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1. 发明公开

EP0964017A3 Process for separating from one another the non-functional, monofunctional and bifunctional species contained in perfluoropolyoxyalkylenes 失效
标题翻译： Verfahren zur Abtrennung der nicht-，mono und bifunktionellen Spezies in Perfluoropolyoxoidsenen
公开(公告)号：EP0964017A3
公开(公告)日：2001-06-13
申请号：EP99114057.5
申请日：1992-10-21
申请人： Ausimont S.p.A.
发明人： Tonelli, Claudio , Turri, Stefano , Levi, Marinella , Gianotti, Giuseppe
IPC分类号： C08G65/30 , B01D15/08
CPC分类号： C08G65/007 , B01D15/08 , B01D15/426 , C08G65/30
摘要： A process for separating, or enriching, in non-functional, monofunctional and bifunctional species the perfluoropolyoxyalkylenes of formula (I): Z-O-Rf-Y where Rf = a perfluoropolyoxyalkylene chain comprising one or more monomeric units of formula CFXO (X = F, CF 3 ), and optionally also units (-CF 2 CF 2 O-); Z, Y, like or different from each other, are non-functional groups or functional groups -OH, with at least Z or Y in part of such perfluoropolyoxyalkylenes being or containing an -OH group, which consists in subjecting said perfluoropolyoxyalkylenes to column chromatography using, as eluents, non-polar fluorinated solvents, either alone or in admixture with polar solvents.
摘要翻译：在非功能性单功能和双功能物质中分离或富集式（I）的全氟聚氧化烯的方法：ZO-Rf-Y其中Rf =包含一个或多个式CHEM> CHEM的单体单元的全氟聚氧化烯链， CFXO（X = F，CF 7）和任选地还有单元（-CF 6 C 6 O-）; Z，Y彼此相同或不同，是非官能团或官能团-OH，其中至少Z或Y部分为全氟聚氧化烯是或含有-OH基团，其组成在于使所述全氟聚氧化烯进行柱色谱法使用非极性氟化溶剂作为洗脱液，单独使用或与极性溶剂混合。

2. 发明公开

EP0587997A1 Fluorine-containing copolyacetals and their preparation 失效
标题翻译： Fluor enthaltende Copolyacetale und ihre Herstellung。
公开(公告)号：EP0587997A1
公开(公告)日：1994-03-23
申请号：EP93109104.5
申请日：1993-06-07
申请人： AUSIMONT S.p.A.
发明人： Danusso, Ferdinando , Strepparola, Ezio , Levi, Marinella , Tonelli, Claudio , Turri, Stefano
IPC分类号： C08G2/38 , C08G4/00
CPC分类号： C08G65/324 , C08G2/38 , C08G65/007 , C08G65/329 , C08G65/331
摘要： 1) New fluorine-containing compounds having polyacetalic structure, of general formula:

(I) [Rf-CH₂O(CH₂O) c -CH₂⁆ n

where:
Rf = a perfluorooxyalkylene chain having M ¯ n from 500 to 5,000;
c = 1 - 10;
n = 2 - 100.
2) A process for preparing them, which comprises carrying out the polycondensation of diols having formula:

(II) HOCH₂RfCH₂OH

with formaldehyde, in mass or in the presence of solvents, in an acid medium.

The compounds of formula (I) can be oligomeric compounds (polymerization degree x ¯ n from 2 to about 20) or polymeric compounds ( x ¯ n from about 20 to about 100). They exhibit a high stability to heat and to chemical agents, and Tg values slightly different from the ones of the diols utilized for preparing them.
摘要翻译： 1）具有以下通式的具有聚缩醛结构的新的含氟化合物：（I）[Rf-CH 2 O（CH 2 O）c -CH 2＆rsqbstr＆n其中：Rf = Mn为500-5,000的全氟氧化烯链; c = 1〜10; n = 2-100。2）一种制备它们的方法，其包括在酸性介质中以质量或在溶剂存在下，使式（II）HOCH 2 R f CH 2 OH与甲醛进行缩聚反应。式（I）化合物可以是低聚化合物（聚合度xn为2至约20）或聚合化合物（xn为约20至约100）。它们表现出对热和化学试剂的高稳定性，Tg值与用于制备它们的二醇的Tg值略有不同。

3. 发明授权

EP0538827B1 Process for the separation of the non, mono and bifunctional species in perfluoropolyoxyalkylenes 失效
标题翻译：用于分离全氟聚氧化烯中的非单体和双功能物质的方法
公开(公告)号：EP0538827B1
公开(公告)日：2000-03-08
申请号：EP92118008.9
申请日：1992-10-21
申请人： AUSIMONT S.p.A.
发明人： Tonelli, Claudio , Turri, Stefano , Gianotti, Giuseppe , Levi, Marinella
IPC分类号： C08G65/30 , B01D15/08
CPC分类号： B01D15/08 , C08G65/007 , C08G65/30

