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21. 发明公开

EP2415740A1 METHOD FOR PRODUCING HIGH-PURITY TERMINAL OLEFIN COMPOUND 有权
标题翻译： VERFAHREN ZUR HERSTELLUNG EINERENDSTÄNDIGENOLEFINVERBINDUNG VON HOHER REINHEIT
公开(公告)号：EP2415740A1
公开(公告)日：2012-02-08
申请号：EP10758309.8
申请日：2010-01-08
申请人： Kuraray Co., Ltd.
发明人： MIYOSHI, Kei , ASANUMA, Goro
IPC分类号： C07C7/04 , C07C7/148 , C07C11/12 , C07C45/82 , C07C45/85 , C07C47/21 , C07C67/54 , C07C67/60 , C07C69/533 , C07C253/34 , C07C255/07
CPC分类号： C07C45/85 , C07C7/005 , C07C7/04 , C07C45/82 , C07C67/60 , C07C253/34 , C07C11/02 , C07C47/21 , C07C69/533 , C07C255/07
摘要： PROBLEM
There is provided an industrially advantageous means to obtain a high purity terminal olefin compound (for example, 7-octenal).
SOLUTION
The method for producing a high purity terminal olefin compound of the present invention comprises a step where a mixture containing a terminal olefin compound represented by the following chemical formula 1:

and a corresponding internal olefin compound as an impurity is brought into contact with a brominating agent in the presence of water or an alcohol, to convert the aforementioned internal olefin compound to a compound having a higher boiling point; and a step where the aforementioned terminal olefin compound is purified by distillation from the mixture obtained in the aforementioned step.
摘要翻译：问题提供了获得高纯度末端烯烃化合物（例如，7-辛烯醛）的工业上有利的手段。解决方案本发明的高纯度末端烯烃化合物的制造方法包括将含有由下列化学式1表示的末端烯烃化合物和相应的内部烯烃化合物作为杂质的混合物与溴化物接触的步骤在水或醇的存在下，将上述内部烯烃化合物转化成沸点较高的化合物; 和上述末端烯烃化合物通过蒸馏从上述步骤获得的混合物中纯化的步骤。

22. 发明授权

EP1752439B1 Method of producing high-purity hydroxypivalaldehyde and/or dimer thereof 有权
标题翻译：用于生产高纯度的羟基新戊醛和/或其二聚物的方法
公开(公告)号：EP1752439B1
公开(公告)日：2012-02-01
申请号：EP06118168.1
申请日：2006-07-31
申请人： MITSUBISHI GAS CHEMICAL COMPANY, INC.
发明人： Amemiya, Junichi , Watanabe, Masafumi , Kuzuhara, Ikutaro
IPC分类号： C07C47/19 , C07C45/75 , C07C45/80 , C07C45/81 , C07C45/82 , C07D319/06
CPC分类号： C07C45/75 , C07C45/80 , C07C45/81 , C07C45/82 , C07D319/06 , C07C47/19

23. 发明公开

EP2318349A1 VERFAHREN ZUR GEWINNUNG VON ALIPHATISCHEN C3- BIS C-10-ALDEHYDEN AUS HOCHSIEDENDEN STOFFEN MITELS THERMISCHER VERFAHREN 有权转让
标题翻译：一种从高沸点物质敏迪热工过程OBTAINING脂肪族C3- TO C-10醛
公开(公告)号：EP2318349A1
公开(公告)日：2011-05-11
申请号：EP09777498.8
申请日：2009-07-29
申请人： OXEA GmbH
发明人： BERGHAHN, Barbara , GREB, Wolfgang , SCHÖPPER, Norbert , ZGORZELSKI, Wolfgang
IPC分类号： C07C45/50 , C07C47/02 , C07C45/82
CPC分类号： C07C45/50 , C07C45/82 , C07C47/02
摘要： The invention relates to a method for obtaining aliphatic C
3 - to C
10 -aldehydes from high-boiling substances accumulating in the hydroformylation of the corresponding C
2 - to C
9 -olefins in a heterogenic reaction system using an aqueous solution comprising transition metal complex compounds of Group VIII of the periodic system of the elements as a catalyst, wherein the organic phase that accumulates is subjected to separate distillation steps after separating out volatile components and after separating out the aqueous catalyst phase, and wherein the high-boiling substances are split at a high temperature in the last distillation step into a mixture of n- and iso-aldehyde that is drawn off as the top product.

