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1. 发明授权

US06730712B2 Method of manufacturing porous cross-linked polymer sheet 有权
标题翻译：多孔交联聚合物片的制造方法
公开(公告)号：US06730712B2
公开(公告)日：2004-05-04
申请号：US10169182
申请日：2002-09-27
申请人： Masazumi Sasabe , Katsuhiko Sakamoto , Kozo Nogi , Motohiro Arakawa
发明人： Masazumi Sasabe , Katsuhiko Sakamoto , Kozo Nogi , Motohiro Arakawa
IPC分类号： C08J928
CPC分类号： C08J9/28 , B29C44/5654 , C08J2201/028 , C08J2201/0504
摘要： A method for producing a porous cross-linked polymer sheet capable of slicing quickly is provided. This method comprises a step for obtaining a porous cross-linked polymer by forming and polymerizing an HIPE, a step for dehydrating the porous cross-linked polymer, and a step for subsequently slicing the dehydrated porous cross-linked polymer. According to this invention, by performing the step of dehydration prior to the conventional step of slicing, it is made possible to prevent the porous cross-linked polymer from adhering to the blade and the guides provided for a slicer, and allow the slicing to be attained quickly. By removing the salt from the polymer, it is further made possible to prevent a production device from gathering rust and the porous cross-linked polymer from permitting adhesion of rust thereto.
摘要翻译：提供了能够快速切片的多孔交联聚合物片材的制造方法。该方法包括通过HIPE的形成和聚合获得多孔交联聚合物的步骤，用于使多孔交联聚合物脱水的步骤和用于随后切割脱水多孔交联聚合物的步骤。根据本发明，通过在常规的切片步骤之前进行脱水步骤，可以防止多孔交联聚合物粘附到刀片和设置在切片机上的导向器，并允许切片为快速获得通过从聚合物中除去盐，进一步可以防止生产装置收集生锈和多孔交联聚合物从而允许生锈附着在其上。

2. 发明授权

US06730711B2 Method for production of porous cross-linked polymer material 有权
标题翻译：生产多孔交联聚合物材料的方法
公开(公告)号：US06730711B2
公开(公告)日：2004-05-04
申请号：US10149602
申请日：2002-06-13
申请人： Masazumi Sasabe , Kenji Kadonaga , Hiroki Inoue , Akiko Mitsuhashi , Hirotama Fujimaru , Masatoshi Yoshida , Masuji Izubayashi , Kazutomo Takahashi
发明人： Masazumi Sasabe , Kenji Kadonaga , Hiroki Inoue , Akiko Mitsuhashi , Hirotama Fujimaru , Masatoshi Yoshida , Masuji Izubayashi , Kazutomo Takahashi
IPC分类号： C08J928
CPC分类号： C08F8/00 , C08F20/00
摘要： A method for the production of a porous cross-linked polymer material by the polymerization of an HIPE containing a cross-linking agent, characterized by the fact at least one species of the cross-linking agent is a compound having a double bond equivalent f not less than 120 g/mol. The cross-linking agent is preferred to be a compound possessed of an alkylene oxide moiety or a vinyl polymer containing not less than two polymerizing double bonds in the molecular unit. Thus, it is made possible to produce a porous cross-linked polymer material excellent in absorbency and flexibility, permit the HIPE to be polymerized in a short time, and therefore improve the efficiency of production.
摘要翻译：通过含有交联剂的HIPE的聚合制备多孔交联聚合物材料的方法，其特征在于至少一种交联剂是具有双键当量f的化合物小于120g / mol。交联剂优选为具有烯化氧部分的化合物或在分子单元中含有不少于两个聚合双键的乙烯基聚合物。因此，可以制造吸水性和柔软性优异的多孔交联聚合物材料，能够在短时间内使HIPE聚合，从而提高生产效率。

