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1. 发明申请

US20130032028A1 METHOD FOR OPERATING GAS SEPARATION DEVICE 审中-公开
标题翻译：操作气体分离装置的方法
公开(公告)号：US20130032028A1
公开(公告)日：2013-02-07
申请号：US13641605
申请日：2011-04-08
申请人： Yuzuru Miyazawa , Yoko Aomura , Yoshihiko Kobayashi , Kenji Haraya , Miki Yoshimune
发明人： Yuzuru Miyazawa , Yoko Aomura , Yoshihiko Kobayashi , Kenji Haraya , Miki Yoshimune
IPC分类号： B01D53/22 , B01D71/02
CPC分类号： B01D53/22 , B01D71/021 , B01D2257/108 , B01D2257/11 , B01D2311/13 , B01D2317/022 , B01D2319/04 , C01B3/503 , C01B23/0042 , C01B2210/0029 , C01B2210/0037 , C01B2210/0039 , C01B2210/004 , C01B2210/0053 , C01B2210/0079
摘要： Provided are a method for operating a gas separation device capable of performing gas separation with high separation capability and treatment amount in a small membrane area or in a small number of separation membrane modules, and a method for recovering a residual gas capable of performing more suitable detoxifying treatment or recycling by efficiently separating and recovering a mixed gas remaining in a cylinder, using the operating method. Two or more separation membrane modules are connected with each other in parallel. One separation membrane module is continuously and repeatedly operated in an operation cycle including: a first process for supplying a mixed gas into an airtight container and filling the airtight container with pressure; a second process for, when a predetermined time has elapsed or a predetermined pressure has been reached, stopping the supply of the mixed gas and retaining the supplied mixed gas; a third process for, when a predetermined time has elapsed or a predetermined pressure has been reached, recovering the mixed gas from a non-permeated gas discharge port; and a fourth process for, when a predetermined time has elapsed or a predetermined pressure has been reached, closing the non-permeated gas discharge port. The other separation membrane modules are operated in operation cycles shifted by respective predetermined intervals.
摘要翻译：本发明提供一种能够进行气体分离装置的方法，所述气体分离装置能够在小膜区域或少量分离膜组件中具有高分离能力和处理量的气体分离，以及用于回收能够进行更合适的残留气体的方法通过使用该操作方法有效地分离和回收残留在气缸中的混合气体来进行解毒处理或再循环。两个或更多个分离膜组件彼此并联连接。一个分离膜组件在操作循环中连续重复操作，包括：将混合气体供应到气密容器中并用压力填充气密容器的第一工序; 当经过预定时间或达到预定压力时，停止供应混合气体并保持供应的混合气体的第二过程; 当经过预定时间或达到预定压力时，从未透过气体排出口回收混合气体的第三工序; 以及当达到预定时间或达到预定压力时，关闭非渗透气体排出口的第四过程。其他分离膜组件在以预定间隔移动的操作循环中操作。

2. 发明申请

US20100206164A1 GAS PURIFICATION METHOD 失效
标题翻译：气体净化方法
公开(公告)号：US20100206164A1
公开(公告)日：2010-08-19
申请号：US12682329
申请日：2008-10-09
申请人： Yuzuru Miyazawa , Yoshihiko Kobayashi , Kenji Haraya , Miki Yoshimune
发明人： Yuzuru Miyazawa , Yoshihiko Kobayashi , Kenji Haraya , Miki Yoshimune
IPC分类号： B01D53/22
CPC分类号： C01B7/00 , B01D53/22 , B01D53/228 , B01D63/02 , B01D71/021 , B01D2257/20 , B01D2258/0216 , C01B3/04 , C01B3/503 , C01B2203/0405 , C01B2210/0045 , C01B2210/0051 , C01B2210/0062 , C01C1/024 , Y02E60/364
摘要： A gas purification method of the present invention uses a carbon membrane having a molecular sieving action to purify at least one selected from the group consisting of a hydride gas, a hydrogen halide gas, and a halogen gas, each gas containing an impurity at 10 ppm or less. The present invention can be used for a recovery unit that recoveries a used gas to reuse it as an ultrapure semiconductor material gas, and a unit or equipment that produces or charges an ultrapure semiconductor material gas.
摘要翻译：本发明的气体净化方法使用具有分子筛分作用的碳膜来净化选自氢化物气体，卤化氢气体和卤素气体中的至少一种，每种气体含有10ppm的杂质或更少。本发明可用于回收利用废气的回收单元，以将其用作超纯半导体材料气体，以及产生或充电超纯半导体材料气体的单元或设备。

