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1. 发明授权

US4841027A Process for preparing phenyl- and naphthylazo-aminonaphthol sulphonic acids 失效
标题翻译：制备苯基和萘基氨基萘酚磺酸的方法
公开(公告)号：US4841027A
公开(公告)日：1989-06-20
申请号：US700063
申请日：1985-02-11
申请人： Yutaka Kayane , Takashi Omura , Yasuo Tezuka , Hideharu Sone
发明人： Yutaka Kayane , Takashi Omura , Yasuo Tezuka , Hideharu Sone
IPC分类号： C09B29/30 , C09B41/00 , C09B43/44 , C09B62/028 , C09B62/44
CPC分类号： C09B62/4413 , C09B29/30 , C09B43/44 , C09B62/028
摘要： Improvement in a process for producing an arylazo-aminonaphtholsulfonic acid represented by a free acid of the formula, ##STR1## wherein A is a phenyl or naphthyl group unsubstituted or substituted by one to four members selected from alkyl, alkoxy, phenoxy, sulfonic acid, carboxylic acid, arylamino, amino, nitro and hydroxyl groups and halogen atoms, and m is 0 or 1, which comprises reacting an aminonaphtholsulfonic acid represented by a free acid of the formula, ##STR2## wherein m is as defined above, with a dibasic acid anhydride to obtain an acylaminonaphtholsulfonic acid, coupling a diazonium compound of amine of the formula,A'--NH.sub.2wherein A' is a phenyl or naphthyl group unsubstituted or substituted by one to four members selected from alkyl, alkoxy, phenoxy, sulfonic acid, carboxylic acid, arylamino, acrylamino, nitro and hydroxyl groups and halogen atoms, with the acylaminonaphtholsulfonic acid, and then subjecting the resulting coupling product to hydrolysis in the presence of an acid or an alkali. The arylazo-aminonaphtholsulfonic acid is useful as acid dyes or acid mordant dyes in itself as well as an important intermediate for the production of reactive dyes or direct dyes.
摘要翻译：一种由下式游离酸代表的芳基偶氮氨基萘酚磺酸的方法的改进，其中A是未被取代或被一至四个选自烷基，烷氧基，苯氧基，磺酸，羧酸，芳基氨基，氨基，硝基和羟基和卤素原子，m为0或1，其包括将下式游离酸代表的氨基萘磺酸与其中m如上所定义的二价基团酸酐，得到酰基氨基萘酚磺酸，偶联式为A'-NH 2的胺的重氮化合物，其中A'是未被取代或被一至四个选自烷基，烷氧基，苯氧基，磺酸，羧酸，芳基氨基，丙烯基氨基，硝基和羟基和卤素原子与酰基氨基萘磺酸反应，然后在得到的偶联产物在酸或碱。芳基偶氮氨基萘酚磺酸本身可用作酸性染料或酸性媒染剂染料，以及用于生产活性染料或直接染料的重要中间体。

2. 发明授权

US4341699A Reactive red dye having both monochlorotriazinyl- and vinylsulfone-type reactive groups 失效
标题翻译：具有一氯三嗪基和乙烯基砜型反应性基团的活性红色染料
公开(公告)号：US4341699A
公开(公告)日：1982-07-27
申请号：US166194
申请日：1980-07-07
申请人： Yasuo Tezuka , Masaki Sunami , Takashi Omura , Yutaka Kayane
发明人： Yasuo Tezuka , Masaki Sunami , Takashi Omura , Yutaka Kayane
IPC分类号： C09B62/44 , C07C107/08 , C09B62/085 , C09B62/51
CPC分类号： C09B62/4413
摘要： A dye represented by a free acid of the formula, ##STR1## wherein A is ##STR2## in which Z is --CH.sub.2 CH.sub.2 OSO.sub.3 H or --CH.dbd.CH.sub.2. This dye is usable for dyeing cellulose fibers in brilliant red color with good fastness, particularly, too chlorine, light and perspiration-light and possesses level dyeing properties.
摘要翻译：由下式游离酸代表的染料，其中A是Z，其中Z是-CH 2 CH 2 OSO 3 H或-CH = CH 2。该染料可用于染色具有良好牢度的亮红色纤维素纤维，特别是氯，轻和排汗光，并具有良好的染色性能。