3. 发明授权

US06472443B1 Porous polymer media 有权
标题翻译：多孔聚合物介质
公开(公告)号：US06472443B1
公开(公告)日：2002-10-29
申请号：US09603466
申请日：2000-06-22
申请人： Timothy J. Shepodd
发明人： Timothy J. Shepodd
IPC分类号： C08J928
CPC分类号： B01J20/28042 , B01D15/325 , B01J20/26 , B01J20/261 , B01J20/267 , B01J20/28014 , B01J20/28059 , B01J20/285 , B01J2220/54 , B01J2220/82 , B01J2220/84 , C08F2/06 , G01N27/44747 , Y10T428/249953 , Y10T428/249972 , Y10T428/249982
摘要： Highly crosslinked monolithic porous polymer materials for chromatographic applications. By using solvent compositions that provide not only for polymerization of acrylate monomers in such a fashion that a porous polymer network is formed prior to phase separation but also for exchanging the polymerization solvent for a running buffer using electroosmotic flow, the need for high pressure purging is eliminated. The polymer materials have been shown to be an effective capillary electrochromatographic separations medium at lower field strengths than conventional polymer media. Further, because of their highly crosslinked nature these polymer materials are structurally stable in a wide range of organic and aqueous solvents and over a pH range of 2-12.
摘要翻译：用于色谱应用的高度交联的整体多孔聚合物材料。通过使用不仅提供丙烯酸酯单体聚合的溶剂组合物，使得在相分离之前形成多孔聚合物网络，而且还使用电渗流更换用于运行缓冲液的聚合溶剂，因此对高压吹扫的需要是消除了已经显示聚合物材料是比常规聚合物介质更低场强的有效毛细管电色谱分离介质。此外，由于其高度交联的性质，这些聚合物材料在宽范围的有机和水性溶剂中以及在2-12的pH范围内在结构上是稳定的。

4. 发明授权

US06395792B1 Method for production of porous cross-linked poymer 有权
标题翻译：多孔交联聚合物的生产方法
公开(公告)号：US06395792B1
公开(公告)日：2002-05-28
申请号：US09689350
申请日：2000-10-12
申请人： Kinya Nagasuna , Hirotama Fujimaru , Kenji Kadonaga , Kozo Nogi , Katsuhiko Sakamoto , Masazumi Sasabe , Kenji Minami
发明人： Kinya Nagasuna , Hirotama Fujimaru , Kenji Kadonaga , Kozo Nogi , Katsuhiko Sakamoto , Masazumi Sasabe , Kenji Minami
IPC分类号： C08J928
CPC分类号： C08J9/283 , C08F2/32 , C08J2201/028
摘要： An object of this invention is to provide a method for the production of a porous cross-linked polymer, which permits the polymerization (curing) of a water in oil type high internal phase emulsion (HIPE) in such an exceptionally brief time as not more than 30 minutes, preferably not more than 10 minutes without impairing the stability of the HIPE. The object of this invention mentioned above can be accomplished by a method for the production of a porous cross-linked polymer which comprises steps of mixing an oil phase containing a polymerizing monomer, a cross-linking monomer, and a surfactant as essential components with a water phase containing water as an essential component thereby obtaining a water in oil type high internal phase emulsion and heating said emulsion to a prescribed curing temperature thereby polymerizing the emulsion, wherein said emulsion is formed in a thickness of not more than 50 mm and the temperature-increasing rate of the emulsion is not less than 5° C./minute.
摘要翻译：本发明的目的是提供一种生产多孔交联聚合物的方法，其允许在非常短的时间内将油包水型高内相乳液（HIPE）中的聚合（固化）不再多超过30分钟，优选不超过10分钟，而不损害HIPE的稳定性。上述本发明的目的可以通过生产多孔交联聚合物的方法来实现，该方法包括以下步骤：将含有聚合单体的油相，交联单体和表面活性剂作为必需组分混合，水相作为必要成分，由此获得油包水型高内相乳液，并将所述乳液加热到规定的固化温度，从而使乳液聚合，其中所述乳液的形成厚度不大于50mm，温度 - 乳液的增加速度不低于5℃/分钟。