4. 发明授权

EP0822215B1 Perfluoropolyethers having polycarbonate structure 失效
标题翻译：具有聚碳酸酯结构的全氟聚醚
公开(公告)号：EP0822215B1
公开(公告)日：2000-03-01
申请号：EP97112701.4
申请日：1997-07-24
申请人： Ausimont S.p.A.
发明人： Turri, Stefano , Levi, Marinella , Tonelli, Claudio , Danusso, Ferdinando
IPC分类号： C08G64/02 , C08G64/30 , C08G64/18
CPC分类号： C08G64/0233 , C08G64/183

5. 发明公开

EP0538828A2 Process for the separation of the non, mono and bifunctional species in perfluoropolyoxyalkylenes 失效
标题翻译：用于分离全氟聚氧化烯中的非单体和双功能物质的方法
公开(公告)号：EP0538828A2
公开(公告)日：1993-04-28
申请号：EP92118009.7
申请日：1992-10-21
申请人： AUSIMONT S.p.A.
发明人： Tonelli, Claudio , Turri, Stefano , Levi, Marinella , Gianotti, Giuseppe
IPC分类号： C08G65/30 , B01D15/08
CPC分类号： C08G65/007 , B01D15/08 , B01D15/426 , C08G65/30
摘要： A process for separating, or enriching, in non-functional, monofunctional and bifunctional species the perfluoropolyoxyalkylenes of formula (I):

Z-O-Rf-Y
where Rf = a perfluoropolyoxyalkylene chain comprising one or more monomeric units of formula

CFXO (X = F, CF 3 ), and optionally also units (-CF 2 CF 2 0-);
Z, Y, like or different from each other, are non-functional groups or functional groups -OH, with at least Z or Y in part of such perfluoropolyoxyalkylenes being or containing an -OH group,
which consists in subjecting said perfluoropolyoxyalkylenes to column chromatography using, as eluents, non-polar fluorinated solvents, either alone or in admixture with polar solvents.
摘要翻译：一种用于在非官能单官能和双官能物质中分离或富集式（I）全氟聚氧化烯的方法：其中Rf =全氟聚氧化烯链，其包含一个或多个式CFXO单体单元（X = F， CF3），以及任选还有单元（-CF2CF2O-）; Z，Y彼此相同或不同，为非官能团或官能团-OH，其中至少部分该全氟聚氧化亚烷基中的Z或Y为或包含-OH基团，其包括将所述全氟聚氧化烯进行柱色谱使用单独或与极性溶剂混合的非极性氟化溶剂作为洗脱剂。

6. 发明公开

EP1059319A3 Fluorinated oligourethanes 审中-公开
标题翻译： Fluorierte低聚的氨基甲酸酯
公开(公告)号：EP1059319A3
公开(公告)日：2002-01-23
申请号：EP00112141.7
申请日：2000-06-06
申请人： Ausimont S.p.A.
发明人： Turri, Stefano , Levi, Marinella , Trombetta, Tania
IPC分类号： C08G18/38 , C08G18/50 , C08G18/28 , C08G18/08
CPC分类号： C08G18/792 , C08G18/0814 , C08G18/2885 , C08G18/5015 , C08G18/672 , C08G18/50
摘要： Fluorinated oligourethanes, having number average molecular weight lower than or equal to 9,000, having a branched structure, formed of the following monomers and macromers: a) aliphatic, cycloaliphatic or aromatic polyisocyanates, b) heterofunctional hydrogenated monomers having general formula:X0-(CR1AR2A)b-Y0 one or more of the following compounds: c) bifunctional hydroxyl (per)fluoropolyethers (PFPE diols) having number average molecular weight in the range 400-3,000, e) monofunctional hydroxyl (per)fluoropolyethers or monofunctional hydroxyl (per)fluoroalkanes (e'), having number average molecular weight in the range 300-1,000, and optionally the following compunds: d) heterofunctional monomers, dI) hydrogen-active compounds, capable to form bonds with the NCO functions stable at the hydrolysis but weak at heat.

7. 发明授权

EP0621296B1 Thermoplastic polyesters containing perfluoropolyoxyalkylene sequences 失效
标题翻译：含全氟聚氧化烯序列的热塑性聚酯
公开(公告)号：EP0621296B1
公开(公告)日：1998-12-16
申请号：EP94105854.7
申请日：1994-04-15
申请人： AUSIMONT S.p.A.
发明人： Turri, Stefano , Gianotti, Giuseppe , Levi, Marinella , Tonelli, Claudio
IPC分类号： C08G63/682 , C08G63/672
CPC分类号： C08G63/6826 , C08G63/672

8. 发明公开

EP0621296A2 Thermoplastic polyesters containing perfluoropolyoxyalkylene sequences 失效
标题翻译：热塑性聚酯薄膜全氟氧烷基烯烃。
公开(公告)号：EP0621296A2
公开(公告)日：1994-10-26
申请号：EP94105854.7
申请日：1994-04-15
申请人： AUSIMONT S.p.A.
发明人： Turri, Stefano , Gianotti, Giuseppe , Levi, Marinella , Tonelli, Claudio
IPC分类号： C08G63/682 , C08G63/672
CPC分类号： C08G63/6826 , C08G63/672
摘要： Fluorinated thermoplastic elastomers having a block structure:

