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1. 发明授权

US06281350B1 Methods for the reduction of bleeding of lignosulfonates from lignosulfonate-treated substrates 失效
标题翻译：从木质素磺酸盐处理的底物中减少木素磺酸盐出血的方法
公开(公告)号：US06281350B1
公开(公告)日：2001-08-28
申请号：US09466164
申请日：1999-12-17
申请人： Blair Alex Owens , Dimitris Ioannis Collias , Andrew Julian Wnuk
发明人： Blair Alex Owens , Dimitris Ioannis Collias , Andrew Julian Wnuk
IPC分类号： C08B100
CPC分类号： C08H6/00 , C08G73/02 , C08G73/022 , C08G73/0226 , C08G73/0286 , C08G73/0293 , D21H17/23 , D21H17/56 , Y10T428/31993
摘要： The bleeding of lignosulfonates from lignosulfonate-treated substrates when contacted under humid conditions is reduced by rendering the lignosulfonates water-insoluble via reacting them with an amine polymer-epichlorohydrin adduct containing at least one quaternary ammonium group under acidic conditions.
摘要翻译：在酸性条件下，通过使木质素磺酸盐与含有至少一个季铵基团的胺聚合物 - 表氯醇加合物反应，使得木质素磺酸盐不溶于水，从而降低了木质素磺酸盐处理的底物在潮湿条件下接触时的渗出。

2. 发明授权

US06197950B1 Cationized hydroxyalkylcellulose and process for producing the same 有权
标题翻译：阳离子羟烷基纤维素及其制备方法
公开(公告)号：US06197950B1
公开(公告)日：2001-03-06
申请号：US09246247
申请日：1999-02-08
申请人： Hiroyuki Nakamura , Shigenobu Sato
发明人： Hiroyuki Nakamura , Shigenobu Sato
IPC分类号： C08B100
CPC分类号： A61Q5/02 , A61K8/731 , A61K2800/5426 , C08B11/145 , C08B11/193 , C08B11/20
摘要： Cationized hydroxyalkylcelluloses, which are highly compatible with surfactants, are represented by the following formula (I): wherein R1, R2 and R3 represent a hydrogen atom or a group represented by the formula CH2CH2OCH2CH (OH) CH2N+(CH3)Cl−, etc.; and “n” is a number of from 50 to 2,000; which have a mobility distribution (&Dgr;U) determined by electrophoresis ranging from 0.1×105 to 2.0×105 cm2/sec·V.
摘要翻译：与表面活性剂高度相容的阳离子羟烷基纤维素由下式（I）表示：其中R1，R2和R3表示氢原子或由式CH2CH2OCH2CH（OH）CH2N +（CH3）Cl-等表示的基团等。 ; “n”为50〜2000的数; 其具有由0.1×10 5至2.0×10 5 cm 2 / sec.V的电泳测定的迁移率分布（DELTAU）。

3. 再颁专利

USRE38484E1 Cationized hydroxyalkylcellulose and process for producing the same 失效
标题翻译：阳离子羟烷基纤维素及其制备方法
公开(公告)号：USRE38484E1
公开(公告)日：2004-03-30
申请号：US10120341
申请日：2002-04-11
申请人： Hiroyuki Nakamura , Shigenobu Sato
发明人： Hiroyuki Nakamura , Shigenobu Sato
IPC分类号： C08B100
CPC分类号： C08B11/20 , A61K8/731 , A61K2800/5426 , A61Q5/02 , C08B11/193
摘要： Cationized hydroxyalkylcelluloses, which are highly compatible with surfactants, are represented by the following formula (I): wherein R1, R2 and R3 represent a hydrogen atom or a group represented by the formula CH2CH2OCH2CH (OH) CH2N+(CH3)Cl−, etc.; and “n” is a number of from 50 to 2,000; which have a mobility distribution (&Dgr;U) determined by electrophoresis ranging from 0.1×105 10−5 to 2.0×105 10−5 cm2sec·V.