5. 发明授权

US06353037B1 Foams containing functionalized metal oxide nanoparticles and methods of making same 有权
标题翻译：含有官能化金属氧化物纳米颗粒的泡沫及其制备方法
公开(公告)号：US06353037B1
公开(公告)日：2002-03-05
申请号：US09614574
申请日：2000-07-12
申请人： Kristin LaVelle Thunhorst , Douglas Alan Hanggi
发明人： Kristin LaVelle Thunhorst , Douglas Alan Hanggi
IPC分类号： C08J928
CPC分类号： C08J9/283
摘要： The invention discloses methods for making foams comprising functionalized metal oxide nanoparticles by photopolymerizing or thermally polymerizing emulsions comprising a reactive phase and a phase immiscible with the reactive phase components. Foams made from water-in-oil emulsions, including high internal phase emulsion are also disclosed. Articles and uses for the foams are also described.
摘要翻译：本发明公开了制备包含官能化金属氧化物纳米颗粒的泡沫的方法，其通过光聚合或热聚合包含反应相和不与反应相组分混合的相的乳液。还公开了由包含高内相乳液的油包水乳液制成的泡沫。还描述了泡沫的用途和用途。

6. 发明授权

US06284077B1 Stable, foamed caulk and sealant compounds and methods of use thereof 有权
标题翻译：稳定的，泡沫填缝料和密封剂化合物及其使用方法
公开(公告)号：US06284077B1
公开(公告)日：2001-09-04
申请号：US09269001
申请日：1999-12-16
申请人： Patrick J. Lucas , Anthony J. Taylor
发明人： Patrick J. Lucas , Anthony J. Taylor
IPC分类号： C08J928
CPC分类号： E04F21/06 , C08L25/14 , C08L31/04 , C09J5/08 , C09J2425/00 , C09J2431/00
摘要： Stable foam caulk, sealant and insulation compositions are disclosed. The compositions comprise solid, waxy non-ionic lipophilic surfactants having low HLB values. These surfactants, upon foamed dispensing of the composition, provide stable support for bubbles formed from drying of a latex emulsion of a film forming polymer and a volatile liquid hydrocarbon propellant. In addition to use in caulking, sealant or insulation methods, the composition can be used to form artificial terrains and other hardenable structural surfaces as backgrounds or support means for hobbies, crafts, and the like.
摘要翻译：公开了稳定的泡沫填缝料，密封剂和绝缘组合物。组合物包含具有低HLB值的固体，蜡状非离子亲脂性表面活性剂。在组合物发泡分配时，这些表面活性剂为由成膜聚合物和挥发性液体烃推进剂的胶乳乳液的干燥形成的气泡提供稳定的支持。除了用于填缝，密封剂或绝缘方法之外，组合物可以用于形成人造地形和其他可硬化结构表面作为爱好，工艺品等的背景或支撑手段。

