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41. 发明公开

EP3305749A1 METHOD FOR PRODUCING FLUORINE-CONTAINING OLEFIN 审中-实审转让
标题翻译：生产含氟烯烃的方法
公开(公告)号：EP3305749A1
公开(公告)日：2018-04-11
申请号：EP16803051.8
申请日：2016-05-18
申请人： Daikin Industries, Ltd.
发明人： CHAKI, Takehiro , OHKUBO, Shun , KARUBE, Daisuke
IPC分类号： C07C17/25 , B01J23/26 , C07C21/18 , C07B61/00
CPC分类号： C07C17/25 , B01D3/14 , B01D3/40 , B01J23/26 , C07B61/00 , C07C21/18 , C08F14/18
摘要： The present invention provides a method for producing a target fluorine-containing olefin with high conversion and selectivity using a process comprising a dehydrofluorination reaction of a hydrofluorocarbon. The method comprises a first reaction step comprising subjecting a hydrofluorocarbon to dehydrofluorination in the presence of a catalyst. The hydrofluorocarbon is a compound represented by Formula (1): R f CFYCHZ 2 , wherein R f represents a straight or branched C 1-3 perfluoroalkyl group, and Y and Z each independently represent H or F wherein when all Zs are H, Y represents F. The catalyst comprises chromium oxide represented by the chemical formula: CrO m (1.5
摘要翻译：本发明提供一种使用包含氢氟烃的脱氟化氢反应的方法以高转化率和选择性制造目标含氟烯烃的方法。该方法包括第一反应步骤，其包括使氢氟烃在催化剂存在下进行脱氟化氢。氢氟烃是由式（1）表示的化合物：RfCFYCHZ2，其中Rf表示直链或支链的C1-3全氟烷基，并且Y和Z各自独立地表示H或F，其中当所有Z为H时，Y表示F.催化剂包含由化学式：CrOm（1.5

42. 发明公开

EP3283606A1 IMPROVED METHOD AND APPARATUS FOR EXTRACTING BOTANICAL OILS 有权转让
标题翻译：改进的提取植物油的方法和设备
公开(公告)号：EP3283606A1
公开(公告)日：2018-02-21
申请号：EP16774400.2
申请日：2016-04-04
申请人： Natural Extraction Services, LLC
发明人： THOMAS, C., Russell
IPC分类号： C11B1/10 , A61K8/97 , B01D1/14 , B01D3/40 , B01D11/00 , B01D11/02
CPC分类号： B01D11/0242 , B01D1/14 , B01D1/16 , B01D3/40 , B01D11/028 , B01D11/0296 , B01D53/1418 , B01D53/1493 , B01D53/18 , B01D2011/007 , C11B1/10
摘要： A system for extracting oil from plant material includes a gas moving device propelling a gas stream, the gas stream being a stream of air or gas with or without entrained vapor, solids or droplets of liquid therein. The gas stream is directed through an extraction chamber, which is operable to volatize at least a portion of an oil from a plant material such that the volatilized oil is disposed in the gas stream as an extracted oil. A collection chamber is in communication with the extraction chamber such that the gas stream flows through the collection chamber. The collection chamber has collection solvent operable to collect at least a portion of the extracted oil from the gas stream. A liquid collector is in fluid communication with the collection chamber for collecting at least a portion of the collection solvent and extracted oil.

43. 发明授权

EP2269728B1 Verwendung von geordneten Packungen, die eine oder mehrere Anstaulagen, sowie ein oder mehrere Abscheidelagen aufweisen 有权
标题翻译：使用有一个或多个停滞层的有序包装，以及一个或多个镀层
公开(公告)号：EP2269728B1
公开(公告)日：2018-01-31
申请号：EP10164635.4
申请日：2010-06-01
申请人： BASF SE
发明人： Kaibel, Gerd , Heida, Bernd , Hugo, Randolf
IPC分类号： B01J19/32 , B01D3/40
CPC分类号： B01J19/32 , B01D3/40 , B01D3/42 , B01J2219/3221 , B01J2219/32213 , B01J2219/32227 , B01J2219/32258

44. 发明授权

EP2718274B1 METHODS FOR ALKYLENE OXIDE SEPARATION USING EXTRACTIVE DESTILLATION COLUMNS 有权
标题翻译：用萃取蒸馏塔分离氧化烯的方法
公开(公告)号：EP2718274B1
公开(公告)日：2018-01-24
申请号：EP12728898.3
申请日：2012-06-07
申请人： Lyondell Chemical Technology L.P.
发明人： LI, Xiangmin , LEYSHON, David, W. , CHANG, Te
IPC分类号： B01D3/40 , C07D301/19 , C07D301/32 , C07D303/04
CPC分类号： C07D303/04 , B01D3/40 , C07D301/19 , C07D301/32
摘要： The disclosure relates to a process for separating propylene oxide for a crude propylene oxide stream, for example an intermediate stream from a PO/TBA process. The crude propylene oxide stream can be passed through an extractive distillation column. The distillation column is operated at a pressure in a range of greater than 25 up to 50 psig, and/or at a temperature in a range of from 70 to 150 degrees Celsius using C8-C20 paraffin as extractive solvent with an overhead distillate water wash drum. The crude propylene oxide stream include from 0.001 to 0.1 wt % methanol, based on the total composition of the crude propylene oxide stream. The systems, methods, and apparatuses can produce a propylene oxide stream having less formaldehyde and acetaldehyde than the prior art.