-[-R f -H₁-H₂-H₁-]-

where -R f - is a perfluoropolyoxyalkylene sequence of formula:

-CF₂O-(CF₂CF₂O) m -(CF₂O) n -CF₂-

with m/n = 0.2 + 5, H₁ and H₂, equal or different from each other, are bivalent radicals having arylene, alkylarylene, alkylene or cycloalkylene structure, optionally containing fluorine and/or other heteroatoms selected among oxygen, sulphur, nitrogen.
Such products are obtainable by utilizing a perfluoropolyoxyalkylene diol having a functionality at least equal to 1.97, preferably at least equal to 1.99, and are characterized by a tensile strength at 23°C at least 50% higher than that of the corresponding polyesters obtained starting from perfluoropolyoxyalkylene diols having a functionality not higher than 1.96.
摘要翻译：具有嵌段结构的氟化热塑性弹性体：其中-Rf-是式-CF 2 O-（CF 2 CF 2 O）m - （CF 2 O）n -CF 2 - 的全氟聚氧亚烷基，m- n = 0.2 + 5，H1和H2彼此相同或不同，是具有亚芳基，烷基亚芳基，亚烷基或亚环烷基结构的二价基团，任选地含有选自氧，硫，氮中的氟和/或其它杂原子。这样的产物可通过使用具有至少等于1.97，优选至少等于1.99的官能度的全氟聚氧亚烷基二醇获得，其特征在于在23℃下的拉伸强度比从相应的聚酯开始获得的相应聚酯的拉伸强度高至少50％全氟聚氧亚烷基二醇的官能度不高于1.96。

9. 发明公开

EP0538827A3 Process for the separation of the non, mono and bifunctional species in perfluoropolyoxyalkylenes 失效
标题翻译：在全氟聚氧乙烯中分离非单，双功能物种的方法
公开(公告)号：EP0538827A3
公开(公告)日：1993-05-26
申请号：EP92118008.9
申请日：1992-10-21
申请人： AUSIMONT S.p.A.
发明人： Tonelli, Claudio , Turri, Stefano , Gianotti, Giuseppe , Levi, Marinella
IPC分类号： C08G65/30 , B01D15/08
CPC分类号： B01D15/08 , C08G65/007 , C08G65/30
摘要： A process for separating from one another the non-functional, monofunctional and bifunctional species in perfluoropolyoxyxalkylenes of gerneral formula
X-O-Rf-Y
where:
Rf = a perfluoropolyoxyalkylene chain comprising monomeric units of formulas
(CF₂O), (CF₂CF₂O), (CF₂CF₂CF₂O), X, Y, like or different from each other, are non-functional end groups containing functions OH and/or NH₂, with at least X and Y in parts of such perfluoropolyoxyalkylenes being or containing a group -OH, which consists in subjecting said perfluoropolyoxyalkylenes to column chromatography using, as eluents, non-polar fluorinated solvents, either alone or in admixture with polar solvents.

10. 发明公开

EP1059319A2 Fluorinated oligourethanes 审中-公开
标题翻译：氟代低聚氨酯
公开(公告)号：EP1059319A2
公开(公告)日：2000-12-13
申请号：EP00112141.7
申请日：2000-06-06
申请人： Ausimont S.p.A.
发明人： Turri, Stefano , Levi, Marinella , Trombetta, Tania
IPC分类号： C08G18/38 , C08G18/50
CPC分类号： C08G18/792 , C08G18/0814 , C08G18/2885 , C08G18/5015 , C08G18/672 , C08G18/50
摘要： Fluorinated oligourethanes, having number average molecular weight lower than or equal to 9,000, having a branched structure, formed of the following monomers and macromers:

a) aliphatic, cycloaliphatic or aromatic polyisocyanates,
b) heterofunctional hydrogenated monomers having general formula:

X 0 -(CR 1 A R 2 A ) b -Y 0 (Ib)

one or more of the following compounds:
c) bifunctional hydroxyl (per)fluoropolyethers (PFPE diols) having number average molecular weight in the range 400-3,000,
e) monofunctional hydroxyl (per)fluoropolyethers or monofunctional hydroxyl (per)fluoroalkanes (e'), having number average molecular weight in the range 300-1,000,
and optionally the following compunds:
d) heterofunctional monomers,
d I ) hydrogen-active compounds, capable to form bonds with the NCO functions stable at the hydrolysis but weak at heat.
摘要翻译：数均分子量低于或等于9,000的氟化低聚氨酯具有支链结构，由以下单体和大分子单体形成：a）脂族，脂环族或芳族多异氰酸酯，b）具有通式X 0-（CR 1）的异型氢化单体 b）一种或多种以下化合物：c）数均分子量在400-3,000范围内的双官能羟基（全）氟聚醚（PFPE二醇），e）单官能羟基（每）含氟聚醚或数均分子量在300-1,000范围内的单官能羟基（全）氟代烷（e'），以及任选的以下化合物：d）能形成键的异型官能单体d 1）氢活性化合物 NCO的功能在水解时稳定，但在加热下较弱。

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