the resulting crystals from the mother liquor and d) returning at least a part of the mother liquor from stage (c) to stage (a).

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