7. 发明授权

US06251960B1 Process for production of water absorbent resin 有权
标题翻译：吸水树脂生产工艺
公开(公告)号：US06251960B1
公开(公告)日：2001-06-26
申请号：US09343460
申请日：1999-06-30
申请人： Kunihiko Ishizaki , Hisanobu Obara , Nobuyuki Harada , Yoshihiro Motono , Koji Miyake
发明人： Kunihiko Ishizaki , Hisanobu Obara , Nobuyuki Harada , Yoshihiro Motono , Koji Miyake
IPC分类号： C08J928
CPC分类号： C08J9/06 , A61L15/425 , A61L15/60 , C07C257/14 , C08J2207/12 , C08J2300/00 , Y02P20/149 , C08L33/00
摘要： A water-absorbent resin is produced by dispersing a solid blowing agent having an average particle diameter within a range of from 1 &mgr;m to 100 &mgr;m in an aqueous monomer solution containing an unsaturated monomer and a cross-linking agent, and then polymerizing the unsaturated monomer. The water-absorbent resin has excellent water absorption characteristics, such as improved dispersion and absorption rate of aqueous fluid, enhanced water retention capacity and dry touch, lower water-soluble component content, and lower residual monomer content. When a water-absorbent resin composition using the water-absorbent resin is used for, for example, a sanitary material, it is possible to improve the absorption rate and water retention capacity, and prevent leakage of fluid from the sanitary material.
摘要翻译：通过将平均粒径为1〜100μm的固体发泡剂在含有不饱和单体和交联剂的单体水溶液中分散，然后使不饱和单体聚合而制造吸水性树脂。吸水性树脂具有优异的吸水性，例如改善水性流体的分散性和吸水率，增加保水能力和干触感，降低水溶性成分含量，降低残留单体含量。当使用吸水性树脂的吸水性树脂组合物用于例如卫生材料时，可以提高吸收速率和保水能力，并且防止流体从卫生材料泄漏。

8. 发明授权

US06225362B1 Microbiological fire-fighting formulation 有权
标题翻译：微生物消防制剂
公开(公告)号：US06225362B1
公开(公告)日：2001-05-01
申请号：US09256010
申请日：1999-02-23
申请人： Charles S. Cox
发明人： Charles S. Cox
IPC分类号： C08J928
CPC分类号： B09C1/10 , A62D1/0071 , A62D3/02 , A62D2101/22
摘要： An improved microbiological fire-fighting foam which comprises a bioremediating component, surfactants, foaming agents, and inorganic nutrients, the bioremediating component consisting substantially of sporulating bacteria which are tolerant of the surfactants used, the surfactants selected being innocuous to the bioremediating component used both when the microbes are in a spore state and when activated, and the selected surfactants further being biodegradable by the microbes of the microbial solution. Alternative embodiments of the invention include formulations which comprise perfumes and/or preservatives in addition to the constituents mentioned above. The improved formulation enables microbiological digestion to inert volatile organic compounds and hydrocarbons which may indeed be ablaze when applied.
摘要翻译：一种改进的微生物灭火泡沫，其包含生物中和组分，表面活性剂，发泡剂和无机营养物质，所述生物中和组分基本上由耐受所用表面活性剂的芽孢细菌组成，所选择的表面活性剂对生物中和组分无害，微生物处于孢子状态并且当被活化时，所选择的表面活性剂进一步由微生物溶液的微生物生物降解。除了上述成分之外，本发明的替代实施方案包括包含香料和/或防腐剂的制剂。改进的配方使微生物消化成惰性挥发性有机化合物和碳氢化合物，当应用时可能会发生燃烧。