24. 发明公开

EP2234952A1 CYCLOHEXANONE PRODUCTION PROCESS WITH MODIFIED POST-DISTILLATION 审中-公开
标题翻译： Herstellungsverfahren von Cyclohexanon mit modifizierter Post-Destillation
公开(公告)号：EP2234952A1
公开(公告)日：2010-10-06
申请号：EP08864701.1
申请日：2008-12-16
申请人： DSM IP Assets B.V.
发明人： HORSELS, Marleen , PARTON, Rudy Francois Maria Jozef , TINGE, Johan Thomas
IPC分类号： C07C45/82 , C07C49/403 , B01J10/00 , C07C29/48 , C07C45/00 , C07C45/29 , C07C51/00 , C07C55/14 , C07C35/08 , C08F232/00
CPC分类号： C07C29/50 , C07C45/006 , C07C45/82 , C07C51/00 , C07C2601/14 , C07C49/403 , C07C55/14 , C07C35/08
摘要： The present invention relates to a method for continuously preparing cyclohexanone from phenol making use of a catalyst comprising at least one catalytically active metal selected from platinum and palladium comprising a) hydrogenating phenol to form a product stream comprising cyclohexanone and unreacted phenol; b) separating at least part of the product stream, or at least part of the product stream from which one or more components having a lower boiling point than cyclohexanone have been removed, into a first fraction comprising cyclohexanone and a second fraction comprising phenol and cyclohexanol, using distillation; c) separating the second fraction into a third fraction, rich in cyclohexanol, and a fourth fraction, rich in phenol and, using distillation; d) subjecting at least part of the fourth fraction to a further distillation step, thereby forming a fifth fraction and a sixth fraction, wherein the fifth fraction is enriched in phenol compared to the sixth fraction, and wherein the sixth fraction comprises side-products having a higher boiling point than phenol, and phenol, wherein step d) is carried out in a vacuum distillation column equipped with trays in the lower part of the column, and wherein in the upper part of the column, i.e. in the part above the feed inlet, packing material is present instead of trays in at least part of said upper part, which packing material has a comparable or improved separating efficiency, and provides a reduction of the pressure drop by at least 30%, preferably more than 50%, as compared to the case with trays in the upper part, under otherwise similar distillation conditions.
摘要翻译：从苯酚连续制备环己酮的方法使用具有至少一种选自铂和钯的催化活性金属的催化剂。该方法包括与后续馏分相比富集蒸馏馏分中的苯酚，其中后续馏分包括苯酚和沸点高于苯酚的副产物。蒸馏在塔底部装有塔板的真空蒸馏塔中进行。在塔的上部，即在进料入口上方的部分，在其至少一部分中存在填料材料代替塔盘。包装材料具有相当或改进的分离效率，并且与其他类似的蒸馏条件下的上部塔板的情况相比，压降降低至少30％，优选大于50％。

