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1. 发明授权

US06281373B1 Process for the preparation of dimeric fatty acid C1-4 alkyl esters 失效
标题翻译：制备二聚脂肪酸C 1-4烷基酯的方法
公开(公告)号：US06281373B1
公开(公告)日：2001-08-28
申请号：US09081878
申请日：1998-05-19
申请人： Setsuo Sato , Carlos Alberto de Moura , Michael Sublett , C. William Blewett
发明人： Setsuo Sato , Carlos Alberto de Moura , Michael Sublett , C. William Blewett
IPC分类号： C11C100
CPC分类号： C11C3/003
摘要： Process for the preparation of dimeric fatty acid C1-4 alkyl esters comprising the steps of A) reacting a soybean oil condensate obtained from the deodorization of refined soybean oil and which contains less than 30% by weight of free and esterified oleic acid based on the total weight of free and esterified fatty acids in said condensate, with a C1-4 alkanol in the presence of a zinc oxide catalyst to convert free fatty acids and fatty acid glyceride esters to fatty acid C1-4 alkyl esters; B) removing excess C1-4 alkanol, volatile reaction by-products, water, and the zinc oxide catalyst from the resulting reaction mixture; C) heating the reaction mixture from step B) under vacuum to obtain a distillate of fatty acid C1-4 alkyl esters; D) separating the distillate from step C) into a fraction containing mostly C16-18 saturated fatty acid C1-4 alkyl esters and a second fraction containing mostly C16-18 unsaturated fatty acid C1-4 alkyl esters wherein the oleic acid C1-4 alkyl ester content is less than about 35% by weight thereof; and E) dimerizing said second fraction in the presence of montmorillonite clay.
摘要翻译：用于制备二聚脂肪酸C 1-4烷基酯的方法，包括以下步骤：A）将由精制大豆油除臭得到的大豆油缩合物与基于总计的含有少于30重量％的游离和酯化油酸反应所述缩合物中游离和酯化的脂肪酸的重量与C1-4链烷醇在氧化锌催化剂存在下将游离脂肪酸和脂肪酸甘油酯转化为脂肪酸C 1-4烷基酯; B）除去过量的C 1 -C 4烷基酯， 4链烷醇，挥发性反应副产物，水和氧化锌催化剂; C）在真空下加热来自步骤B）的反应混合物，得到脂肪酸C 1-4烷基酯的馏出物; D）分离来自步骤C）的馏出物成为主要含有C 16-18饱和脂肪酸C 1-4烷基酯的馏分和主要含有C 16-18不饱和脂肪酸C 1-4烷基酯的第二馏分，其中油酸C 1-4烷基酯含量小于约35重量％; 和E）在蒙脱石粘土存在下使所述第二级分二聚。

2. 发明授权

US06548717B1 Process for making branched, substantially unsaturated fatty alcohols 失效
标题翻译：制备支链，基本不饱和脂肪醇的方法
公开(公告)号：US06548717B1
公开(公告)日：2003-04-15
申请号：US09602988
申请日：2000-06-23
申请人： Alfred Westfechtel , Norbert Huebner , Lothar Friesenhagen , Gerrit Pelzer , Norbert Klein , Ansgar Behler , Thomas B. Downing , Steven A. Kennedy , C. William Blewett
发明人： Alfred Westfechtel , Norbert Huebner , Lothar Friesenhagen , Gerrit Pelzer , Norbert Klein , Ansgar Behler , Thomas B. Downing , Steven A. Kennedy , C. William Blewett
IPC分类号： C07C2704
CPC分类号： A61K8/342 , A61K47/10 , A61Q19/00 , C07C29/149 , C11D3/2031 , C07C33/035 , C07C33/02
摘要： A process for making branched, substantially unsaturated fatty alcohols involving: (a) providing a C16-22 fatty acid; (b) dimerizing the C16-22 fatty acid to form a monomer fraction containing branched, substantially unsaturated fatty acids; (c) removing the monomer fraction; (d) esterifying the branched, substantially unsaturated fatty acids contained in the monomer fraction into branched, substantially unsaturated fatty acid methyl esters; and (e) hydrogenating the branched, substantially unsaturated fatty acid methyl esters with their double bonds intact, to form the branched, substantially unsaturated fatty alcohols.
摘要翻译：一种制备支化的，基本上不饱和的脂肪醇的方法，包括：（a）提供C16-22脂肪酸; （b）使C16-22脂肪酸二聚以形成含有支链，基本上不饱和脂肪酸的单体级分; （c）除去单体馏分; （d）将单体部分中所含的支化的，基本上不饱和的脂肪酸酯化成支链的，基本上不饱和的脂肪酸甲酯; 和（e）使其支链，基本上不饱和的脂肪酸甲酯以其双键完整氢化，形成支链的，基本上不饱和的脂肪醇。