3. 发明授权

US4937326A Reactive scarlet dyes having both monochlorotriazinyl and vinylsulfone type reactive groups linked via N-alkylated amino 失效
标题翻译：具有通过N-烷基化氨基连接的单氯三嗪基和乙烯基砜型反应性基团的活性猩红染料
公开(公告)号：US4937326A
公开(公告)日：1990-06-26
申请号：US714361
申请日：1985-03-22
申请人： Yutaka Kayane , Masaki Sunami , Katsumasa Otake , Yasuo Tezuka
发明人： Yutaka Kayane , Masaki Sunami , Katsumasa Otake , Yasuo Tezuka
IPC分类号： C09B62/44
CPC分类号： C09B62/4413
摘要： A novel reactive monoazo dye, which can give to cellulose fiber materials a deep orange to scarlet color superior in build-up property and chlorine fastness, represented by a free acid of the formula, ##STR1## wherein D is a phenyl group substituted with 1 to 3 substitutes selected from methyl, ethyl, methoxy, ethoxy, halogen, acetylamino, propionylamino, benzoylamino, succinylamino, maleinylamino, nitro, suflonic acid and carboxyl groups; R.sub.1 is a hydrogen atom, or a methyl or ethyl group; R.sub.2 is an alkyl group having 1 to 4 carbon atoms which is unsubstituted or substituted with a hydroxy, cyano, alkoxy, halogen, carboxy, alkoxycarbonyl or sulfonic acid group; Z is a hydrogen atom or a sulfonic acid group; A is a phenylene residue which is unsubstituted or substituted with 1 or 2 substituents selected from methyl, ethyl, methoxy, ethoxy, chlorine, bromine and sulfonic acid groups; or a naphthylene residue which is unsubstituted or substituted with one sulfonic acid group; and X is --SO.sub.2 CH.dbd.CH.sub.2 or --SO.sub.2 CH.sub.2 CH.sub.2 Y in which Y is a group which is splittable by alkalis.
摘要翻译：一种新型的反应性单偶氮染料，其可以赋予纤维素纤维材料深层橙色至具有优异的聚集性能和耐氯牢度的猩红色，由下式的游离酸代表：其中D是被1个至3个选自甲基，乙基，甲氧基，乙氧基，卤素，乙酰氨基，丙酰氨基，苯甲酰基氨基，琥珀酰氨基，马来酰氨基，硝基，磺酰基和羧基的取代基。 R1是氢原子，或甲基或乙基; R2是未取代的或被羟基，氰基，烷氧基，卤素，羧基，烷氧基羰基或磺酸基团取代的具有1至4个碳原子的烷基; Z是氢原子或磺酸基; A是未取代的或被1或2个选自甲基，乙基，甲氧基，乙氧基，氯，溴和磺酸基的取代基取代的亚苯基; 或未被取代或被一个磺酸基团取代的亚萘基残基; X为-SO 2 CH = CH 2或-SO 2 CH 2 CH 2 Y，其中Y为可被碱分解的基团。

4. 发明授权

US4841031A Reactive dye having both monochlorotriazinyl and vinylsulfone type reactive groups 失效
标题翻译：具有单氯三嗪基和乙烯基砜型反应性基团的活性染料
公开(公告)号：US4841031A
公开(公告)日：1989-06-20
申请号：US648349
申请日：1984-09-07
申请人： Yutaka Kayane , Katsumasa Otake , Yasuo Tezuka
发明人： Yutaka Kayane , Katsumasa Otake , Yasuo Tezuka
IPC分类号： C09B62/44
CPC分类号： C09B62/4413
摘要： A novel reactive monoazo dye, capable of giving cellulose fiber materials a deep orange to scarlet color and superior in build-up and chlorine fastness properties, represented by a free acid of the formula, ##STR1## wherein R.sub.1 is hydrogen, methyl or ethyl; R.sub.2 is an alkyl having 1 to 4 carbons that is either unsubstituted or substituted with hydroxy, cyano, alkoxy, halogen, carboxy, alkoxycarbonyl or sulfonic acid; Z is hydrogen or sulfonic acid; A is phenylene and is either unsubstituted or substituted with 1 or 2 substituents selected from the group consisting of methyl, ethyl, methoxy, ethoxy, chlorine, bromine and sulfonic acid, or natphthylene that is either unsubstituted or substituted with sulfonic acid; X is --SO.sub.2 CH.dbd.CH.sub.2 or --SO.sub.2 CH.sub.2 CH.sub.2 Y in which Y is a group that is splittable by alkalis; and m is an integer of 1 to 3.
摘要翻译：一种新型的反应性单偶氮染料，其能够使纤维素纤维材料具有深橙色至猩红色，并且具有优异的聚集性和耐氯性质，由下式的游离酸代表：其中R1是氢，甲基或乙基; R2是未取代的或被羟基，氰基，烷氧基，卤素，羧基，烷氧基羰基或磺酸取代的具有1至4个碳原子的烷基; Z是氢或磺酸; A是亚苯基，并且是未取代的或被1或2个选自甲基，乙基，甲氧基，乙氧基，氯，溴和磺酸的取代基取代，或未被取代或被磺酸取代的萘基; X是-SO 2 CH = CH 2或-SO 2 CH 2 CH 2 Y，其中Y是可以被碱分解的基团; m为1〜3的整数。

