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    • 12. 发明公开
    • Continuous digester for the implementaion of dissolved solids profiling
    • 连续蒸煮器用于执行制浆与溶解的固体的控制
    • EP0822288A2
    • 1998-02-04
    • EP97118114.4
    • 1994-07-20
    • Ahlstrom Machinery, Inc.
    • MARCOCCIA, Bruno, S.PROUGH, J., RobertLAAKSO, Richard, O.CHASSE, R., Fred
    • D21C7/00D21C7/12D21C3/24D21C3/22
    • D21C3/02D21C3/022D21C3/22D21C3/224D21C3/24D21C7/00D21C7/12D21C7/14D21C9/02D21C11/0021D21C11/04D21G7/00
    • Digester systems for producing paper pulp from comminuted cellulosic fibrous material take into account the level of dissolved organic materials (DOM), such as lignin, hemi-cellulose, and cellulose, maintaining the DOM level at about 100 g/l throughout the cook (particularly kraft cook). In order to make sure there is sufficient liquid to slurry the material in the feed system of a two vessel system, some liquid is withdrawn from the circulation conduits between the digester and impregnation vessel, cooled, and fed to the feed system. In a vapor phase digester, the level of liquid at the top of the digester is more precisely controlled by circulating some of the withdrawn liquid from a circulatory loop of the digester to the level tank associated with the feed system. An in-line drainer may be provided in the feed system between a make-up liquor pump and a liquid inlet conduit leading to the top of an impregnation vessel. Within the digester, a set of extraction/dilution screens is provided specifically positioned and spaced from each other, and with respect to a reintroduction conduit opening, so that mixing of different DOM concentration liquids is minimized.
    • 从粉碎了的纤维素纤维材料生产纸浆蒸煮系统考虑到溶解的有机材料(DOM)的电平:例如木质素,半纤维素,和纤维素,保持在约100克/升的DOM水平在整个厨师(特别是 硫酸盐蒸煮)。 为了确保有足够的液体,以浆料在两个血管系统的进料系统的材料,一些液体从蒸煮和浸渍容器之间的循环导管中取出,冷却,并供给到进料系统,在一个汽 态蒸煮,液体在蒸煮器的顶部的电平更准确地通过从蒸煮与进料系统相关联的水平槽的循环回路中循环的一些排出的液体的控制。所述的直列式排水可被提供 化妆液泵和液体入口导管通向一个浸渍容器的顶部之间的进料系统。 内蒸煮,一组提取/稀释屏幕提供特别定位且彼此间隔开,并且相对于一个重新引入导管开口所以并混合的不同DOM的浓度液体被最小化。
    • 15. 发明公开
    • METHOD FOR ISOLATING LIGNIN FROM A BIOMASS AND PRODUCTS PROVIDED THEREFROM
    • 从生物体中分离木质素的方法和由此提供的产品
    • EP3180300A1
    • 2017-06-21
    • EP15829162.5
    • 2015-02-11
    • Green Extraction Technologies, Inc.
    • MITCHELL, Melvin Glenn
    • C07C37/54F15D1/00
    • C08H6/00C08B15/08C08B37/0057C08G63/06C08G63/912C08H8/00D21C1/02D21C3/02D21C3/224D21H11/00
    • The process includes pretreating the biomass to provide a fluidized biomass. The fluidized biomass is then subjected to high frequency pulses and shear forces without denaturing/degrading the individual components of the biomass. The biomass is then subjected to compressive force to separate a first liquid fraction from a first fractionated biomass. The first fractionated biomass may again then be subjected to the same high frequency pulses and shear forces as previously, particularly if there are hemicellulose and/or sugars still present in the first fractionated biomass. Compressive forces are used to separate a second liquid fraction from a second fractionated biomass. The second fractionated biomass is subjected to oxidation such as with hydrogen peroxide and base at a pH above 7. The second fractioned biomass is then subjected to compressive forces to provide water soluble lignin which may be precipitated by reducing the pH.