25. 发明公开

EP2231577A1 CYCLOHEXANONE PRODUCTION PROCESS WITH MULTIPLE POST-DISTILLATION 有权
标题翻译： VERFAHREN ZUR HERSTELLUNG VON CYCLOHEXANON麻省理工学院
公开(公告)号：EP2231577A1
公开(公告)日：2010-09-29
申请号：EP08863517.2
申请日：2008-12-16
申请人： DSM IP Assets B.V.
发明人： DORTMONT, VAN, Godefridus Maria , HORSELS, Marleen , PARTON, Rudy Francois Maria Jozef , TINGE, Johan Thomas
IPC分类号： C07C45/82 , C07C29/48 , C07C45/00 , C07C45/29 , C07C51/00 , B01J10/00 , C08F232/00 , C07C49/403 , C07C55/14 , C07C35/08
CPC分类号： C07C29/50 , C07C45/006 , C07C45/82 , C07C51/00 , C07C2601/14 , C07C49/403 , C07C55/14 , C07C35/08
摘要： The present invention relates to a method for continuously preparing cyclohexanone from phenol making use of a catalyst comprising at least one catalytically active metal selected from platinum and palladium comprising hydrogenating phenol to form a product stream comprising cyclohexanone and unreacted phenol; separating at least part of the product stream, or at least part of the product stream from which one or more components having a lower boiling point than cyclohexanone have been removed, into a first fraction comprising cyclohexanone and a second fraction comprising phenol and cyclohexanol, using distillation; separating the second fraction into a third fraction, rich in cyclohexanol, and a fourth fraction, rich in phenol, using distillation; - subjecting at least part of the fourth fraction to a further distillation step, thereby forming a fifth fraction and a sixth fraction, wherein the fifth fraction is enriched in phenol compared to the sixth fraction, and wherein the sixth fraction comprises side-products having a higher boiling point than phenol, and phenol; and which method is characterized in the additional step of continuously or intermittently separating at least part of the sixth fraction to yet a further distillation step, thereby forming a seventh fraction and an eight fraction, wherein the seventh fraction is enriched in phenol compared to the eight fraction, and wherein the eight fraction comprises side-products having a higher boiling point than phenol.
摘要翻译：本发明涉及一种使用包含至少一种选自铂和钯的催化活性金属的催化剂从苯酚连续制备环己酮的方法，其包括氢化苯酚以形成包含环己酮和未反应苯酚的产物流; 将至少部分产物流或至少部分产物流从其中除去一个或多个沸点低于环己酮的组分的产物流转化成包含环己酮的第一馏分和包含苯酚和环己醇的第二馏分，使用蒸馏; 将第二级分分离成富含环己醇的第三级分，和使用蒸馏富含苯酚的第四级分; - 将第四部分的至少一部分喷射至另一蒸馏步骤，从而形成第五馏分和第六馏分，其中与第六馏分相比，第五馏分富含苯酚，其中第六馏分包含具有沸点高于苯酚，苯酚; 并且该方法的特征在于将第六馏分的至少一部分连续或间歇地分离成另外的蒸馏步骤的另外步骤，从而形成第七馏分和八馏分，其中第七馏分富含苯酚，与八馏分，其中八馏分包含沸点高于苯酚的副产物。

26. 发明公开

EP2134669A1 VERFAHREN ZUR HERSTELLUNG VON HYDROXYPIVALINALDEHYD UND NEOPENTYLGLYKOL 有权
标题翻译：用于生产羟基新和新戊二醇
公开(公告)号：EP2134669A1
公开(公告)日：2009-12-23
申请号：EP08709204.5
申请日：2008-02-25
申请人： BASF SE
发明人： SIRCH, Tilman , STEININGER, Michael , MAAS, Steffen , RITTINGER, Stefan , SCHLITTER, Stephan
IPC分类号： C07C29/141 , C07C45/75 , C07C45/82 , C07C47/19
CPC分类号： C07C45/75 , C07C29/141 , C07C45/82 , C07C47/19 , C07C31/20
摘要： The invention relates to hydroxy pivalin aldehyde, which is produced by the aldolization of isobutyraldehyde with formaldehyde and subsequent processing of the reaction product by distillation, wherein the reaction product is fed to a distillation column, which is operated at a top pressure ranging between 0.5 and 1.5 bar and in which a two-stage condensation process is provided in the top region. In this process, the vapors are first fed to a partial condenser operated at a temperature ranging between 50 and 80ºC, the condensate of which is returned at least partially to the distillation column, and the vapors that are not condensed in the partial condenser are fed to a downstream condenser operated at a temperature ranging between -40º and +30ºC, the condensate of which is discharged at least partially.