45. 发明公开

EP3230244A1 PROCESS FOR THE SEPARATION OF GLYCOLS 有权转让
标题翻译：分离甘醇的方法
公开(公告)号：EP3230244A1
公开(公告)日：2017-10-18
申请号：EP15805464.3
申请日：2015-12-04
申请人： Shell Internationale Research Maatschappij B.V.
发明人： HUIZENGA, Pieter , FISCHER, Kai Jürgen
IPC分类号： C07C29/80 , C07C31/20
CPC分类号： C07C29/84 , B01D3/40 , B01D3/4294 , C07C29/80 , C07C31/202 , C07C31/207
摘要： The invention provides a process for the separation of MEG and 1,2-BDO from a first mixture comprising MEG and 1,2-BDO, said process comprising the steps of: (i) providing said first mixture comprising MEG and 1,2-BDO as a feed to a distillation column; (ii) providing a feed comprising glycerol to the distillation column above the first mixture; (iii) operating the distillation column at a temperature in the range of from 50 to 250° C. and a pressure in the range of from 0.1 to 400 kPa; (iv) removing a stream comprising MEG and glycerol as a bottoms stream from the distillation column; and (v) (v) removing a stream comprising 1,2-BDO above the point at which the feed comprising glycerol is provided to the distillation column.
摘要翻译：本发明提供了从包含MEG和1,2-BDO的第一混合物中分离MEG和1,2-BDO的方法，所述方法包括以下步骤：（i）提供包含MEG和1,2- BDO作为蒸馏塔的进料; （ii）将包含甘油的进料提供至第一混合物上方的蒸馏塔; （iii）在50-250℃的温度范围和0.1-400kPa的压力下操作蒸馏塔; （iv）从蒸馏塔中除去包含MEG和甘油的作为底部料流的料流; 和（v）（v）在提供包含甘油的进料到蒸馏塔的点之上去除包含1,2-BDO的物流。

46. 发明公开

EP3222607A1 METHOD FOR ISOLATING HFC-245cb AND (E)-HFO-1234ze FROM COMPOSITION CONTAINING BOTH COMPOUNDS 有权
标题翻译：从含有两种化合物的组合物中分离HFC-245cb和（E）-HFO-1234ze的方法
公开(公告)号：EP3222607A1
公开(公告)日：2017-09-27
申请号：EP15862093.0
申请日：2015-11-12
申请人： Daikin Industries, Ltd.
发明人： SHIMOKAWA, Mana , TAKAKUWA, Tatsuya , TAKAHASHI, Kazuhiro
IPC分类号： C07C17/386 , C07C19/08 , C07C21/18
CPC分类号： C07C17/386 , B01D3/40 , C07C19/08 , C07C21/18
摘要： The present invention provides a method for separating HFC-245cb and (E)-HFO-1234ze having close boiling points, i.e., boiling points with only 1°C difference, by extractive distillation from a composition containing the HFC-245cb and the (E)-HFO-1234ze.
More specifically, the present invention is a method for separating HFC-245cb and (E)-HFO-1234ze from a composition containing the HFC-245cb and the (E)-HFO-1234ze, the method comprising subjecting the composition to extractive distillation using at least one extractant selected from the group consisting of halogenated hydrocarbons, halogenated unsaturated hydrocarbons, nitriles, ketones, carbonates, alcohols, hydrocarbons, esters and ethers.
摘要翻译：本发明提供一种通过从含有HFC-245cb和（E）的组合物中提取蒸馏来分离具有接近沸点（即沸点仅为1℃差异）的HFC-245cb和（E）-HFO- ）-HfO式-1234ze。更具体地说，本发明是从含有HFC-245cb和（E）-HFO-1234ze的组合物中分离HFC-245cb和（E）-HFO-1234ze的方法，所述方法包括使用组合物进行萃取蒸馏至少一种选自卤代烃，卤代不饱和烃，腈，酮，碳酸酯，醇，烃，酯和醚的萃取剂。