9. 发明授权

US06806299B2 Preparation of hydrophobic organic aeorgels 失效
标题翻译：疏水性有机物的制备
公开(公告)号：US06806299B2
公开(公告)日：2004-10-19
申请号：US10132893
申请日：2002-04-24
申请人： Theodore F. Baumann , Joe H. Satcher, Jr. , Alexander E. Gash
发明人： Theodore F. Baumann , Joe H. Satcher, Jr. , Alexander E. Gash
IPC分类号： C08J928
CPC分类号： C08J9/28 , C08J2201/05 , C08J2203/08 , C08J2361/02 , Y02P20/544
摘要： Synthetic methods for the preparation of hydrophobic organics aerogels. One method involves the sol-gel polymerization of 1,3-dimethoxybenzene or 1,3,5-trimethoxybenzene with formaldehyde in non-aqueous solvents. Using a procedure analogous to the preparation of resorcinol-formaldehyde (RF) aerogels, this approach generates wet gels that can be dried using either supercritical solvent extraction to generate the new organic aerogels or air dried to produce an xerogel. Other methods involve the sol-gel polymerization of 1,3,5 trihydroxy benzene (phloroglucinol) or 1,3 dihydroxy benzene (resorcinol) and various aldehydes in non-aqueous solvents. These methods use a procedure analogous to the one-step base and two-step base/acid catalyzed polycondensation of phloroglucinol and formaldehyde, but the base catalyst used is triethylamine. These methods can be applied to a variety of other sol-gel precursors and solvent systems. These hydrophobic organics aerogels have numerous application potentials in the field of material absorbers and water-proof insulation.
摘要翻译：制备疏水性有机物气凝胶的合成方法。一种方法涉及1,3-二甲氧基苯或1,3,5-三甲氧基苯与甲醛在非水溶剂中的溶胶 - 凝胶聚合。使用类似于间苯二酚 - 甲醛（RF）气凝胶的制备方法，该方法产生湿凝胶，其可以使用超临界溶剂萃取干燥以产生新的有机气凝胶或空气干燥以产生干凝胶。其他方法涉及在非水溶剂中1,3,5-三羟基苯（间苯三酚）或1,3-二羟基苯（间苯二酚）和各种醛的溶胶 - 凝胶聚合。这些方法使用类似于间苯三酚和甲醛的一步碱和两步碱/酸催化缩聚的方法，但所用的碱催化剂是三乙胺。这些方法可以应用于各种其他溶胶 - 凝胶前体和溶剂体系。这些疏水性有机气凝胶在材料吸收体和防水绝缘领域具有许多应用潜力。

10. 发明授权

US06664305B2 Chromatography material and a process of manufacturing that material 有权
标题翻译：色谱材料和制造该材料的过程
公开(公告)号：US06664305B2
公开(公告)日：2003-12-16
申请号：US10182768
申请日：2002-10-28
申请人： Alois Jungbauer , Rainer Hahn , Ales Podgornik , Milos Barut , Ales Strancar
发明人： Alois Jungbauer , Rainer Hahn , Ales Podgornik , Milos Barut , Ales Strancar
IPC分类号： C08J928
CPC分类号： G01N30/482 , B01D15/361 , B01D15/3804 , B01D15/3809 , B01J20/26 , B01J20/28042 , B01J20/285 , B01J20/3204 , B01J20/321 , B01J20/3212 , B01J20/3219 , B01J20/327 , B01J20/3272 , B01J20/3282 , B01J2220/54 , B01J2220/82
摘要： A process of manufacturing of a chromatography material comprising the steps of (i) reacting a polymerizable at least bifunctional monomer A with a ligand also having a functional group which binds covalently with one of the functional groups of said polymerizable bifunctional monomer A, (ii) to form a compound B comprising at least one polymerizable functional moiety (iii) polymerizing the compound B essentially alone or with the polymerizable monomers in presence of porogenes to obtain a block of porous polymerizate which is self-supporting or (iv) reacting the ligand and a spacer via a covalent bond which is cleavable to form a ligand-spacer conjugate and binding the ligand-spacer conjugate to the surface of a chromatographic support or reacting the ligand-spacer conjugate via a covalent bond to the at least bi-functional monomer A and polymerizing it essentially alone or with the polymerizable monomers in presence of porogenes to obtain a block of porous polymerizate which is self-supporting.
摘要翻译：一种制备色谱材料的方法，包括以下步骤：（i）使可聚合的至少双官能单体A与还具有与所述可聚合双官能单体A的一个官能团共价键合的官能团的配体反应，（ii）以形成包含至少一个可聚合官能部分的化合物B（iii）在致孔剂存在下基本上单独或与可聚合单体聚合化合物B以获得自支撑的多孔聚合物嵌段，或（iv）使配体和通过共价键的间隔物，其可切割以形成配体 - 间隔基缀合物并将配体 - 间隔物缀合物结合到色谱载体的表面或通过共价键与配体 - 间隔物缀合物反应至至少双官能单体A 并在致孔剂存在下基本上单独或与可聚合单体聚合，得到多孔聚合物嵌段，其为自支撑锻炼。

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