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3. 发明公开

EP2332897A1 METHOD FOR PRODUCING ALKYLBENZENE AND A REACTOR FOR THE SULFURIC ACID ALKYLATION OF ISOBUTANE WITH OLEFINS 有权
标题翻译：用于生产烷基苯和电抗器与烯烃异丁烷硫酸烷基化
公开(公告)号：EP2332897A1
公开(公告)日：2011-06-15
申请号：EP08876798.3
申请日：2008-08-18
申请人： Gershuni, Semen Shikovich , Emelkina, Valentina Andreevna , Zhikharev, Roman Vladimirovich
发明人： Gershuni, Semen Shikovich , Emelkina, Valentina Andreevna , Zhikharev, Roman Vladimirovich
IPC分类号： C07C2/62 , C07C9/14 , C10L1/06 , B01J8/00
CPC分类号： B01J4/002 , B01J19/2415 , B01J19/242 , B01J2219/0004 , C07C2/62 , C10G29/205 , C10G2300/1081 , C10G2300/1088 , C10G2300/4006 , C10G2400/30 , C07C9/16
摘要： The invention relates to a method (two variants) for producing alkylbenzene by alkylating isobutene with olefins and to a reactor (two variants) for carrying out said method. In the first variant, the reactor comprises a reaction chamber consisting of a vertical cylindrical housing and coaxial return pipe, units for the inlet of sulfuric acid and of circulating reaction products, wherein the sulfuric acid inlet unit is in the form of a chamber with an inlet connection that is situated below the return pipe at a distance from the end thereof and is separated therefrom by a transverse partition in which nozzles for introducing sulfuric acid into the circulating acid are secured, said nozzles being oriented upwards and being arranged in a circle, the diameter of which is less than the inside diameter of the return pipe. The unit for the inlet of circulating reaction products mixed with an olefin-containing raw material is in the form of an annular chamber with an inlet connection, which chamber is situated above the return pipe and is provided with nozzles that are oriented downwards and are arranged in a circle, the diameter of which is greater than the outside diameter of the return pipe, and with a reaction mixture removal conduit situated inside the annular chamber. In the second variant, the reactor is in the form of two coaxial reaction chambers, arranged one above the other, which are similar to the above-mentioned reaction chambers, wherein a connection for removing a portion of the reaction mixture from the upper chamber is situated in the housing of said chamber above the level of a transverse partition in which nozzles for the flow of emulsion from the lower chamber to the upper chamber are secured. The use of the method (variants) and the reactor (variants) makes it possible to produce better quality alkylbenzene and to provide high operational reliability.
摘要翻译：本发明涉及用于通过与烯烃和一种用于实施所述方法的反应器（两个变体）的烷基化生产异丁烯烷基苯的方法（两种变体）。在第一变型中，反应器包括反应室由垂直圆柱形外壳和同轴返回管的，单位为硫酸的入口和循环的反应产物，worin硫酸入口部的与在腔室的形式入口连接确实在从其端部的距离位于回流管的下方，通过在其中喷嘴用于将硫酸到循环酸被固定的横向分隔从那里分离，所述被向上定向的喷嘴和被布置成圆形，所有其直径小于所述返回管的内径。在含烯烃的原料循环反应产物与混合的入口处的单元是在入口连接，所述腔室位于所述回流管上方，并设置有喷嘴的环形设计腔室与的形式没有被向下定向并且被布置转了一圈，所有这一切的直径比回油管的外径大，并且与反应混合物中去除管道里面位于所述环形设计香槟。在第二变型中，反应器是在两个同轴的反应室的形式，布置成一个在另一个之上，其类似于上述的反应室，worin用于从所述上部腔室中除去反应混合物中的一部分的连接是位于所述室中，其中喷嘴乳液的从下室到上腔室中的流动的横向隔板的水平上方的壳体被固定。使用该方法（变体）和反应器（变体）的，能够产生更好的质量和烷基苯以提供高的操作可靠性。

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