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1. 发明授权

US06359157B2 Process for the transesterification of fat and/or oil of biological origin by means of alcoholysis 失效
标题翻译：通过醇解将生物来源的脂肪和/或油的酯交换反应的方法
公开(公告)号：US06359157B2
公开(公告)日：2002-03-19
申请号：US09884328
申请日：2001-06-19
申请人： Siegfried Peter , Eckhard Weidner , Hans-Peter Neuner , Ruth Ganswindt
发明人： Siegfried Peter , Eckhard Weidner , Hans-Peter Neuner , Ruth Ganswindt
IPC分类号： C11C100
CPC分类号： C11C3/003 , Y02E50/13
摘要： A process for the transesterification of fat and/or oil of biological origin by means of alcoholysis comprises the following steps: provision in a vessel of fat and/or oil of biological origin to be transesterified, and implementation of alcoholysis by addition of an alkanol, in particular of a monohydric alkanol, and of a catalyst to the fat and/or oil that has been provided. with a view to eliminating the disadvantages of traditional transesterification processes, a metal salt of an amino acid or of an amino-acid derivative is used as catalyst, said metal salt being insoluble in alkanols.
摘要翻译：通过醇解将生物来源的脂肪和/或油的酯交换的方法包括以下步骤：在容器中提供待酯交换的生物来源的脂肪和/或油，以及通过加入链烷醇来进行醇解的实施特别是一元烷醇，以及提供的脂肪和/或油的催化剂。为了消除传统酯交换方法的缺点，使用氨基酸或氨基酸衍生物的金属盐作为催化剂，所述金属盐不溶于链烷醇。

2. 发明授权

US06608223B2 Cholesterol lowering structured lipids containing omega 3 polyunsaturated fatty acids and their process thereof 失效
标题翻译：含有ω3多不饱和脂肪酸的降胆固醇的结构脂质及其制备方法
公开(公告)号：US06608223B2
公开(公告)日：2003-08-19
申请号：US10014247
申请日：2001-10-22
申请人： Reena Rao , Kari Sambaiah , Belur Ramaswamy Lokesh
发明人： Reena Rao , Kari Sambaiah , Belur Ramaswamy Lokesh
IPC分类号： C11C100
CPC分类号： A23D9/02 , A23D9/00 , C11C3/10
摘要： Unique structured lipids obtained from interestifying coconut oil with free fatty acids obtained from hydrolysis of triglycerides of an animal source, said structured lipids rich in omega-3-poly unsaturated fatty acid and medium chain fatty acid and a process for the production of said structured lipids.
摘要翻译：通过从动物来源的甘油三酸酯的水解得到的游离脂肪酸从所述椰子油中获得的独特结构化脂质，富含ω-3-多不饱和脂肪酸和中链脂肪酸的所述结构化脂质以及所述结构化脂质的生产方法。

3. 发明授权

US06281373B1 Process for the preparation of dimeric fatty acid C1-4 alkyl esters 失效
标题翻译：制备二聚脂肪酸C 1-4烷基酯的方法
公开(公告)号：US06281373B1
公开(公告)日：2001-08-28
申请号：US09081878
申请日：1998-05-19
申请人： Setsuo Sato , Carlos Alberto de Moura , Michael Sublett , C. William Blewett
发明人： Setsuo Sato , Carlos Alberto de Moura , Michael Sublett , C. William Blewett
IPC分类号： C11C100
CPC分类号： C11C3/003
摘要： Process for the preparation of dimeric fatty acid C1-4 alkyl esters comprising the steps of A) reacting a soybean oil condensate obtained from the deodorization of refined soybean oil and which contains less than 30% by weight of free and esterified oleic acid based on the total weight of free and esterified fatty acids in said condensate, with a C1-4 alkanol in the presence of a zinc oxide catalyst to convert free fatty acids and fatty acid glyceride esters to fatty acid C1-4 alkyl esters; B) removing excess C1-4 alkanol, volatile reaction by-products, water, and the zinc oxide catalyst from the resulting reaction mixture; C) heating the reaction mixture from step B) under vacuum to obtain a distillate of fatty acid C1-4 alkyl esters; D) separating the distillate from step C) into a fraction containing mostly C16-18 saturated fatty acid C1-4 alkyl esters and a second fraction containing mostly C16-18 unsaturated fatty acid C1-4 alkyl esters wherein the oleic acid C1-4 alkyl ester content is less than about 35% by weight thereof; and E) dimerizing said second fraction in the presence of montmorillonite clay.
摘要翻译：用于制备二聚脂肪酸C 1-4烷基酯的方法，包括以下步骤：A）将由精制大豆油除臭得到的大豆油缩合物与基于总计的含有少于30重量％的游离和酯化油酸反应所述缩合物中游离和酯化的脂肪酸的重量与C1-4链烷醇在氧化锌催化剂存在下将游离脂肪酸和脂肪酸甘油酯转化为脂肪酸C 1-4烷基酯; B）除去过量的C 1 -C 4烷基酯， 4链烷醇，挥发性反应副产物，水和氧化锌催化剂; C）在真空下加热来自步骤B）的反应混合物，得到脂肪酸C 1-4烷基酯的馏出物; D）分离来自步骤C）的馏出物成为主要含有C 16-18饱和脂肪酸C 1-4烷基酯的馏分和主要含有C 16-18不饱和脂肪酸C 1-4烷基酯的第二馏分，其中油酸C 1-4烷基酯含量小于约35重量％; 和E）在蒙脱石粘土存在下使所述第二级分二聚。