5. 发明授权

US4378313A Reactive yellow dye having both monochlorotriazinyl and vinylsulfone type reactive groups 失效
标题翻译：具有单氯三嗪基和乙烯基砜型反应性基团的活性黄色染料
公开(公告)号：US4378313A
公开(公告)日：1983-03-29
申请号：US153633
申请日：1980-05-27
申请人： Yutaka Kayane , Masaki Sunami , Yasuo Tezuka
发明人： Yutaka Kayane , Masaki Sunami , Yasuo Tezuka
IPC分类号： C09B62/44 , C09B62/085 , D06P1/382 , D06P3/66
CPC分类号： C09B62/4413
摘要： The compounds represented, in the form of free acid, by the following general formula (I): ##STR1## (wherein A is ##STR2## (wherein R.sub.3 and R.sub.4 are each hydrogen or a methyl, ethyl, methoxy, ethoxy, acetylamino, propionylamino, benzoylamino or ureido group, and R.sub.5 and R.sub.6 are each hydrogen or a methyl or methoxy group), R.sub.1 and R.sub.2 are each hydrogen or a methyl, ethyl or sulfomethyl group, X.sub.1 and X.sub.2 are each hydrogen, chlorine or a methyl, methoxy, carboxyl or sulfonic acid group, m is a number of 0, 1 or 2, and n is a number of 1 or 2, provided that the sum of m and n is 1, 2 or 3).These compounds are capable of dyeing cellulose fibers in yellow with excellent color fastness to hypochlorite, light, perspiration and sunlight and high acid stability.
摘要翻译：化合物以游离酸的形式由以下通式（I）表示：其中A为（其中R 3和R 4各自为氢或甲基，乙基，甲氧基，乙氧基，乙酰氨基，丙酰氨基，苯甲酰氨基或脲基，R 5和R 6各自为氢或甲基或甲氧基），R 1和R 2各自为氢或甲基，乙基或磺基甲基，X 1和X 2各自为氢，氯或甲基，甲氧基，羧基或磺酸基，m为0,1或2的数，n为1或2的数，条件是m和n之和为1,2或3）。这些化合物能够以黄色染色纤维素纤维，对次氯酸盐，光，汗和阳光具有优异的色牢度和高酸稳定性。

6. 发明授权

US5266696A 1-aminoanthraquinone dye compound having fiber reactive group through sulfur or oxygen atom at 4-position and imparting red color 失效
标题翻译：具有纤维反应性基团的1-氨基蒽醌染料化合物，通过硫或氧原子在4位上赋予红色
公开(公告)号：US5266696A
公开(公告)日：1993-11-30
申请号：US836825
申请日：1992-02-19
申请人： Kingo Akahori , Naoki Harada , Yutaka Kayane , Takashi Omura
发明人： Kingo Akahori , Naoki Harada , Yutaka Kayane , Takashi Omura
IPC分类号： C09B62/024 , C09B62/44 , C09B62/505 , C07D251/70 , C09B62/06 , D06P1/382 , D06P1/384
CPC分类号： C09B62/024 , C09B62/4409 , C09B62/505
摘要： Anthraquinone compounds of the formula, ##STR1## wherein R is hydrogen, alkyl or the like, R.sub.1 and R.sub.2 are each hydrogen, halogen or sulfo, l is 1 or 2, X is sulfo or the like or --V--A--(W).sub.m --Z, and Y is --V.sub.1 --A.sub.1 --U, wherein V and V.sub.1 are each --O-- or --S--, A and A.sub.1 are each a divalent group such as ##STR2## W is --NH-- or the like, Z is hydrogen or a fiber reactive group, and U is hydrogen, a fiber reactive group or a fiber reactive group-containing group, provided that at least one of Z and U is or has a fiber reactive group, which is useful for dyeing or printing fiber materials such as cotton to give a dyed or printed product having excellent fastness properties, particularly those such as light fastness and perspiration-light fastness.
摘要翻译：下式的蒽醌化合物，其中R是氢，烷基等，R 1和R 2各自为氢，卤素或磺基，l为1或2，X为磺基等或-VA-（W）mZ ，Y为-V1-A1-U，其中V和V1各自为-O-或-S-，A和A1各自为二价基团，例如W为-NH-等，Z为氢或纤维反应性基团，U为氢，纤维反应性基团或含纤维反应性基团，条件是Z和U中的至少一个为或具有纤维反应性基团，其可用于染色或印刷纤维材料例如棉，以得到具有优异坚牢性的染色或印刷产品，特别是耐光牢度和耐汗牢度等。

