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    • 2. 发明授权
    • Process for obtaining gaseous nitrogen
    • 获得气态氮的方法
    • US06470707B2
    • 2002-10-29
    • US09810708
    • 2001-03-19
    • Dietrich RottmannChristian Kunz
    • Dietrich RottmannChristian Kunz
    • F25J304
    • F25J3/044F25J3/04321F25J3/04351
    • For obtaining gaseous nitrogen by low-temperature separation from air, a distillation column system has a single column (4). Compressed air (1) is cooled in a main heat exchanger (2) and fed (3) to single column (4). A nitrogen-rich fraction (5, 7, 8) is drawn off from the distillation column system and compressed at least in part in a circulation compressor (9, 1063). A first part (12, 13) of nitrogen-rich fraction (5, 7, 8) is fed downstream from circulation compressor (9) to the liquefaction chamber of a condenser-evaporator (14) and is condensed under a pressure higher than the operating pressure of single column (4), so to form nitrogen-rich liquid (15, 16). A liquid oxygen-enriched fraction (231) from the distillation column system is at least partially evaporated in the evaporation chamber of condenser-evaporator (14). A first oxygen-enriched gas (234, 533) formed in the evaporation chamber of condenser-evaporator (14), is introduced into single column (4). A second portion (19, 20, 1064) of the nitrogen-rich fraction (5, 7, 8) is drawn off at least at times as gaseous nitrogen product. A second oxygen-enriched gas (221, 521) is removed from the evaporation chamber of condenser-evaporator (14), work expanded (23), and heated in main heat exchanger (2).
    • 为了通过与空气进行低温分离获得气态氮,蒸馏塔系统具有单柱(4)。 压缩空气(1)在主热交换器(2)中冷却,并将(3)供给单塔(4)。 将富氮馏分(5,7,8)从蒸馏塔系统中排出并至少部分压缩在循环压缩机(9,1063)中。 将富氮馏分(5,7,8)的第一部分(12,13)从循环压缩机(9)的下游供给到冷凝器 - 蒸发器(14)的液化室,并在高于 单塔(4)的操作压力,从而形成富氮液体(15,16)。 来自蒸馏塔系统的液体富氧馏分(231)在冷凝器 - 蒸发器(14)的蒸发室中至少部分蒸发。 形成在冷凝器 - 蒸发器(14)的蒸发室中的第一富氧气体(234,533)被引入单塔(4)中。 至少有时作为气态氮产物排出富氮馏分(5,7,8)的第二部分(19,20,1046)。 第二富氧气体(221,521)从冷凝器 - 蒸发器(14)的蒸发室中移出,工作膨胀(23),并在主热交换器(2)中加热。
    • 5. 发明授权
    • Process and device for production of oxygen and nitrogen
    • 用于生产氧气和氮气的方法和装置
    • US06490884B2
    • 2002-12-10
    • US09990365
    • 2001-11-23
    • Herbert SchoeneckerJurgen Voit
    • Herbert SchoeneckerJurgen Voit
    • F25J304
    • F25J3/04224F25J3/04357F25J3/04393F25J3/04412F25J2200/54F25J2200/90F25J2205/02F25J2245/42
    • Oxygen and nitrogen are produced by low-temperature separation of air in a rectification system that has a pressure column (4) and a low-pressure column (5). Charging air (1, 3) is introduced into pressure column (4). An oxygen-containing liquid fraction (8, 10) is removed from pressure column (4) and fed into low-pressure column (5). Gaseous nitrogen (17) from low-pressure column (5) is at least partially condensed in a top condenser (7) by indirect heat exchange with an evaporating cooling fluid (15). A nitrogen product stream (19) is removed from low-pressure column (5) and/or pressure column (4). An oxygen product stream (61, 62, 63) is pulled off from low-pressure column (5). The cooling fluid for top condenser (7) of low-pressure column (5) is formed by an intermediate liquid (15) that is drawn off from an intermediate point on low-pressure column (5).
    • 在具有压力塔(4)和低压塔(5)的精馏系统中通过空气的低温分离产生氧气和氮气。 将充气空气(1,3)引入压力塔(4)。 将含氧液体馏分(8,10)从压力塔(4)中取出并进料到低压塔(5)中。 来自低压塔(5)的气态氮(17)通过与蒸发冷却流体(15)的间接热交换在顶部冷凝器(7)中至少部分地冷凝。 氮气产物流(19)从低压塔(5)和/或压力塔(4)中移出。 将氧气产物流(61,62,63)从低压塔(5)中拉出。 用于低压塔(5)的顶部冷凝器(7)的冷却流体由从低压塔(5)上的中间点排出的中间液体(15)形成。
    • 7. 发明授权
    • Process and apparatus for producing pressurized oxygen and krypton/xenon by low-temperature fractionation of air
    • 通过空气的低温分馏产生加压氧和氪/氙的方法和装置
    • US06301929B1
    • 2001-10-16
    • US09452167
    • 1999-12-01
    • Stefan Lochner
    • Stefan Lochner
    • F25J304
    • F25J3/04412F25J3/04745F25J2200/34F25J2200/92F25J2200/94F25J2235/50
    • The process and the apparatus serve for producing pressurized oxygen and krypton/xenon by low-temperature fractionation of air. The rectifying system has a low-pressure column (3) for the nitrogen-oxygen separation and a krypton-xenon enrichment column (15). Compressed and prepurified feed air (4) is introduced into the rectifying system. A first oxygen fraction (11) is taken off from the low-pressure column (3), brought (12) to an elevated pressure in the liquid state, vaporized and removed as gaseous pressurized oxygen product (24). In addition, a second oxygen fraction (16) is taken off from the low-pressure column (3) and passed (18) into the lower or central region of the krypton-xenon enrichment column (15). The first oxygen fraction (11) is taken off at least one actual or theoretical plate above the bottom of the low-pressure column (3) and, after the pressure elevation (12) is introduced (14) in the liquid state into the upper region of the krypton-xenon enrichment column (15). A krypton-enriched and/or xenon-enriched fraction (19) is taken off from the lower region of the krypton-xenon enrichment column (15). The pressurized oxygen product (24) is withdrawn in the gaseous state from the upper region of the krypton-xenon enrichment column (15).
    • 该方法和装置用于通过空气的低温分馏产生加压氧和氪/氙。 整流系统具有用于氮 - 氧分离的低压塔(3)和氪 - 氙浓缩塔(15)。 将压缩和预净化的进料空气(4)引入整流系统。 第一氧气馏分(11)从低压塔(3)中取出,使(12)处于液态的升高的压力下,作为气体加压氧产物(24)蒸发并除去。 此外,第二氧分数(16)从低压塔(3)中取出并通过(18)进入氪 - 氙浓缩塔(15)的下部或中心区域。 第一氧气馏分(11)从低压塔(3)底部的至少一个实际或理论塔板上取出,并且在压力升高(12)以液体状态引入(14)之后,上部 氪 - 氙浓缩柱(15)的区域。 从氪 - 氙浓缩塔(15)的下部区域取出富氪和/或氙浓缩馏分(19)。 加压氧产物(24)以气态从氪 - 氙浓缩塔(15)的上部区域排出。