3. 发明授权

US5907067A Method of alkoxylating alcohols 失效
标题翻译：烷醇化醇的方法
公开(公告)号：US5907067A
公开(公告)日：1999-05-25
申请号：US827896
申请日：1997-04-09
申请人： Jeffrey A. Barnhorst , A. Frederick Elsasser, Jr. , C. William Blewett
发明人： Jeffrey A. Barnhorst , A. Frederick Elsasser, Jr. , C. William Blewett
IPC分类号： C07C41/03 , C07C41/36 , C07C43/11
CPC分类号： C07C41/36 , C07C41/03
摘要： Alkoxylated alcohols containing no insoluble matter which would prevent the spray application of such materials are obtained by reacting an alcohol and epoxide in the presence of a catalytic amount of a calcined hydrotalcite catalyst to form a crude alkoxylated product. The crude product is then passed through silica gel to remove insoluble by-products.
摘要翻译：通过在催化量的煅烧水滑石催化剂存在下使醇和环氧化物反应形成粗制烷氧基化产物，可获得不含不溶物的不含不溶物的烷氧基化醇，这些不溶物可防止这种物质的喷雾施用。然后将粗产物通过硅胶以除去不溶性副产物。

4. 发明授权

US06623604B1 Method of recovering free fatty acids having low ester content and high acid value 失效
标题翻译：回收具有低酯含量和高酸值的游离脂肪酸的方法
公开(公告)号：US06623604B1
公开(公告)日：2003-09-23
申请号：US09586917
申请日：2000-06-05
申请人： A. Fred Elsasser , C. William Blewett
发明人： A. Fred Elsasser , C. William Blewett
IPC分类号： B01D300
CPC分类号： B01D3/143 , B01D3/38 , C07C29/80 , C11C1/10 , C11C1/103 , C07C31/04 , C07C31/08 , C07C31/10 , C07C31/12 , C07C31/125
摘要： Methods of recovering free fatty acids having a low ester content from alkanol-containing solutions and oil mixtures containing tocopherols are disclosed which involve atmospheric or vacuum stripping at low temperatures. The recovered fatty acids have a high acid value, and have high commercial value in the production of high quality (high acid value) products, e.g., dimerized fatty acids, useful in polyamide resins.
摘要翻译：公开了从含有链烷醇的溶液和含有生育酚的油混合物中回收具有低酯含量的游离脂肪酸的方法，其涉及在低温下的大气或真空汽提。回收的脂肪酸具有高酸值，并且在用于聚酰胺树脂的高品质（高酸值）产物例如二聚脂肪酸的生产中具有高商业价值。