7. 发明授权

US6136970A Asymmetric dioxazine compounds and method for dyeing or printing fiber materials using the same 失效
标题翻译：不对称二恶嗪化合物及其染色或印花方法
公开(公告)号：US6136970A
公开(公告)日：2000-10-24
申请号：US967617
申请日：1992-10-29
申请人： Kazufumi Yokogawa , Takahiko Fujisaki , Miyao Takahashi , Shigeru Kawabata , Naoki Harada , Kingo Akahori , Yutaka Kayane , Takashi Omura
发明人： Kazufumi Yokogawa , Takahiko Fujisaki , Miyao Takahashi , Shigeru Kawabata , Naoki Harada , Kingo Akahori , Yutaka Kayane , Takashi Omura
IPC分类号： C07D265/34 , C09B19/00 , C09B62/002 , C09B62/02 , C09B62/44 , C09B62/503 , C07D498/04
CPC分类号： C09B62/5033 , C09B62/0025 , C09B62/021 , C09B62/4405
摘要： An asymmetric dioxazine compound represented by the following formula (I) in the free acid form: ##STR1## wherein A.sub.1 and A.sub.2 independently of one another are each sulfo, halo, alkyl or alkoxy, X.sub.1 and X.sub.2 independently of one another are each hydrogen, halo, alkyl, alkoxy or phenoxy, R.sub.1 is hydrogen or unsubstituted or substituted alkyl, R.sub.2 and R.sub.3 independently of one another are each hydrogen, alkyl, alkoxy, halo or unsubstituted or substituted amino, Z is a fiber-reactive group, m and n independently of one another are each 0 or 1, provided that m.noteq.n, and L is 1 or 2. This compound is suitable for dyeing and printing cellulose fiber, natural and synthetic polyamide fibers, polyurethane fiber, leather and the like and mixed yarns thereof, to obtain dyed or printed products of a color fast to light, wetness and chlorine with superior build-up and level dyeing properties.
摘要翻译：由游离酸形式的下式（I）表示的不对称二嗪类化合物：其中A1和A2彼此独立地各自为磺基，卤素，烷基或烷氧基，X 1和X 2彼此独立地为氢，卤素，烷基，烷氧基或苯氧基，R 1是氢或未取代或取代的烷基，R 2和R 3彼此独立地各自为氢，烷基，烷氧基，卤素或未取代或取代的氨基，Z为纤维反应性基团，m和n独立地为一个另外每个都为0或1，条件是m注意n和L为1或2.该化合物适用于将纤维素纤维，天然和合成聚酰胺纤维，聚氨酯纤维，皮革等及其混合纱线染色和印刷到获得染色或印刷的产品，颜色快速到轻，湿和氯，具有优异的积聚和水平的染色性能。

8. 发明授权

US4511507A Monoazo compound having both monochlorotriazinyl and vinylsulfone type reactive groups 失效
标题翻译：具有单氯三嗪基和乙烯基砜型反应性基团的单偶氮化合物
公开(公告)号：US4511507A
公开(公告)日：1985-04-16
申请号：US563587
申请日：1983-12-20
申请人： Yutaka Kayane , Takashi Omura , Katsumasa Otake , Akira Takeshita
发明人： Yutaka Kayane , Takashi Omura , Katsumasa Otake , Akira Takeshita
IPC分类号： C09B33/10 , C09B62/44 , C09B62/51 , D06P1/38 , C09B62/08 , D06P3/10
CPC分类号： D06P1/38 , C09B62/4413 , Y10S8/918
摘要： A monoazo compound which is useful for dyeing or printing fiber materials, particularly cellulose fiber materials in red color, and which is represented by a free acid of the formula, ##STR1## wherein D is a phenyl group substituted with one to three substituents selected from the group consisting of halogen atoms and methyl, ethyl, methoxy, ethoxy, acetylamino, propionylamino, sulfo and carboxyl groups, R is a C.sub.1 to C.sub.4 alkyl group unsubstituted or substituted with a halogen atom or a hydroxyl, cyano, alkyl, alkoxy, carboxyl, carbamoyl, alkoxycarbonyl or sulfo group, A is a phenylene group unsubstituted or substituted with one or two substituents selected from the group consisting of methyl, ethyl, methoxy, ethoxy and sulfo groups and chlorine and bromine atoms, or a naphthylene group unsubstituted or substituted with one sulfo group, and X is --SO.sub.2 CH.dbd.CH.sub.2 or --SO.sub.2 CH.sub.2 CH.sub.2 Y in which Y is a group capable of being split by the action of an alkali.
摘要翻译：用于染色或印刷纤维材料，特别是红色的纤维素纤维材料的单偶氮化合物，其由下式的游离酸表示，其中D是被一至三个选自以下的取代基取代的苯基：由卤素原子和甲基，乙基，甲氧基，乙氧基，乙酰氨基，丙酰氨基，磺基和羧基组成的基团，R是未被取代或被卤素原子或羟基，氰基，烷基，烷氧基，羧基取代的C1至C4烷基，氨基甲酰基，烷氧基羰基或磺基，A是未被取代或被一个或两个选自甲基，乙基，甲氧基，乙氧基和磺基以及氯和溴原子的取代基取代的亚苯基，或未取代或取代的亚萘基具有一个磺基，X是-SO 2 CH = CH 2或-SO 2 CH 2 CH 2 Y，其中Y是能够通过碱的作用而分裂的基团。