3. 发明授权

US08357228B2 Gas purification method 失效
标题翻译：气体净化方法
公开(公告)号：US08357228B2
公开(公告)日：2013-01-22
申请号：US12682329
申请日：2008-10-09
申请人： Yuzuru Miyazawa , Yoshihiko Kobayashi , Kenji Haraya , Miki Yoshimune
发明人： Yuzuru Miyazawa , Yoshihiko Kobayashi , Kenji Haraya , Miki Yoshimune
IPC分类号： B01D53/22
CPC分类号： C01B7/00 , B01D53/22 , B01D53/228 , B01D63/02 , B01D71/021 , B01D2257/20 , B01D2258/0216 , C01B3/04 , C01B3/503 , C01B2203/0405 , C01B2210/0045 , C01B2210/0051 , C01B2210/0062 , C01C1/024 , Y02E60/364
摘要： A gas purification method of the present invention uses a carbon membrane having a molecular sieving action to purify at least one selected from the group consisting of a hydride gas, a hydrogen halide gas, and a halogen gas, each gas containing an impurity at 10 ppm or less. The present invention can be used for a recovery unit that recoveries a used gas to reuse it as an ultrapure semiconductor material gas, and a unit or equipment that produces or charges an ultrapure semiconductor material gas.
摘要翻译：本发明的气体净化方法使用具有分子筛分作用的碳膜来净化选自氢化物气体，卤化氢气体和卤素气体中的至少一种，每种气体含有10ppm的杂质或更少。本发明可用于回收利用废气的回收单元，以将其用作超纯半导体材料气体，以及产生或充电超纯半导体材料气体的单元或设备。

4. 发明授权

US08303690B2 Hollow fiber carbon membrane and method for production thereof 有权
标题翻译：中空纤维碳膜及其制造方法
公开(公告)号：US08303690B2
公开(公告)日：2012-11-06
申请号：US12671003
申请日：2008-07-31
申请人： Miki Yoshimune , Kenji Haraya
发明人： Miki Yoshimune , Kenji Haraya
IPC分类号： B01D53/22
CPC分类号： B01D71/021 , B01D53/22 , B01D63/02 , B01D63/021 , B01D67/0067 , B01D69/02 , B01D69/08 , B01D69/081 , B01D71/52 , B01D2325/24 , D01D5/24 , D01D5/34 , D01F9/24
摘要： A hollow fiber carbon membrane is provided, which has excellent gas separation performance, unbreakable flexibility and high utility. The hollow fiber carbon membrane comprises carbonized substance obtained by calcination of a hollow fiber-like material formed from a polyphenylene oxide derivative, and has an external diameter in the range of 0.08 mm to 0.25 mm. The polyphenylene oxide derivative substantially comprises repeating units represented by the following (a) and (b) (in the structural formula, R11 and R12 independently represent hydrogen atom or sulfone group, except that R11 and R12 are both hydrogen atoms), wherein the ratio A (%) of the repeating unit (b) to the repeating units (a)+(b) satisfies 15%
摘要翻译：提供中空纤维碳膜，具有优异的气体分离性能，不易破碎的灵活性和高效用性。中空纤维碳膜包括通过煅烧由聚苯醚衍生物形成的中空纤维状材料而获得的碳化物质，其外径在0.08mm至0.25mm的范围内。聚苯醚衍生物基本上包含由以下（a）和（b）表示的重复单元（在结构式中，R 11和R 12独立地表示氢原子或砜基，除了R 11和R 12均为氢原子），其中，重复单元（b）与重复单元（a）+（b）的（％）的比例满足15％