    • 该方法包括用第一种碱性溶液如氢氧化钠预处理生物质,并机械地改变纤维以提供流化的生物质。 然后使流化的生物质经受高频脉冲和剪切力,而不使生物质的各个组分变性。 然后使生物质经受压缩力以从第一分馏生物质中分离出第一液体部分。 第一分级生物质可再次经受与先前相同的高频脉冲和剪切力,特别是如果在第一分级生物质中仍存在半纤维素和/或糖。 使用压缩力从第二分馏生物质分离第二液体部分。 第二分级生物质例如用8-12的pH值的过氧化氢进行氧化。然后对第二分级生物质施加压缩力以分离水溶性形式的生物质的一种或多种水不溶性组分。
    • 16. 发明公开
    • VERFAHREN ZUR GEWINNUNG VON CELLULOSE
    • EP3024974A1
    • 2016-06-01
    • EP14744103.4
    • 2014-07-25
    • Fülling, Rainer
    • SCHLABACH, HeikoFÜLLING, Rainer
    • D21C1/10C08H8/00D21C7/00D21C7/14D21C11/00D21C11/04C08L97/02C02F9/00D21C5/02C12P7/10
    • D21C3/02C08B1/00C08H8/00C08L1/02C08L97/02D21C1/10D21C3/224D21C5/02D21C7/00D21C7/14D21C9/08D21C11/00D21C11/04Y02E50/16Y02W30/648
    • The present invention relates to a process for obtaining cellulose or a mixture containing at least cellulose and at least lignocellulose from at least one substrate that is at least to some extent amenable to fermentation comprising at least the steps of (1) to (3) and optionally (4), namely conversion of the substrate via addition of at least one inorganic base into an aqueous mixture with pH ≥ 8.5 (step 1), ultrasound treatment of the aqueous mixture obtained after step (1) (step 2), separation of the aqueous mixture obtained after step (2) into a liquid aqueous phase and a disperse mixture containing cellulose or a mixture containing at least cellulose and at least lignocellulose (step 3) and optionally purification of the disperse mixture obtained after step (3) containing cellulose or of the mixure containing at least cellulose and at least lignocellulose (step 4), where step (1) and step (2) of the process respectively are carried out at a temperature
    • 本发明涉及一种获得纤维素或至少含有纤维素和至少一种木质纤维素的混合物的方法,该至少一种底物至少在一定程度上适于发酵,其包括至少步骤(1)至(3)和 任选地(4),即通过将至少一种无机碱加入到具有pH≥8.5(步骤1)的水性混合物中的底物的转化,超声处理在步骤(1)(步骤2)之后获得的含水混合物,分离 步骤(2)中获得的含水混合物加入到液体水相中,以及含有至少纤维素和至少木质纤维素(步骤3)的纤维素或混合物的分散混合物,并任选地纯化在步骤(3)之后获得的分散混合物, 纤维素或至少含有纤维素和至少木质纤维素的混合物(步骤4),其中该方法的步骤(1)和步骤(2)分别在<100℃的温度下进行,其中u 步骤(2)中的超声处理在一个或多个处理阶段进行,其中处理阶段的瓷砖持续时间在0.2至60秒的范围内,并且每个处理阶段以超声波频率在14至22范围内进行 千赫。
    • 20. 发明公开
    • Dissolved solids control in pulp production
    • 纸浆生产中的溶解固体控制
    • EP1308555A2
    • 2003-05-07
    • EP03075034.3
    • 1994-02-25
    • Andritz Inc.
    • Marcoccia, Bruno S.Prough, Robert J.Laakso, Richard O.Phillips, Joseph R.Ryham, Rolf C.Richardsen, Jen T., Andritz Inc.Chasse, R. Fred
    • D21C7/12D21C7/14D21C3/24
    • D21C3/02D21C3/22D21C3/224D21C3/24D21C7/00D21C7/12D21C7/14D21C9/02D21C11/0021D21C11/04D21G7/00
    • A single vessel digester system for digesting cellulosic fibrous material comprises a substantially upright vessel (221) having a top (220) and bottom (222) with a slurry of comminuted cellulosic material to be digested introduced adjacent the top (220), and pulp withdrawn adjacent the bottom (222); the vessel having a continuous cooking zone disposed at a first level of said digester (221), and including a first screen (225) for removing liquor from the cooking zone and a cooking circulation loop (230, 235, 238, 239) associated with said first screen (225) for circulating removed liquor to the interior of said digester (221) near the vicinity of said first screen (225); and an extraction screen (245) with extraction conduit (246) located at a second vertical level in said vessel (221), below said first level, and having means for adding dilution liquid (241; 242), having a lower dissolved organic material concentration than the liquor removed in said cooking circulation loop (230, 235, 238, 239), to said cooking circulation loop (230, 235, 238, 239), to reduce the concentration of DOM in the digester and thereby increase the strength of the pulp so-produced.
    • 用于消化纤维素纤维材料的单容器消化器系统包括具有顶部(220)和底部(222)的基本直立的容器(221),其具有待被消化的粉碎的纤维素材料的浆料,所述纤维素材料被引入邻近顶部(220),并且纸浆回收 邻近底部(222); 所述容器具有设置在所述消化器(221)的第一层上的连续烹饪​​区,并且包括用于从所述烹饪区移除液体的第一筛网(225)和与所述烹饪区相关联的烹饪循环回路(230,235,238,239) 所述第一筛(225)用于将去除的液体循环到靠近所述第一筛(225)附近的所述蒸煮器(221)的内部; 以及具有位于所述容器(221)中的第二垂直高度处并在所述第一高度之下并且具有用于添加稀释液体(241; 242)的装置的提取导管(246)的提取筛网(245),所述稀释液体具有较低溶解的有机材料 浓度低于在所述蒸煮循环回路(230,235,238,239)中去除到所述蒸煮循环回路(230,235,238,239)中的液体,以降低蒸煮器中DOM的浓度,从而增加 这样生产的纸浆。