4. 发明授权

US06548659B1 Process for ammoniating cellulosic materials 有权
标题翻译：氨化纤维素材料的工艺
公开(公告)号：US06548659B1
公开(公告)日：2003-04-15
申请号：US09823206
申请日：2001-03-30
申请人： Gary Breitenbeck , Keith Kember
发明人： Gary Breitenbeck , Keith Kember
IPC分类号： C08B100
CPC分类号： C08H8/00 , C08B1/00 , C08B15/06 , C08L1/02 , C08L97/02 , Y10S426/807
摘要： Process for enriching the organic nitrogen content of commercial scale quantities of cellulosic materials which includes the steps of: a) placing substantially dry or unwetted cellulosic material in a pressurizable reactor; b) injecting an ammonia or ammonia-forming nitrogen solution into the reactor until the cellulosic material is approximately submerged; c) setting the temperature in the reactor to maintain a liquid temperature between about 80 and 200° C.; d) pressurizing the reactor to at least 750 psi; e) maintaining the temperature and pressure in the reactor for a period of time sufficient for the organically bound nitrogen content of the cellulosic material to exceed about 1.5%; and f) drying the cellulosic material to a moisture content sufficiently low to arrest microbial activity.
摘要翻译：用于富集商业规模量的纤维素材料的有机氮含量的方法，其包括以下步骤：a）将基本上干燥或未净化的纤维素材料放置在可加压的反应器中; b）将氨或形成氨的氮溶液注入反应器，直到纤维素材料近似浸没; c）设置反应器中的温度以保持液体温度在约80和200℃之间; d）将反应器加压至至少750psi; e）将反应器中的温度和压力维持足以使纤维素材料的有机结合的氮含量超过约1.5％的时间; 和f）将纤维素材料干燥至足够低的水分含量以阻止微生物活性。

5. 发明授权

US06821531B2 Powdered/microfibrillated cellulose 失效
标题翻译：粉末/微纤维素纤维素
公开(公告)号：US06821531B2
公开(公告)日：2004-11-23
申请号：US09946658
申请日：2001-09-05
申请人： Vijay Kumar
发明人： Vijay Kumar
IPC分类号： C08B100
CPC分类号： A61K47/38 , A61K9/0014 , A61K9/1652 , A61K9/2054 , C08B15/02
摘要： A new cellulose excipient suitable for use as a binder, filler, and/or disintegrant in the development of solid dosage forms and as a bodying agent or a drug carrier in the preparation of topical formulations is described. The cellulose excipient is formed by soaking a source of cellulose in an aqueous alkali metal hydroxide solution. The cellulose is then regenerated, washed, and optionally hydrolyzed with a dilute mineral acid. The cellulose excipient is also useful as an aqueous dispersion in topical formulations and in the manufacture of cellulose beads.
摘要翻译：描述了适用于在制备固体剂型中作为粘合剂，填充剂和/或崩解剂的新型纤维素赋形剂以及作为局部制剂制剂中的保护剂或药物载体。通过将纤维素源浸入碱金属氢氧化物水溶液中形成纤维素赋形剂。然后将纤维素再生，洗涤并任选地用稀无机酸水解。纤维素赋形剂也可用作局部制剂中的水性分散体和纤维素珠的制造。

6. 发明授权

US06677447B1 Process for preparing homogeneous cellulose solution by using supercooled liquid N-methylmorpholine-N-oxide hydrate solvent 失效
标题翻译：使用过冷液体N-甲基吗啉-N-氧化物水合物溶剂制备均匀纤维素溶液的方法
公开(公告)号：US06677447B1
公开(公告)日：2004-01-13
申请号：US09706846
申请日：2000-11-07
申请人： Wha Seop Lee , Seong Mu Jo , Seok Gu Ko , Dong Bok Kim
发明人： Wha Seop Lee , Seong Mu Jo , Seok Gu Ko , Dong Bok Kim
IPC分类号： C08B100
CPC分类号： C08L1/02 , C08B1/003
摘要： Disclosed is a process for preparing a homogeneous cellulose solution which is capable of, forming a mixture where a cellulose pulp powder is mixed and swollen with a liquid NMMO hydrate solvent supercooled under a melting point and subjecting the mixture to a dissolution treatment, thereby producing a homogeneous cellulose solution having a substantially low decomposition characteristic. The process produces a cellulose pulp mixing powder that is first swollen in a liquid NMMO solvent supercooled under a melting point by minimizing the dissolution of cellulose by the liquid NMMO solvent and maximizing the swelling thereof by the liquid NMMO solvent, thereby resulting in a maximum homogeneity of the solution and maintains the minimized decomposition states of the cellulose and the NMMO solvent, thereby resulting in the improvement of productivity and the simplicity of the process.
摘要翻译：公开了一种制备均匀纤维素溶液的方法，该方法能够形成混合物，其中纤维素纸浆粉末与在熔点过冷的液体NMMO水合物溶剂混合并溶胀，并使混合物进行溶解处理，从而产生均匀的纤维素溶液具有基本上低的分解特性。该方法产生纤维素浆混合粉末，其首先在熔点过冷的液体NMMO溶剂中溶胀，通过使液体NMMO溶剂使纤维素溶解最小化，并通过液体NMMO溶剂使其溶胀最大化，从而产生最大的均匀性的溶液，并维持纤维素和NMMO溶剂的最小分解状态，从而导致生产率的提高和方法的简单性。

