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1. 发明专利

ES2032026T3 未知
公开(公告)号：ES2032026T3
公开(公告)日：1993-01-01
申请号：ES88312261
申请日：1988-12-22
申请人： INDSPEC CHEMICAL CORPORATION (A DELAWARE CORPORATION)
发明人： WU, CHING-YONG
IPC分类号： B01J27/12 , B01J27/128 , B01J27/135 , C07B61/00 , C07C27/00 , C07C37/08 , C07C39/08 , C07C45/53 , C07C67/00 , C07C409/12
摘要： In a process for the preparation of resorcinol, an extract of selected oxidation products of diisopropylbenzene is contacted with hydrogen peroxide to convert m-HHP to m-DHP, the extract so treated is dried and thereafter, the m-DHP present is decomposed in the presence of an effective amount, preferably with the range of from 10 to 50 ppm, of a catalyst selected from boron trifluoride, ferric chloride and stannic chloride.

2. 发明申请

US20040162391A1 Modified resorcinol resins and applications thereof 失效
标题翻译：改性间苯二酚树脂及其应用
公开(公告)号：US20040162391A1
公开(公告)日：2004-08-19
申请号：US10368753
申请日：2003-02-18
申请人： INDSPEC Chemical Corporation
发明人： Raj Durairaj , Mark A. Lawrence
IPC分类号： C08L061/00
CPC分类号： C08G8/22 , C08G8/30
摘要： A modified resorcinol resin is prepared by reacting a phenolic compound (e.g., resorcinol) with an olefinically unsaturated compound (e.g., styrene) and two types of aldehyde: a formaldehyde and an alkyl aldehyde (e.g., butyraldehyde). The reaction is typically carried out in the presence of an acid catalyst. The resulting resin has a lower softening point and can be used as a methylene acceptor compound in a vulcanizable rubber composition.
摘要翻译：通过使酚类化合物（例如间苯二酚）与烯属不饱和化合物（例如苯乙烯）和两种醛：甲醛和烷基醛（例如丁醛）反应来制备改性间苯二酚树脂。反应通常在酸催化剂存在下进行。所得树脂具有较低的软化点，可用作可硫化橡胶组合物中的亚甲基受体化合物。

3. 发明申请

US20040241331A1 Silane-modified phenolic resins and applications thereof 失效
标题翻译：硅烷改性酚醛树脂及其应用
公开(公告)号：US20040241331A1
公开(公告)日：2004-12-02
申请号：US10446968
申请日：2003-05-28
申请人： INDSPEC Chemical Corporation
发明人： Raj B. Durairaj , C. Michael Walkup , Mark A. Lawrence
IPC分类号： B05D003/02
CPC分类号： C08L61/06 , C08L61/12 , C08L61/14
摘要： A silane-modified phenolic resin is prepared by reacting a phenolic compound (e.g., resorcinol) with an aldehyde to produce a phenolic novolak resin. The phenolic novolak resin is further reacted with at least one silane compound to produce the silane-modified phenolic resin. The reaction is typically carried out in the presence of an acid or base catalyst. The resulting resin has a lower softening point and can be used as a methylene acceptor compound in a vulcanizable rubber composition.
摘要翻译：通过使酚类化合物（例如间苯二酚）与醛反应以制备酚醛清漆树脂来制备硅烷改性酚醛树脂。酚醛清漆树脂进一步与至少一种硅烷化合物反应以制备硅烷改性酚醛树脂。反应通常在酸或碱催化剂的存在下进行。所得树脂具有较低的软化点，可用作可硫化橡胶组合物中的亚甲基受体化合物。