5. 发明申请

US20100212503A1 HOLLOW FIBER CARBON MEMBRANE AND METHOD FOR PRODUCTION THEREOF 有权
标题翻译：中空纤维碳膜及其生产方法
公开(公告)号：US20100212503A1
公开(公告)日：2010-08-26
申请号：US12671003
申请日：2008-07-31
申请人： Miki Yoshimune , Kenji Haraya
发明人： Miki Yoshimune , Kenji Haraya
IPC分类号： B01D53/22 , D01D5/00
CPC分类号： B01D71/021 , B01D53/22 , B01D63/02 , B01D63/021 , B01D67/0067 , B01D69/02 , B01D69/08 , B01D69/081 , B01D71/52 , B01D2325/24 , D01D5/24 , D01D5/34 , D01F9/24
摘要： A hollow fiber carbon membrane is provided, which has excellent gas separation performance, unbreakable flexibility and high utility. The hollow fiber carbon membrane comprises carbonized substance obtained by calcination of a hollow fiber-like material formed from a polyphenylene oxide derivative, and has an external diameter in the range of 0.08 mm to 0.25 mm. The polyphenylene oxide derivative substantially comprises repeating units represented by the following (a) and (b) (in the structural formula, R11 and R12 independently represent hydrogen atom or sulfone group, except that R11 and R12 are both hydrogen atoms), wherein the ratio A (%) of the repeating unit (b) to the repeating units (a)+(b) satisfies 15%
摘要翻译：提供中空纤维碳膜，具有优异的气体分离性能，不易破碎的灵活性和高效用性。中空纤维碳膜包括通过煅烧由聚苯醚衍生物形成的中空纤维状材料而获得的碳化物质，其外径在0.08mm至0.25mm的范围内。聚苯醚衍生物基本上包含由以下（a）和（b）表示的重复单元（在结构式中，R 11和R 12独立地表示氢原子或砜基，除了R 11和R 12均为氢原子），其中，重复单元（b）与重复单元（a）+（b）的（％）的比例满足15％

6. 发明授权

US09132381B2 Hydrogen separation device 有权
标题翻译：氢分离装置
公开(公告)号：US09132381B2
公开(公告)日：2015-09-15
申请号：US13993937
申请日：2011-12-13
申请人： Shigeki Hara , Masakazu Mukaida , Hiroyuki Suda , Kenji Haraya
发明人： Shigeki Hara , Masakazu Mukaida , Hiroyuki Suda , Kenji Haraya
IPC分类号： B01D53/22 , B01D63/08 , C01B3/50 , H01M8/06
CPC分类号： B01D53/22 , B01D63/082 , B01D2256/16 , C01B3/503 , C01B3/505 , C01B2203/0405 , C01B2203/047 , C01B2203/0475 , H01M8/0687
摘要： The hydrogen separation device comprises a laminate formed by laminating and integrating a hydrogen separation layer, a mixed gas layer kept adjacent to one surface of the hydrogen separation layer and having a mixed gas flow path, and a transmitted gas layer kept adjacent to the other surface of the hydrogen separation layer and having a transmitted gas flow path, and a vessel containing the laminate therein and filled with a buffer gas, wherein a buffer space is provided between the laminate and the inner wall of the vessel in which a buffer gas can reach at least one end face of the laminate in the lamination direction, and wherein the pressure in the buffer space is equal to or higher than the higher one of the pressure in the mixed gas flow path and the pressure in the transmitted gas flow path.
摘要翻译：氢分离装置包括通过层压和集成氢分离层，与氢分离层的一个表面相邻并具有混合气体流动路径的混合气体层和与另一表面保持邻近的透射气体层而形成的层压体的氢分离层并具有透射气体流路，容器内装有层叠体并填充有缓冲气体，其中缓冲空间设置在层压体和缓冲气体可到达的容器的内壁之间层叠体的层叠方向的至少一个端面，其中缓冲空间中的压力等于或高于混合气体流路中的压力和透气的流动路径中的压力中的较高者。

7. 发明授权

US5445669A Membrane for the separation of carbon dioxide 失效
标题翻译：膜分离二氧化碳
公开(公告)号：US5445669A
公开(公告)日：1995-08-29
申请号：US288198
申请日：1994-08-09
申请人： Makoto Nakabayashi , Kazuhiro Okabe , Takayuki Mishima , Hiroshi Mano , Kenji Haraya
发明人： Makoto Nakabayashi , Kazuhiro Okabe , Takayuki Mishima , Hiroshi Mano , Kenji Haraya
IPC分类号： B01D53/22 , B01D61/38 , B01D69/10 , B01D69/14 , B01D69/08
CPC分类号： B01D69/142 , B01D53/228 , B01D61/38 , B01D69/10 , Y02C10/10
摘要： A membrane for the separation of carbon dioxide is disclosed which includes a hydrogel film of a cross-linked, vinyl alcohol/acrylic acid salt copolymer impregnated with an aqueous carrier solution containing a carbon dioxide carrier dissolved therein. A composition containing a solvent, an alkali metal carbonate or bicarbonates, and a polydentate ligand capable of forming a complex with an alkali metal ion is suitably used as the carrier solution. This composition may also be used for the preparation of a liquid film of a carbon dioxide separation membrane.
摘要翻译：公开了一种用于分离二氧化碳的膜，其包括浸渍有溶解有二氧化碳载体的水性载体溶液的交联乙烯醇/丙烯酸盐共聚物的水凝胶膜。作为载体溶液，可以适当使用含有溶剂，碱金属碳酸盐或碳酸氢盐，能与碱金属离子形成络合物的多齿配体的组合物。该组合物也可用于制备二氧化碳分离膜的液膜。