4. 发明授权

US06407269B2 Catalyst for transesterification 有权
标题翻译：酯交换催化剂
公开(公告)号：US06407269B2
公开(公告)日：2002-06-18
申请号：US09885962
申请日：2001-06-22
申请人： Jun Kaita , Taku Mimura , Noriaki Fukuoka , Yasuyuki Hattori
发明人： Jun Kaita , Taku Mimura , Noriaki Fukuoka , Yasuyuki Hattori
IPC分类号： C11C100
CPC分类号： C11C3/003 , B01J27/16 , B01J27/1811 , B01J27/1853
摘要： The present invention provides a heterogeneous catalyst which is highly active, excellent in selectivity and free from elution of its catalyst-components during reaction and which has long lifetime. That is, a phosphate of a metal selected from the group consisting of aluminum, gallium and iron is used as the catalyst for transesterification of the present invention.
摘要翻译：本发明提供了一种非均相催化剂，它具有高活性，选择性优异，反应期间催化剂组分不溶解，寿命长。也就是说，使用选自铝，镓和铁的金属的磷酸盐作为本发明的酯交换反应的催化剂。

5. 发明授权

US06262285B1 Process for dry synthesis and continuous separation of a fatty acid methyl ester reaction product 有权
标题翻译：干法合成和连续分离脂肪酸甲酯反应产物的方法
公开(公告)号：US06262285B1
公开(公告)日：2001-07-17
申请号：US09339436
申请日：1999-06-24
申请人： William M. McDonald
发明人： William M. McDonald
IPC分类号： C11C100
CPC分类号： C11C1/10 , C11C3/003
摘要： A continuous separation of fatty acid methyl esters (FAME) from glycerol in a low pressure dry transesterification process for vegetable oil is provided. Improved purity of the FAME and the glycerol fractions are achieved via the use of continuous decantation so as to thereby eliminate the need for a water wash step for the FAME fraction. Excess methanol from the FAME and the glycerol fractions is readily recovered in a dry vacuum extraction process. Water which has been inadvertently introduced into the process is removed from the recovered excess methanol by desiccant columns equipped with molecular sieves instead of the traditional energy and capital intensive fractionation processes practiced for this purpose.
摘要翻译：提供了在植物油低压干燥酯交换法中从甘油中连续分离脂肪酸甲酯（FAME）。通过使用连续倾析来实现FAME和甘油馏分的纯度提高，从而消除了对FAME级分的水洗步骤的需要。来自FAME的过量甲醇和甘油馏分在干燥真空萃取过程中很容易回收。通过装备有分子筛的干燥剂塔，而不是为此目的实行的传统能量和资本密集型分馏方法，从回收的过量甲醇中除去已经无意地引入该方法的水。

6. 发明授权

US06762313B2 Processes for preparing linoleic acid raw materials for subsequent conjugation 有权
标题翻译：制备亚油酸原料用于后续共轭的方法
公开(公告)号：US06762313B2
公开(公告)日：2004-07-13
申请号：US10380564
申请日：2003-03-13
申请人： Albert Strube , Uwe Hoemmerich , Bernhard Gutsche
发明人： Albert Strube , Uwe Hoemmerich , Bernhard Gutsche
IPC分类号： C11C100
CPC分类号： C11C3/04 , C11B3/12 , C11C3/10
摘要： Processes for preparing linoleic acid raw materials are described wherein the processes comprise: (a) transesterifying a triglyceride component with an alcohol having from 1 to 4 carbon atoms, at a temperature of from 80 to 120° C., to form a transesterification mixture comprising linoleic acid esters and one or more by-products selected from the group consisting of glycerides, free glycerol, and soaps, wherein the triglyceride component is comprised of at least 60% by weight linoleic acid; and (b) removing the one or more by-products from the transesterification mixture.
摘要翻译：描述了制备亚油酸原料的方法，其中所述方法包括：（a）在80至120℃的温度下将甘油三酯组分与具有1至4个碳原子的醇进行酯交换以形成酯交换混合物，其包含亚油酸酯和选自甘油酯，游离甘油和皂的一种或多种副产物，其中甘油三酯组分由至少60重量％的亚油酸组成; 和（b）从酯交换混合物中除去一种或多种副产物。