5. 发明授权

US06242620B1 Process for making carboxylic acid esters 失效
标题翻译：制备羧酸酯的方法
公开(公告)号：US06242620B1
公开(公告)日：2001-06-05
申请号：US09035681
申请日：1998-03-05
申请人： A. Fred Elsasser , C. William Blewett , Charles M. White
发明人： A. Fred Elsasser , C. William Blewett , Charles M. White
IPC分类号： C11C300
CPC分类号： C11C3/003 , C07C29/149 , C07C67/56 , C07C69/58 , C07C69/24 , C07C31/125
摘要： Sulfur and soap contaminants are removed from carboxylic acid esters by a process comprising the steps of: (1) contacting a carboxylic acid ester with an aqueous base at a temperature of from about 225° F. to about 280° F. while removing water to form a dry, crude ester; (2) contacting the dry, crude ester with an absorbent selected from the group consisting of silica gel, hydro-silica gel and mixtures thereof; (3) separating the absorbent from the ester.
摘要翻译：通过包括以下步骤的方法从羧酸酯中除去硫和皂污染物：（1）在约225°F至约280°F的温度下使羧酸酯与碱水溶液接触，同时将水除去形成干燥的粗酯; （2）使干的粗酯与选自硅胶，水硅胶及其混合物的吸收剂接触; （3）将吸收剂与酯分离。

6. 发明授权

US4775745A Diazonium compounds useful as components for nucleic acid probes 失效
标题翻译：可用作核酸探针成分的重氮化合物
公开(公告)号：US4775745A
公开(公告)日：1988-10-04
申请号：US939370
申请日：1986-12-08
申请人： John P. Ford , Bernard F. Erlanger , C. William Blewett
发明人： John P. Ford , Bernard F. Erlanger , C. William Blewett
IPC分类号： C12Q1/68 , C07C113/00 , C07C113/04
CPC分类号： C12Q1/6827 , C12Q1/6816 , Y10S436/804 , Y10S436/828
摘要： This invention relates to a diazonium compound of the formula: ##STR1## wherein Z is selected from the group consisting of biotin, an antigen, an antibody, a photoreactive group, a fluorescent group and heavy metal-containing compounds;X is an alkylene group containing up to 18 carbon atoms in the principle chain and a total of up to 24 carbon atoms or a substituted alkylene group containing up to 18 carbon atoms in the principle chain with substituents selected from the group consisting of solubility-enhancing groups and cleavable --S--S-- containing moieties;Ar is an unsubstituted or substituted aryl or heteroaryl; andY is an anion and n is an integer from 1-3.Such compounds are useful as components for nucleic acid probes.
摘要翻译：本发明涉及下式的重氮化合物：其中Z选自生物素，抗原，抗体，光反应性基团，荧光基团和含重金属的化合物; X是在原则链中含有至多18个碳原子的亚烷基，在原理链中含有至多24个碳原子或含有至多18个碳原子的取代的亚烷基，所述取代基选自溶解度增强基团和可切割的含-SS的部分; Ar是未取代或取代的芳基或杂芳基; Y为阴离子，n为1-3的整数。这些化合物可用作核酸探针的组分。

7. 发明授权

US4069236A Aluminum acyloxides 失效
标题翻译：铝酰氧化铝
公开(公告)号：US4069236A
公开(公告)日：1978-01-17
申请号：US185805
申请日：1971-10-01
申请人： Robert B. Hutchison , C. William Blewett
发明人： Robert B. Hutchison , C. William Blewett
IPC分类号： C09K3/00 , A61K8/26 , A61K8/34 , A61Q19/00 , C07F5/06 , C08G79/00 , C08G79/10 , C11C1/00
CPC分类号： A61K8/342 , A61K8/042 , A61K8/26 , A61Q19/00 , C07F5/069 , C08G79/10
摘要： Aluminum acyloxide polymers are formed in a reaction involving approximately equimolar amounts of aluminum alkoxide, water and a branched chain, saturated aliphatic monocarboxylic acid having from about 10 to about 25 carbon atoms. These novel compounds from stable gels with non-polar liquids.
摘要翻译：在涉及大约等摩尔量的烷氧基铝，水和具有约10至约25个碳原子的支链，饱和脂肪族单羧酸的反应中形成铝酰氧化铝聚合物。这些来自具有非极性液体的稳定凝胶的新型化合物。

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