47. 发明公开

EP2575992A4 SYSTEM AND METHOD FOR REDUCTION OF WATER CONSUMPTION IN PURIFIED TEREPHTHALIC ACID PRODUCTION 审中-公开
标题翻译： SYSTEM UND VERFAHREN ZUR REDUZIERUNG DES WASSERVERBRAUCHS贝德尔斯通公司VER GEREINIGTERTEREPHTHALSÄURE
公开(公告)号：EP2575992A4
公开(公告)日：2017-07-26
申请号：EP11803211
申请日：2011-05-16
申请人： AMT INT INC
发明人： JANG JI-YOUNG , WU KUANG-YEU , YANG MING-MOU
IPC分类号： B01D3/36 , B01D3/14 , B01D3/40
CPC分类号： B01D3/36 , B01D3/143 , B01D3/40
摘要： The invention disclosed is an apparatus and method for the recovery of acetic acid, azeotropic agent, extraction agent, re-usable water and other reaction products such as p-toluic acid, from an aqueous stream generated during a terephthalic acid production process, having superior energy efficiency and reduced water consumption. The apparatus of the invention includes: an azeotropic distillation column to remove water from acetic acid, a pair of mother liquor extraction columns sequentially connected in series for primary recovery of extraction solvent and other organics, an azeotropic agent stripper for recovery of azeotropic agent and a post-separation solvent stripper distillation column for further separation of the aqueous bottoms stream from said extraction columns into a volatiles stream comprising mainly organics with a very low amount of water and a liquid stream comprising water containing very low amounts of organics, each stream being sufficiently pure that it can be recycled for reuse in the purification of crude terephthalic acid.
摘要翻译：所公开的发明是从对苯二甲酸生产过程中产生的含水物流中回收乙酸，共沸剂，萃取剂，可再用水和其它反应产物如对甲苯甲酸的装置和方法，能源效率和减少用水量。本发明的装置包括：从乙酸中除去水的共沸蒸馏塔，串联连接的一对母液萃取塔，用于萃取溶剂和其它有机物的一次回收，用于回收共沸剂的共沸剂汽提塔和后分离溶剂汽提塔蒸馏塔，用于将来自所述萃取塔的含水底部物流进一步分离成主要包含具有非常少量水的有机物的挥发性物流和包含含有非常少量有机物的水的液体物流，每个物流足够纯净的是它可以被回收再利用来纯化粗制对苯二甲酸。

48. 发明授权

EP2788457B1 VERFAHREN ZUR DURCHFÜHRUNG EINER EXTRAKTIVDESTILLATION MIT EINEM SELEKTIVEN LÖSUNGSMITTEL, MIT EINEM GEREINIGTEN DAMPFFÖRMIGEN ROH-C4-SCHNITT ALS EINSATZSTROM 有权
标题翻译：一种使用选择性溶剂具体的萃取蒸馏，与蒸汽CLEANED SHAPED ROH-C4馏分作为用电
公开(公告)号：EP2788457B1
公开(公告)日：2017-02-22
申请号：EP12794723.2
申请日：2012-12-04
申请人： BASF SE
发明人： HEIDA, Bernd , HUGO, Randolf
IPC分类号： C10G21/28 , C10G21/14 , C10L3/12 , B01D3/14
CPC分类号： C10L3/12 , B01D3/40 , C10G21/14 , C10G21/28

49. 发明授权

EP2930178B1 DESTILLATION VON SILANGEMISCHEN IN ANWESENHEIT EINES NITRILS ODER AMINS 有权
标题翻译：西班牙语西班牙语西班牙语西班牙语西班牙语
公开(公告)号：EP2930178B1
公开(公告)日：2017-02-01
申请号：EP15162057.2
申请日：2015-03-31
申请人： Wacker Chemie AG
发明人： Mohsseni, Javad , Mautner, Konrad , Nürnberg, Peter , Kaltenmarkner, Christian , Kaeppler, Klaus , Bockholt, Andreas
IPC分类号： C07F7/12 , C07F7/20
CPC分类号： B01D3/40 , C07F7/121 , C07F7/20

50. 发明公开

EP2937329A4 METHOD FOR PRODUCING ACETIC ACID 有权转让
公开(公告)号：EP2937329A4
公开(公告)日：2016-08-17
申请号：EP13864464
申请日：2013-12-02
申请人： DAICEL CORP
发明人： SHIMIZU MASAHIKO , SAITO RYUJI , MIURA HIROYUKI
IPC分类号： C07C51/12 , C07C51/44 , C07C53/08
CPC分类号： C07C51/12 , B01D3/40 , B01J31/16 , C07C51/44 , C07C53/08
摘要： A process for removing acetaldehyde efficiently and producing high-purity acetic acid stably is provided. Methanol is allowed to continuously react with carbon monoxide in a carbonylation reactor 1 in the presence of a catalyst system; the reaction mixture is continuously fed to a flasher 2 to form a volatile phase (2A) containing acetic acid and methyl iodide; the volatile phase (2A) is continuously fed to a splitter column 3 to form an overhead (3A) containing methyl iodide and acetaldehyde and a stream (3B) containing acetic acid; the volatile phase (2A) and/or the overhead (3A) is cooled by a first condenser C1, C3 at a predetermined cooling temperature; and the noncondensed gaseous component is further cooled by a second condenser C2, C4 to form a concentrate having a lower temperature and a higher acetaldehyde concentration. Acetaldehyde is efficiently removed by distilling the concentrate having a high acetaldehyde concentration.

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