7. 发明授权

US06600034B2 Method of producing cellulose polymers 有权
标题翻译：生产纤维素聚合物的方法
公开(公告)号：US06600034B2
公开(公告)日：2003-07-29
申请号：US09785322
申请日：2001-02-20
申请人： Tadahisa Sato , Katsuyoshi Yamakawa , Hiroshi Onishi , Tadahiro Tsujimoto
发明人： Tadahisa Sato , Katsuyoshi Yamakawa , Hiroshi Onishi , Tadahiro Tsujimoto
IPC分类号： C08B100
CPC分类号： C08J3/14 , C08J3/091 , C08J2301/12 , C08L1/12 , Y02P20/544
摘要： A method of making cellulose polymer solution comprises dissolving a cellulose polymer raw material in a chlorine-free organic solvent system under a high temperature and a high pressure condition belonging to the nearcritical or the supercritical region of the system. By removing the solvent from the thus obtained cellulose polymer solution, cellulose polymer powders are also produced.
摘要翻译：制造纤维素聚合物溶液的方法包括在属于系统的临界或超临界区域的高温和高压条件下将纤维素聚合物原料溶解在无氯有机溶剂体系中。通过从由此得到的纤维素聚合物溶液中除去溶剂，也生产纤维素聚合物粉末。

8. 发明授权

US06190596B1 Process for producing cellulosic shaped objects 失效
标题翻译：纤维素状物的制造方法
公开(公告)号：US06190596B1
公开(公告)日：2001-02-20
申请号：US09242321
申请日：1999-04-09
申请人： Derek Budgell , Ulrich Wachsmann , Wilhelm Kramer
发明人： Derek Budgell , Ulrich Wachsmann , Wilhelm Kramer
IPC分类号： C08B100
CPC分类号： D01F2/00 , C08B1/003 , C08L1/02 , C08L2666/02
摘要： A process for producing cellulosic shaped objects includes extruding and coagulating a solution of chemical wood pulp in a tertiary amine oxide, and possibly a liquid that does not dissolve wood pulp and is miscible with the tertiary amine oxide, the solution capable of being shaped into objects, the process of producing the shapeable solution employing a first wood pulp with a higher degree of polymerization and a second wood pulp with a lower degree of polymerization, and whereby initially a solution of the first wood pulp with a higher degree of polymerization in the tertiary amine oxide and possibly non-dissolving liquid, and a composition containing the second wood pulp with a lower degree of polymerization, tertiary amine oxide, and possibly non-dissolving liquid, are prepared separately, and the solution and composition are subsequently at least mixed to obtain the shapeable solution.
摘要翻译：用于生产纤维素形物体的方法包括将化学木浆的溶液挤出和凝结在叔胺氧化物中，并且可能的是不溶解木浆的液体，并且可与叔胺氧化物混溶，该溶液能够成形为物体使用具有较高聚合度的第一木浆和具有较低聚合度的第二木浆生产可成形溶液的方法，并且由此最初在第三级中具有较高聚合度的第一木浆的溶液氧化胺和可能不溶解的液体，并且分别制备含有聚合度较低的第二木浆，叔胺氧化物和可能不溶解的液体的组合物，然后将溶液和组合物至少混合获得可塑的解决方案。

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