27. 发明授权

EP1300384B1 Process for recovering acrolein or propionaldehyde from dilute aqueous streams 有权
标题翻译：一种回收的丙烯醛或丙醛的方法，从稀的水性流
公开(公告)号：EP1300384B1
公开(公告)日：2006-12-13
申请号：EP02292393.2
申请日：2002-09-27
申请人： Arkema Inc.
发明人： Schon, Steven G. , Daniel, Samuel M. , Sander, Richard A.
IPC分类号： C07C45/82 , C07C47/22 , C07C47/02
CPC分类号： C07C45/82 , C07C47/02 , C07C47/22

28. 发明授权

EP1226102B1 METHOD FOR PURIFYING ACETONE 有权
标题翻译：清理方法丙酮
公开(公告)号：EP1226102B1
公开(公告)日：2006-10-25
申请号：EP00968915.9
申请日：2000-10-10
申请人： GENERAL ELECTRIC COMPANY
发明人： FULMER, John, William , ARISTOVICH, Valery Jurievich , ARISTOVICH, Yury Valerievich , SOKOLOV, Andrey Jurievich
IPC分类号： C07C45/82 , C07C45/85 , C07C49/08
CPC分类号： C07C45/82 , C07C45/85 , C07C49/08
摘要： A process is described for purifying acetone from a crude acetone-phenol mixture produced upon oxidizing cumene. In the process, an alkaline agent and an oxidizing agent are both added to the mixture to help remove aldehyde contaminants upon purification.

29. 发明公开

EP1620383A1 AUSGANGSVERBINDUNGEN FÜR DIE HERSTELLUNG VON POLYURETHANEN 审中-公开
标题翻译：原料化合物聚氨酯的生产
公开(公告)号：EP1620383A1
公开(公告)日：2006-02-01
申请号：EP04727865.0
申请日：2004-04-16
申请人： BASF Aktiengesellschaft
发明人： GROER, Peter , HENDREICH, Regina , KIERKUS, Paul, Ch. , OSTROWSKI, Thomas , STROEFER, Eckhard , THIELE, Kai , SCHNORPFEIL, Christoph , DEXHEIMER, Edward, Michael
IPC分类号： C07C45/82 , C08G2/34 , C08G18/54 , C08G65/26
CPC分类号： C08G65/2609 , C07C43/315 , C08G2/34 , C08G18/546 , C08G2650/34
摘要： The invention relates to initial compounds for producing polyurethanes and is characterised in that said polyurethanes can be produced by reaction of hydroxyl group containing formaldehyde oligomers.

30. 发明公开

EP1567514A1 VERFAHREN ZUR GEWINNUNG EINES ALIPHATISCHEN DIALDEHYD-MONOACETALS 有权
标题翻译：程序为获得脂肪二醛单缩醛
公开(公告)号：EP1567514A1
公开(公告)日：2005-08-31
申请号：EP03811775.0
申请日：2003-11-27
申请人： BASF Aktiengesellschaft
发明人： HADERLEIN, Gerd , GÖBBEL, Hans-Georg , SIEGEL, Wolfgang
IPC分类号： C07D317/26 , C07C45/82 , C07C47/198
CPC分类号： C07D317/26 , B01D1/22 , B01D3/141 , B01D3/148 , B01D3/322 , C07C45/60 , C07C45/71 , C07C45/82 , C07C47/198
摘要： The invention relates to a method for producing a pure aliphatic dialdehyde monoacetal by reacting the corresponding aliphatic dialdehyde or a precursor of the corresponding aliphatic dialdehyde with one or more aliphatic monohydric or polyhydric alcohols, during which water is isolated by distillation while obtaining a reaction mixture that is separated by distillation. The invention is characterized in that the separation by distillation is continuously carried out in a partition column during which pure aliphatic dialdehyde monoacetal is obtained as a side-stream of the partition column or the separation by distillation is continuously carried out in two distillation columns during which crude aliphatic dialdehyde monoacetal is obtained as a side-stream in the first distillation column, the crude aliphatic dialdehyde monoacetal is fed to the second distillation column, and pure aliphatic dialdehyde monoacetal is obtained as a side-stream from the second distillation column.

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