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1. 发明申请

US20040181029A1 Oligomeric hydroxy arylether phthalonitiles and synthesis thereof 有权
标题翻译：低聚羟基芳基醚酞腈及其合成
公开(公告)号：US20040181029A1
公开(公告)日：2004-09-16
申请号：US10808266
申请日：2004-03-17
发明人： Teddy M. Keller , Dawn D. Dominguez
IPC分类号： C08G065/38
CPC分类号： G02F1/133615 , C08G65/40 , C08G65/48 , C08G2650/04 , C08G2650/20 , C08L2312/00
摘要： An aromatic ether oligomer or polyaromatic ether comprising the formula: nullOnullArnulln; wherein Ar is an independently selected divalent aromatic radical; formed by reacting a dihydroxyaromatic with a dihaloaromatic; and wherein the reaction is performed in the presence of a copper compound and cesium carbonate. The polyaromatic ether is formed when neither the dihydroxyaromatic nor the dihaloaromatic is present in an excess amount. The aromatic ether oligomer is formed by using an excess of either dihydroxyaromatic or dihaloaromatic. A phthalonitrile monomer comprising the formula: 1 formed by reacting a 3- or 4-nitrophthalonitrile with a hydroxy-terminated aromatic ether oligomer. A thermoset formed by curing the phthalonitrile monomer. Processes for forming all the above.
摘要翻译：芳香醚低聚物或聚芳醚，其包含式：＆Parenopenst; O-Ar＆Parenclosest; n; 其中Ar是独立选择的二价芳族基团; 通过二羟基芳族化合物与二卤代芳族化合物反应形成; 并且其中所述反应在铜化合物和碳酸铯存在下进行。当二羟基芳族化合物和二卤代芳族化合物都不存在时，形成多芳香族醚。芳族醚低聚物通过使用过量的二羟基芳族化合物或二卤代芳族化合物形成。包含下式的邻苯二甲腈单体：通过使3-或4-硝基邻苯二腈与羟基封端的芳族醚低聚物反应形成。通过固化邻苯二甲腈单体形成的热固性材料。用于形成上述所有方法。

2. 发明申请

US20040147712A1 Flexibilized resorcinolic novolak resins and method of making same 失效
标题翻译：柔韧性酚醛清漆树脂及其制备方法
公开(公告)号：US20040147712A1
公开(公告)日：2004-07-29
申请号：US10734521
申请日：2003-12-12
申请人： INDSPEC Chemical Corporation
发明人： Raj B. Durairaj , Mark A. Lawrence
IPC分类号： C08G065/38
CPC分类号： C08G8/08 , C08G8/04 , C08G8/10 , C08G8/22 , C09J161/06 , C09J161/12
摘要： A flexibilized resorcinolic novolak resin is prepared by reacting a phenolic compound, such as resorcinol, with an unsaturated dihydroxy, an unsaturated aldehyde, an aliphatic dialdehyde, or a mixture thereof. An aldehyde (different from the unsaturated aldehyde and the aliphatic dialdehyde) is either simultaneously or subsequently added to the reaction mixture. The flexibilized resorcinolic novolak resin can be used in an adhesive composition for enhancing the adhesion between tire cords and rubber for tire applications.
摘要翻译：通过使酚类化合物（例如间苯二酚）与不饱和二羟基，不饱和醛，脂族二醛或其混合物反应来制备增韧的间苯二酚酚醛清漆树脂。醛（不同于不饱和醛和脂族二醛）同时或随后加入到反应混合物中。可挠曲的间苯二酚酚醛清漆树脂可用于增强轮胎帘线和用于轮胎应用的橡胶之间的粘合性的粘合剂组合物中。

