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    • 78. 发明公开
    • Method for thermal treatment of a refractory dielectric body, such as glass, using plasma
    • 一种用于耐火介电体的热处理过程中,例如由玻璃制成的,通过等离子体的手段
    • EP0905098A1
    • 1999-03-31
    • EP98307668.8
    • 1998-09-22
    • LUCENT TECHNOLOGIES INC.
    • Fleming, James William, Jr.Pafchek, Robert M.
    • C03B37/012C03B29/02C03B32/00C03C23/00C04B41/00
    • C03C25/6293C03B29/02C03B37/01237C03B37/0148C03B37/01493C03B2201/03C03B2201/04C03C23/006
    • A refractory dielectric body, such as glass, is heated with a plasma fireball at conditions which do not result in substantial removal of a surface portion of the body (i.e. ≤0.1mm from the surface of the body), yet which are sufficient to reduce both surface and bulk impurities. Typically such conditions entail ensuring that the plasma heats the body to a surface temperature in the range of 1800 to 2300°C. Typically, the body is treated with the plasma in the absence of simultaneous deposition of material onto the body. The body may be solid or hollow, such as a rod or a tube, and the surface heated by the plasma may be the inside surface or the outer surface of the body. Advantageously, an isothermal, oxygen or oxygen-containing plasma is utilized. The invention is useful for reducing chlorine impurities by at least about 30% to a depth of at least about 10µm, with accompanying reduction of hydroxyl impurities. The invention thus provides a useful method for reducing the concentration of impurities that contribute to imperfections during the process of drawing fiber from an optical fiber preform, without requiring substantial removal of the surface of the preform.
    • 的耐火介电体,颜色:例如玻璃,用等离子体火球在不导致在基本上除去体的(从主体的表面即≤0.1mm)的表面部分的条件下被加热,但这些都足以减少 两个表面和体杂质。 典型地搜索条件要求保证确实的等离子体加热体在1800范围内的表面温度至2300℃。通常,身体治疗与在不存在材料的同时沉积的到主体等离子体。 所述主体可以是实心或空心,:诸如杆或管,以及由等离子体加热可以是内表面或所述主体的所述外表面的表面。 有利的是,在等温,氧或含氧的等离子体被利用。 本发明是用于通过在至少约30%减少氯杂质的至少约10微米的深度处,伴随减少羟基杂质有用的。 因此,本发明提供了用于减少杂质的浓度从在光纤预制件拉制光纤的过程中,也有助于缺陷,而不需要大量的去除预成型体的表面的一种有用的方法。