9. 发明授权

US4977261A Anthraquinone compound 失效
标题翻译：蒽醌化合物
公开(公告)号：US4977261A
公开(公告)日：1990-12-11
申请号：US141762
申请日：1988-01-11
申请人： Yutaka Kayane , Takashi Omura , Naoki Harada , Yasuji Mori , Yosuke Yamamoto , Tetsuya Miyamoto , Takehiro Kusumoto
发明人： Yutaka Kayane , Takashi Omura , Naoki Harada , Yasuji Mori , Yosuke Yamamoto , Tetsuya Miyamoto , Takehiro Kusumoto
IPC分类号： C09B62/505
CPC分类号： C09B62/505
摘要： A compound of the following formula in the free acid form, ##STR1## wherein and R and R.sub.1 are each hydrogen or alkyl, A is a divalent group of the formula, ##STR2## wherein R.sub.3, R.sub.4 and R.sub.5 are each hydrogen, methyl, ethyl, methoxy or ethoxy, m is 0 or 1, n, u and v are each 0, 1 or 2, p is 0, 1, 2 or 3, q and s are each an integer of 2 to 6, and r is 1 or 2, B.sub.1 is phenylene or naphthylene, Z.sub.1 is vinyl, .beta.-sulfatoethyl or the like, l is 0, 1 or 2, and X is a group of the formula, ##STR3## wherein R.sub.2 is hydrogen or alkyl, B.sub.2 is phenylene or naphtylene, Z.sub.2 is vinyl, .beta.-sulfatoethyl or the like, R.sub.6 and R.sub.7 are each hydrogen, alkyl, phenyl, naphthyl or benzyl, and R, A and l are as defined above, which is useful for dyeing or printing fiber materials to give a dyed or printed product of a brilliant blue color superior in fastness properties such as light fastness and perspiration-light fastness, with superior build-up property.

10. 发明授权

US4975094A Anthrapyridone compounds having vinylsulfone type fiber reactive group through triazinyl bridging group 失效
标题翻译：通过三嗪基桥连基团具有乙烯基砜型纤维反应性基团的蒽并吡啶酮化合物
公开(公告)号：US4975094A
公开(公告)日：1990-12-04
申请号：US390278
申请日：1989-08-07
申请人： Masayuki Miki , Kingo Akahori , Yutaka Kayane , Naoki Harada , Takashi Omura
发明人： Masayuki Miki , Kingo Akahori , Yutaka Kayane , Naoki Harada , Takashi Omura
IPC分类号： C09B62/44 , C09B62/505
CPC分类号： C09B62/505 , C09B62/4403
摘要： Anthrapyridone compounds of the formula, ##STR1## wherein R.sub.1 is hydrogen, benzoyl, acetyl or alkyloxycarbonyl, R.sub.2 is hydrogen or alkyl, R.sub.3 is hydrogen, halogen, sulfo, phenoxy, phenylthio or alkoxy, R.sub.4 is hydrogen, halogen or sulfo, R.sub.5 and R.sub.6 are each hydrogen or alkyl, V is --O--, --S-- or ##STR2## in which R.sub.7 is hydrogen, acetyl or alkyl, B is phenylene or naphthylene, D is vinyl or --CH.sub.2 CH.sub.2 L such as --CH.sub.2 CH.sub.2 OSO.sub.3 H, A is a divalent group, and X is halogen, quaternary ammonium, pyridinio, amino or a ##STR3## like group, which are useful for dyeing or printing fiber materials with superior dyeing performance.

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