4. 发明申请

US20040147712A1 Flexibilized resorcinolic novolak resins and method of making same 失效
标题翻译：柔韧性酚醛清漆树脂及其制备方法
公开(公告)号：US20040147712A1
公开(公告)日：2004-07-29
申请号：US10734521
申请日：2003-12-12
申请人： INDSPEC Chemical Corporation
发明人： Raj B. Durairaj , Mark A. Lawrence
IPC分类号： C08G065/38
CPC分类号： C08G8/08 , C08G8/04 , C08G8/10 , C08G8/22 , C09J161/06 , C09J161/12
摘要： A flexibilized resorcinolic novolak resin is prepared by reacting a phenolic compound, such as resorcinol, with an unsaturated dihydroxy, an unsaturated aldehyde, an aliphatic dialdehyde, or a mixture thereof. An aldehyde (different from the unsaturated aldehyde and the aliphatic dialdehyde) is either simultaneously or subsequently added to the reaction mixture. The flexibilized resorcinolic novolak resin can be used in an adhesive composition for enhancing the adhesion between tire cords and rubber for tire applications.
摘要翻译：通过使酚类化合物（例如间苯二酚）与不饱和二羟基，不饱和醛，脂族二醛或其混合物反应来制备增韧的间苯二酚酚醛清漆树脂。醛（不同于不饱和醛和脂族二醛）同时或随后加入到反应混合物中。可挠曲的间苯二酚酚醛清漆树脂可用于增强轮胎帘线和用于轮胎应用的橡胶之间的粘合性的粘合剂组合物中。

5. 发明申请

US20040116592A1 Phenolic modified resorcinolic resins for rubber compounding 有权
标题翻译：酚醛改性酚醛树脂用于橡胶配混
公开(公告)号：US20040116592A1
公开(公告)日：2004-06-17
申请号：US10369366
申请日：2003-02-18
申请人： INDSPEC Chemical Corporation
发明人： Raj Durairaj , C. Michael Walkup , Mark A. Lawrence
IPC分类号： C08K003/04
CPC分类号： C08L61/06 , C08L7/00 , C08L21/00 , C08L61/12 , C08L2666/16 , C08L2666/04
摘要： A vulcanizable rubber composition comprises (a) a rubber component; (b) a methylene donor compound; and (c) a methylene acceptor comprising a blend of a high ortho-ortho bonded phenolic novolak resin and a resorcinolic resin. The resin blend can be made by a number of methods. For example, it can be prepared by first reacting one or more phenolic compounds represented by the following formula: 1 where R is selected from the group consisting of H, an alkyl group chain of 1-16 carbon atoms and an aralkyl group of 8-12 carbon atoms with an aldehyde in the presence of an ortho directing catalyst and then combining a resorcinol-formaldehyde novolak resin to obtain a phenolic and resorcinolic novolak resin blend.
摘要翻译：可硫化橡胶组合物包含（a）橡胶组分; （b）亚甲基给体化合物; 和（c）亚甲基受体，其包含高邻位键合酚醛清漆树脂和间苯二酚树脂的共混物。树脂混合物可以通过多种方法制备。例如，可以通过首先使一种或多种由下式表示的酚类化合物反应来制备：其中R选自H，1-16个碳原子的烷基链和8-12个芳烷基碳原子与邻位导向催化剂存在下的醛，然后将间苯二酚 - 甲醛酚醛清漆树脂混合，得到酚醛树脂和间苯二酚酚醛清漆树脂共混物。

6. 发明申请

WO2006036880A2 PHOSPHATE ESTER FLAME RETRADANTS FROM RESORCINOL-KETONE REACTION PRODUCTS 审中-公开
标题翻译：来自间苯二酚酮酮反应产物的磷酸酯火焰回收剂
公开(公告)号：WO2006036880A2
公开(公告)日：2006-04-06
申请号：PCT/US2005/034391
申请日：2005-09-21
申请人： INDSPEC CHEMICAL CORPORATION , DURAIRAJ, Raj, B. , JESIONOWSKI, Gary, A.
发明人： DURAIRAJ, Raj, B. , JESIONOWSKI, Gary, A.
IPC分类号： C08K5/49
CPC分类号： C07F9/65522 , C08K5/529
摘要： Flavan-based and spirodichroman compound-based phosphate esters prepared by reacting flavans and spirodichroman compounds with phosphorus oxychloride, monophenyl dichlorophosphate, or diphenyl chlorophosphate compounds are described. The flavans and spirodichroman compounds can be synthesized by the reaction of resorcinol with aliphatic acetone. Such phosphate esters can be used as flame retardants.
摘要翻译：描述了通过使黄烷和螺二氢二苯并吡喃化合物与三氯氧化磷，单苯基二氯磷酸酯或二苯基氯磷酸酯化合物反应制备的基于黄烷和螺二氢噻吩类化合物的磷酸酯。黄烷和spirodichroman化合物可以通过间苯二酚与脂族丙酮的反应合成。这种磷酸酯可以用作阻燃剂。