7. 发明授权

US06723863B2 Methods for the preparation of propylene glycol fatty acid esters 有权
标题翻译：丙二醇脂肪酸酯的制备方法
公开(公告)号：US06723863B2
公开(公告)日：2004-04-20
申请号：US10213434
申请日：2002-08-07
申请人： Inmok Lee , George Poppe
发明人： Inmok Lee , George Poppe
IPC分类号： C11C100
CPC分类号： C11C3/10 , C07C67/03 , C11C3/003 , C07C69/52
摘要： A process of producing a light-colored, high-monoester mixture from a polyol and an oil is provided wherein the process eliminates the use of organic solvents, multiple water washings and/or molecular distillation. The reactants, a polyol and an oil, described herein, condense in the presence of a catalyst, described herein, at a temperature range from about 180° C. to about 280° C. under an inert atmosphere or the vapor pressure of the polyol with a pressure of about 0 to about 500 psig to yield a monoester mixture possessing a desirable monoester composition and color. The present process yields a final product similar to that of processes which require the use of solvents, multiple water washings and/or molecular distillation.
摘要翻译：提供了由多元醇和油制备浅色高分子混合物的方法，其中该方法消除了使用有机溶剂，多次水洗和/或分子蒸馏。本文所述的反应物，多元醇和油，在本文所述的催化剂存在下，在约180℃至约280℃的温度范围内，在惰性气氛下或多元醇的蒸气压下冷凝压力为约0至约500psig，以产生具有所需单酯组成和颜色的单酯混合物。本方法产生类似于需要使用溶剂，多次水洗和/或分子蒸馏的方法的最终产物。

8. 发明授权

US06586608B1 Lipidic calcium compounds and use for treatment of osteoporosis 失效
标题翻译：脂质钙化合物和用于治疗骨质疏松症
公开(公告)号：US06586608B1
公开(公告)日：2003-07-01
申请号：US10261959
申请日：2002-10-01
申请人： Elena Avram
发明人： Elena Avram
IPC分类号： C11C100
CPC分类号： C11C1/00 , A23L33/115 , A23L33/16 , A61K31/19 , A61K31/215 , A61K31/336 , A61K33/06 , A61K2300/00
摘要： A method for making a composition containing calcium incorporated into a fatty acid or fatty ester compound and the compositions produced by this method. These compositions can be administered to a patient to increase the calcium content of cells or tissue having a calcium deficiency or to treat at least some of the symptoms of diseases or adverse effects caused by this calcium deficiency.
摘要翻译：一种制备包含掺入脂肪酸或脂肪酸酯化合物中的钙的组合物的方法和通过该方法制备的组合物。这些组合物可以施用于患者以增加具有钙缺乏的细胞或组织的钙含量，或者治疗由该缺钙引起的疾病或不良反应的至少一些症状。

9. 发明授权

US06570030B2 Method for preparing fatty acid esters from seeds or fruits 失效
公开(公告)号：US06570030B2
公开(公告)日：2003-05-27
申请号：US10014591
申请日：2001-12-14
申请人： Fumisato Goto , Toshio Sasaki
发明人： Fumisato Goto , Toshio Sasaki
IPC分类号： C11C100
CPC分类号： C11C3/003 , C11C3/10
摘要： A fatty acid ester prepared by treating botanical seeds or fruits with a monohydric alcohol having 1 to 10 carbon atoms under pressure at a temperature of at least 180° C., preferably under supercritical conditions.

10. 发明授权

US06350890B1 Method for obtaining fatty acids from biomass by combined in/situ extraction, reaction and chromatography using compressed gases 有权
标题翻译：通过使用压缩气体进行原位萃取，反应和色谱联合从生物质中获得脂肪酸的方法
公开(公告)号：US06350890B1
公开(公告)日：2002-02-26
申请号：US09744142
申请日：2001-02-16
申请人： Thomas Kiy , Christoph Siffrin , Heinz Engelhardt , Dirk Fabritius
发明人： Thomas Kiy , Christoph Siffrin , Heinz Engelhardt , Dirk Fabritius
IPC分类号： C11C100
CPC分类号： C11C3/003 , A23L33/12 , A61K31/23 , B01D15/08 , C11B1/104 , C11B7/005 , C11C3/10
摘要： The invention relates to a method for obtaining fatty acid esters and fatty acids, preferably unsaturated fatty acid ethyl esters, from biological sources by continuous, combined in-situ extraction, reaction and chromatography. The invention is characterized in that simultaneously and in the same location, in the presence of a compressed gas and an 0.5-5 % stream of lower alcohols as modifiers and in the presence of an inert catalyst, the fatty acids are fully transesterified from their native fatty acid sources, which are selectively desorbed and eluated in the conditions specified above.
摘要翻译：本发明涉及一种通过连续的原位萃取，反应和层析法从生物来源获得脂肪酸酯和脂肪酸，优选不饱和脂肪酸乙酯的方法。本发明的特征在于，在压缩气体和0.5-5％的低级醇流作为改性剂的同时和在相同的位置，在惰性催化剂的存在下，脂肪酸从它们的天然物完全酯交换脂肪酸源，其在上述条件下被选择性地解吸和洗脱。

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