8. 发明授权

US06531569B1 Resin material for gas separation base and process for producing the same 失效
标题翻译：气体分离基材用树脂及其制造方法
公开(公告)号：US06531569B1
公开(公告)日：2003-03-11
申请号：US09937143
申请日：2001-09-21
申请人： Akira Tachiki , Hiroshi Mano , Kenji Haraya
发明人： Akira Tachiki , Hiroshi Mano , Kenji Haraya
IPC分类号： C08G6944
CPC分类号： B01D71/82 , B01D53/228 , B01D71/24 , B01D71/44 , B01D71/52 , B01D71/56 , B01D71/64 , B01D71/68 , C08G73/10
摘要： This invention relates to resin material for gas separation base containing a cardo polyimide structure in which the hydrogen atoms in the side-chain benzyl and/or allyl position are halogenated at a rate of modification by halogen of 0.1% or more or resin material for gas separation base containing polymer in which the hydrogen atoms in the side-chain benzyl and/or allyl position are halogenated at a rate of modification by halogen of 34% or more and, additionally, relates to polymer which serves as raw material for the aforementioned resin material for gas separation base containing a cardo polymer structure and a process for producing said polymer; said polymer not only excels in such properties as solvent solubility, ease of conversion to film by a wet process, thermal stability, and chemical stability but also performs well in gas permeability and the process of this invention makes it possible to produce gas separation base, particularly gas separation membrane, whose gas permeability and gas selectivity can be readily controlled.
摘要翻译：本发明涉及一种含有聚酰亚胺结构的气相分离基材，其中侧链苄基和/或烯丙基位置中的氢原子以0.1％以上的卤素改性或用于气体的树脂材料被卤化其中侧链苄基和/或烯丙基位置中的氢原子以卤素改性率为34％以上卤化的分离碱的聚合物，另外涉及作为上述树脂的原料的聚合物含有cardo聚合物结构的气体分离基材料和所述聚合物的制造方法; 所述聚合物不仅具有溶剂溶解性，通过湿法转化成膜的容易性，热稳定性和化学稳定性等特性，而且在气体渗透性方面表现良好，本发明的方法使得可以生产气体分离基，特别是气体分离膜，其气体渗透性和气体选择性可以容易地控制。

9. 发明申请

US20130333569A1 HYDROGEN SEPARATION DEVICE 有权
标题翻译：氢分离装置
公开(公告)号：US20130333569A1
公开(公告)日：2013-12-19
申请号：US13993937
申请日：2011-12-13
申请人： Shigeki Hara , Masakazu Mukaida , Hiroyuki Suda , Kenji Haraya
发明人： Shigeki Hara , Masakazu Mukaida , Hiroyuki Suda , Kenji Haraya
IPC分类号： B01D53/22
CPC分类号： B01D53/22 , B01D63/082 , B01D2256/16 , C01B3/503 , C01B3/505 , C01B2203/0405 , C01B2203/047 , C01B2203/0475 , H01M8/0687
摘要： The hydrogen separation device comprises a laminate formed by laminating and integrating a hydrogen separation layer, a mixed gas layer kept adjacent to one surface of the hydrogen separation layer and having a mixed gas flow path, and a transmitted gas layer kept adjacent to the other surface of the hydrogen separation layer and having a transmitted gas flow path, and a vessel containing the laminate therein and filled with a buffer gas, wherein a buffer space is provided between the laminate and the inner wall of the vessel in which a buffer gas can reach at least one end face of the laminate in the lamination direction, and wherein the pressure in the buffer space is equal to or higher than the higher one of the pressure in the mixed gas flow path and the pressure in the transmitted gas flow path.
摘要翻译：氢分离装置包括通过层压和集成氢分离层，与氢分离层的一个表面相邻并具有混合气体流动路径的混合气体层和与另一表面保持邻近的透射气体层而形成的层压体的氢分离层并具有透射气体流路，容器内装有层叠体并填充有缓冲气体，其中缓冲空间设置在层压体和缓冲气体可到达的容器的内壁之间层叠体的层叠方向的至少一个端面，其中缓冲空间中的压力等于或高于混合气体流路中的压力和透气的流动路径中的压力中的较高者。

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