7. 发明申请

WO2004106427A1 SILANE-MODIFIED PHENOLIC RESINS AND APPLICATIONS THEREOF 审中-公开
标题翻译：硅烷改性酚醛树脂及其应用
公开(公告)号：WO2004106427A1
公开(公告)日：2004-12-09
申请号：PCT/US2004/012976
申请日：2004-04-28
申请人： INDSPEC CHEMICAL CORPORATION , DURAIRAJ, Raj B. , WALKUP, C. Michael , LAWRENCE, Mark A.
发明人： DURAIRAJ, Raj B. , WALKUP, C. Michael , LAWRENCE, Mark A.
IPC分类号： C08K9/06
CPC分类号： C08L61/06 , C08L61/12 , C08L61/14
摘要： A silane-modified phenolic resin is prepared by reacting a phenolic compound (e.g., resorcinol) with an aldehyde to produce a phenolic novolak resin. The phenolic novolak resin is further reacted with at least one silane compound to produce the silane-modified phenolic resin. The reaction is typically carried out in the presence of an acid or base catalyst. The resulting resin has a lower softening point and can be used as a methylene acceptor compound in a vulcanizable rubber composition.
摘要翻译：通过使酚类化合物（例如间苯二酚）与醛反应以制备酚醛清漆树脂来制备硅烷改性酚醛树脂。酚醛清漆树脂进一步与至少一种硅烷化合物反应以制备硅烷改性酚醛树脂。反应通常在酸或碱催化剂的存在下进行。所得树脂具有较低的软化点，可用作可硫化橡胶组合物中的亚甲基受体化合物。

8. 发明申请

WO1994015986A2 SUBSTITUTED RESORCINOL-BASED EPOXY RESINS 审中-公开
标题翻译：取代的基于RESORCINOL的环氧树脂
公开(公告)号：WO1994015986A2
公开(公告)日：1994-07-21
申请号：PCT/US1994000556
申请日：1994-01-18
申请人： INDSPEC CHEMICAL CORPORATION , DURAIRAJ, Raj, B. , TACKIE, Michael, N.
发明人： INDSPEC CHEMICAL CORPORATION
IPC分类号： C08G59/24
CPC分类号： C07D303/24 , C08G59/245 , C08G59/3218
摘要： A curable substituted resorcinol-based epoxy resin was developed having structural formula (I), wherein at least one of R1, R2 or R3 is selected from the group consisting of (a) hydrogen, (b) halogen, (c) a saturated hydrocarbon having 1 to 10 carbon atoms, (d) an unsaturated hydrocarbon having 1 to about 10 carbon atoms, (e) an aralkyl group, and (f) a benzoyl group. The aralkyl group has structure (II), wherein at least one of R4, R5 or R6 is selected from the group consisting of (a) hydrogen, (b) an alkyl group having 1 to about 4 carbon atoms and (c) halogen. The benzoyl group has structure (III), wherein R7 is selected from the group consisting of hydrogen, halogen and an alkyl group having 1 to 4 carbon atoms. Another curable substituted resorcinol-based epoxy resin was developed having general structural formula (IV), wherein at least one of R8, R9, R10 or R11 is selected from the group consisting of hydrogen, halogens and alkyl groups having 1 to about 10 carbon atoms. To minimize potential toxicity, the above derivatized resorcinol epoxies were synthesized, along with a series of thermoplastic tougheners. The physical and mechanical properties of the neat resins and of the toughened resins are presented in this patent.
摘要翻译：开发了具有结构式（I）的可固化取代的间苯二酚基环氧树脂，其中R 1，R 2或R 3中的至少一个选自（a）氢，（b）卤素，（c）饱和烃具有1至10个碳原子，（d）具有1至约10个碳原子的不饱和烃，（e）芳烷基和（f）苯甲酰基。芳烷基具有结构（II），其中R 4，R 5或R 6中的至少一个选自（a）氢，（b）具有1至约4个碳原子的烷基和（c）卤素。苯甲酰基具有结构（III），其中R 7选自氢，卤素和具有1至4个碳原子的烷基。开发了另一种可固化取代的间苯二酚基环氧树脂，其具有通式结构式（Ⅳ），其中R 8，R 9，R 10或R 11中的至少一个选自氢，卤素和具有1至约10个碳原子的烷基。为了最小化潜在的毒性，上述衍生的间苯二酚环氧化物与一系列热塑性增韧剂一起被合成。纯树脂和增韧树脂的物理和机械性能在本专利中提出。