3. 发明申请

US20030060590A1 Compositions and methods for thermosetting molecules in organic compositions 失效
公开(公告)号：US20030060590A1
公开(公告)日：2003-03-27
申请号：US10176335
申请日：2002-06-19
申请人： Honeywell International Inc.
发明人： Kreisler S. Lau , Feng Quan Liu , Boris A. Korolev , Emma Brouk , Ruslan Zherebin , David Nalewajek
IPC分类号： C08G065/30 , C08G065/38 , C08F008/00
CPC分类号： C08G61/02 , C08G61/12 , C08G65/40 , C08G2650/60
摘要： In a method of producing a low dielectric constant polymer, a thermosetting monomer is provided, wherein the thermosetting monomer has a cage compound or aryl core structure, and a plurality of arms that are covalently bound to the cage compound or core structure. In a subsequent step, the thermosetting monomer is incorporated into a polymer to form the low dielectric constant polymer, wherein the incorporation into the polymer comprises a chemical reaction of a triple bond that is located in at least one of the arms. Contemplated cage compounds and core structures include adamantane, diamantane, silicon, a phenyl group and a sexiphenylene group, while preferred arms include an arylene, a branched arylene, and an arylene ether. The thermosetting monomers may advantageously be employed to produce low-k dielectric material in electronic devices, and the dielectric constant of the polymer can be controlled by varying the overall length of the arms.

4. 发明申请

US20020077447A1 Curable polyphenylene ether resin, composition made therefrom, and process for preparing the resin 有权
标题翻译：可固化聚苯醚树脂，由其制成的组合物和制备树脂的方法
公开(公告)号：US20020077447A1
公开(公告)日：2002-06-20
申请号：US09848524
申请日：2001-05-03
申请人： Industrial Technology Research Institute
发明人： Gue-Wuu Hwang , Chien-Ting Lin , Chingchen S. Chiu
IPC分类号： C08G065/38 , C08G065/40
CPC分类号： C08G65/485 , C08L71/126 , H05K1/0326 , Y10T428/31547 , Y10T428/31551 , C08L2666/04
摘要： The present invention provides a curable polyphenylene ether (PPE) resin, a composition made therefrom, and a process for preparing the resin. The process involves introducing a vinyl group-containing functional group to the terminal end of PPE by modifying the hydroxy and ester groups on the terminal end. Thus, a curable thermosetting PPE resin including a vinyl group on the terminal end can be obtained. Since the dehydrogenation of side chain methyl using n-BuLi is not conducted in the process of the present invention, the process is much easier, and the cost can be decreased.
摘要翻译：本发明提供一种可固化聚苯醚（PPE）树脂，由其制成的组合物及其制备方法。该方法包括通过改变末端的羟基和酯基将含乙烯基的官能团引入PPE的末端。因此，可以得到在末端具有乙烯基的可固化的热固性PPE树脂。由于在本发明的方法中不进行使用n-BuLi的侧链甲基的脱氢，所以该方法容易得多，成本降低。

5. 发明申请

US20040158024A1 Low dielectric constant materials and methods of preparation thereof 有权
标题翻译：低介电常数材料及其制备方法
公开(公告)号：US20040158024A1
公开(公告)日：2004-08-12
申请号：US10466651
申请日：2004-03-11
发明人： Kreisler Lau , Feng Quan Liu , Paul Apen , Boris Korolev , Emma Brouk , Ruslan Zherebin , David Nalewajek , Roger Leung
IPC分类号： H01L021/31 , C08G065/38
CPC分类号： C08G61/12 , C07C13/615 , C07C13/64 , C07C15/54 , C07C17/10 , C07C17/269 , C07C2603/74 , C07C2603/90 , C07F7/0805 , C08F238/00 , C08G61/02 , H01L2924/0002 , C07C23/46 , C07C25/22 , H01L2924/00
摘要： The present invention is directed to low dielectric polymers and to methods of producing these low dielectric constant polymers, dielectric materials and layers, and electronic components. In one aspect of the present invention, an isomeric mixture of thermosetting monomers, wherein the monomers have a core structure and a plurality of arms, is provided, and the isomeric mixture of thermosetting monomers is polymerized, wherein polymerization comprises a reaction of an ethynyl group that is located in at least one arm of a monomer. In yet another aspect of the inventive subject matter, spin-on low dielectric constant materials are formed having a first backbone with an aromatic moiety and a first reactive group, and a second backbone with an aromatic moiety and a second reactive group, wherein the first and second backbone are crosslinked via the first and second reactive groups in a crosslinking reaction preferably without an additional crosslinker, and wherein a cage structure having at least eight (8) atoms is covalently bound to at least one of the first and second backbone.
摘要翻译：本发明涉及低介电聚合物以及生产这些低介电常数聚合物，介电材料和层以及电子元件的方法。在本发明的一个方面，提供其中单体具有核心结构和多个臂的热固性单体的异构体混合物，并且热固性单体的异构体混合物聚合，其中聚合包括乙炔基其位于单体的至少一个臂中。在本发明主题的另一方面，形成旋涂低介电常数材料，其具有具有芳族部分和第一反应性基团的第一主链和具有芳族部分和第二反应性基团的第二主链，其中第一并且第二主链在交联反应中通过第一和第二反应性基团交联，优选不含另外的交联剂，并且其中具有至少八个（8）原子的笼结构共价结合至第一和第二主链中的至少一个。