9. 发明申请

WO2007106186A3 RESORCINOL RESIN-BLOCKED ISOCYANATES AND THEIR APPLICATIONS 审中-公开
公开(公告)号：WO2007106186A3
公开(公告)日：2007-09-20
申请号：PCT/US2006/061353
申请日：2006-11-29
申请人： INDSPEC CHEMICAL CORPORATION , DURAIRAJ, Raj, B. , JESIONOWSKI, Gary, A. , LAWRENCE, Mark, A.
发明人： DURAIRAJ, Raj, B. , JESIONOWSKI, Gary, A. , LAWRENCE, Mark, A.
IPC分类号： C08G18/54 , C08G8/28 , C09D161/12 , C09D175/16
摘要： Resorcinol resin-blocked isocyanate compositions are derived from the reaction between a resorcinol resin and at least two different isocyanate compounds. The resorcinol resin-blocked isocyanate compositions may have two or more unblocking temperatures and/or melting characteristics that may provide some unique properties, such as improved adhesion of reinforcing materials to rubber compounds. The resorcinol resin-blocked isocyanate compositions can be used in fabric dipping formulations and/or rubber compositions with improved properties.

10. 发明申请

WO2007005086A1 PROCESS FOR MAKING PHENYLENE DIOXYDIACETIC ACID AND USE THEREOF 审中-公开
标题翻译：制备苯乙烯二酸的方法及其用途
公开(公告)号：WO2007005086A1
公开(公告)日：2007-01-11
申请号：PCT/US2006/013768
申请日：2006-04-13
申请人： INDSPEC CHEMICAL CORPORATION , DURAIRAJ, Raj, B. , TACKIE, Michael, N.
发明人： DURAIRAJ, Raj, B. , TACKIE, Michael, N.
IPC分类号： C08G63/78 , C08G63/672 , C07C51/367 , C07C59/70
CPC分类号： C08G63/672 , C07C51/367 , C07C59/70
摘要： A process for making phenylene dioxydiacetic acid comprises (a) contacting a dihydroxybenzene under reaction conditions with a salt of haloacetic acid in a solution without adding a haloacetic acid to produce a salt of phenylene dioxydiacetic acid; and (b) optionally converting the salt of phenylene dioxydiacetic acid to free phenylene dioxydiacetic acid. In some embodiments, 1,3-phenylene dioxydiacetic acid (RDOA) is made by reacting resorcinol with sodium chloroacetic acid in a reaction mixture with a pH in the range of about 7 to about 11 and at a temperature from about 70 °C to 105 °C. By adjusting the reactions conditions, a relatively high yield of 1,3-phenylene dioxydiacetic acid (i.e., greater than 80%) is obtained. The purified acid can be used in the synthesis of polyester, such as polyethylene terephthalate.
摘要翻译：制备亚苯基二氧基二乙酸的方法包括（a）在反应条件下使二羟基苯与卤代乙酸盐在溶液中接触而不添加卤代乙酸以产生亚苯基二氧二肟酸的盐; 和（b）任选将亚苯基二氧代二乙酸的盐转化为游离的亚苯基二氧基二乙酸。在一些实施方案中，1,3-亚苯基二氧二氢乙酸（RDOA）是通过使间苯二酚与氯乙酸钠在反应混合物中反应制备的，反应混合物的pH为约7至约11，温度为约70℃至105℃ C。通过调整反应条件，可以获得相当高的1,3-亚苯基二氧二氢乙酸的收率（即大于80％）。纯化的酸可用于合成聚酯，如聚对苯二甲酸乙二醇酯。

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