6. 发明申请

US20020055608A1 Process for the manufacture of low molecular weight polyphenylene ether resins 有权
公开(公告)号：US20020055608A1
公开(公告)日：2002-05-09
申请号：US09943575
申请日：2001-08-30
发明人： Adrianus J.F.M. Braat , Hugo Ingelbrecht , Ruud Trion
IPC分类号： C08G065/38 , C08G065/44
CPC分类号： C08G65/44 , C08G65/46
摘要： The invention relates to a novel process for the manufacture of very low molecular weight polyphenylene ether resin, typically within the intrinsic viscosity range of about 0.08 dl/g to about 0.16 dl/g as measured in chloroform at 25null C. The method preferably comprises 2,6-dimethylphenol as a monovalent phenol species. The invention also relates to the polyphenylene ether resin made by the process as well as blends and articles containing the polyphenylene ether resin made by the process.

7. 发明申请

US20020042494A1 Process for the manufacture of low molecular weight polyphenylene ether resins through redistribution 失效
公开(公告)号：US20020042494A1
公开(公告)日：2002-04-11
申请号：US09943122
申请日：2001-08-30
发明人： Adrianus J.F.M. Braat , Hugo G.E. Engelbrecht , Juraj Liska
IPC分类号： C08G065/38 , C08G065/44 , C08G065/46
CPC分类号： C08G65/44
摘要： The invention relates to a novel process for the manufacture of functionalized polyphenylene ether resins through redistribution with a functionalized phenolic compound in the polyphenylene ether resin polymerization reaction solution without the addition of an added redistribution catalyst or promoter. The invention also relates to the functionalized polyphenylene ether resin made by the process as well as blends and articles containing the functionalized polyphenylene ether resin made by the process.

8. 发明申请

US20020010314A1 Production process of polyphenylene ether 有权
标题翻译：聚苯醚的生产工艺
公开(公告)号：US20020010314A1
公开(公告)日：2002-01-24
申请号：US09883388
申请日：2001-06-19
发明人： Akira Mitsui , Yuji Takeda
IPC分类号： C08G065/44 , C08G065/38 , C08F006/08
CPC分类号： C08G65/44
摘要： A process for producing a polyphenylene ether by oxidative polymerization of a phenol compound using a catalyst and an oxygen-containing gas, wherein the catalyst comprises a copper compound, a bromine compound, a diamine compound represented by the following formula (1): 1 (wherein, R1, R2, R3 and R4 each independently represents hydrogen or a C1-6 linear or branched alkyl group with the proviso that all of them do not represent hydrogen simultaneously, and R5 represents a linear or methyl-branched C2-5 alkylene group), a tertiary monoamine compound and a secondary monoamine compound, wherein the process comprises the steps of: controlling an absolute pressure at a gaseous phase of a reaction vessel to a range of from 0.098 MPa to less than 0.392 MPa; and feeding the oxygen-containing gas to the reaction vessel, the oxygen-containing gas having an oxygen partial pressure, in terms of an absolute pressure, of from 0.0147 MPa to 0.0883 MPa.
摘要翻译： 1.一种通过使用催化剂和含氧气体的酚化合物的氧化聚合制备聚苯醚的方法，其中所述催化剂包含铜化合物，溴化合物，由下式（1）表示的二胺化合物：（其中，R 1，R 2，R 3和R 4各自独立地表示氢或C 1-6直链或支链烷基，条件是它们全部不同时代表氢，R5表示直链或支链的C 2-5亚烷基）叔胺化合物和仲单胺化合物，其中该方法包括以下步骤：将反应容器气相的绝对压力控制在0.098MPa至小于0.392MPa的范围内; 并将含氧气体供给到反应容器中，具有0.0147MPa〜0.0883MPa的氧分压为绝对压力的含氧气体。

9. 发明申请

US20010000520A1 Process for the manufacture of low molecular weight polyphenylene ether resins 失效
标题翻译：制备低分子量聚苯醚树脂的方法
公开(公告)号：US20010000520A1
公开(公告)日：2001-04-26
申请号：US09735990
申请日：2000-12-13
申请人： General Electric Co.
发明人： Adrianus J.F.M. Braat , Hugo Ingelbrecht , Ruud Trion
IPC分类号： C08G065/38 , C08G065/44 , C07C041/09 , C07C041/00
CPC分类号： C08G65/44 , C08G65/46
摘要： The invention relates to a novel process for the manufacture of very low molecular weight polyphenylene ether resin, typically within the intrinsic viscosity range of about 0.08 dl/g to about 0.16 dl/g as measured in chloroform at 25null C. The method preferably comprises 2,6-dimethylphenol as a monovalent phenol species. The invention also relates to the polyphenylene ether resin made by the process as well as blends and articles containing the polyphenylene ether resin made by the process.
摘要翻译：本发明涉及一种用于制造极低分子量聚苯醚树脂的新方法，通常在25℃下在氯仿中测得的特性粘度范围为约0.08dl / g至约0.16dl / g。该方法优选包含 2,6-二甲基苯酚作为一价酚类物质。本发明还涉及通过该方法制备的聚苯醚树脂以及含有通过该方法制备的聚苯醚树脂的共混物和制品。

10. 发明申请

US20040249109A1 Polyphenylene ether resin composition 有权
标题翻译：聚苯醚树脂组合物
公开(公告)号：US20040249109A1
公开(公告)日：2004-12-09
申请号：US10491490
申请日：2004-04-01
发明人： Akira Mitsui , Mutsumi Maeda
IPC分类号： C08G065/38
CPC分类号： C08L71/123 , C08G65/46
摘要： A polyphenylene ether resin composition comprising a polyphenylene ether, wherein the polyphenylene ether has a polymer chain comprising recurring units each represented by the following formula (1): 1 and has the following characteristics (a), (b) and (c): (a) when the polyphenylene ether is analyzed by 1H-NMR, the polyphenylene ether exhibits a triplet signal (S1) at 3.55 ppm, wherein the triplet signal (S1) has a relative intensity of 0.05 to 0.25 in terms of the percentage of the integrated intensity of the triplet signal (S1), based on the integrated intensity of a signal (S2) observed at 6.47 ppm; (b) the polyphenylene ether exhibits an absorbance of from 0.01 to 0.40 at a wavelength of 480 nm; and (c) the polyphenylene ether has a weight average molecular weight of from 30,000 to 100,000.
摘要翻译：一种聚苯醚树脂组合物，其包含聚苯醚，其中所述聚苯醚具有包含由下式（1）表示的重复单元的聚合物链：并具有以下特征（a），（b）和（c）：（a ）当通过1 H-NMR分析聚苯醚时，聚苯醚在3.55ppm处显示出三重态信号（S1），其中三重态信号（S1）的相对强度为0.05-0.25的相对强度基于在6.47ppm处观察到的信号（S2）的积分强度，三重态信号（S1）的积分强度; （b）聚苯醚在波长480nm处的吸光度为0.01〜0.40; 和（c）聚苯醚的重均分子量为30,000〜100,000。

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