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1. 发明授权

US08552204B2 Zinc cluster 有权
标题翻译：锌簇
公开(公告)号：US08552204B2
公开(公告)日：2013-10-08
申请号：US13395312
申请日：2010-05-31
申请人： Yoshimasa Matsushima , Hideki Nara , Takahiro Fujiwara
发明人： Yoshimasa Matsushima , Hideki Nara , Takahiro Fujiwara
IPC分类号： C07D263/12 , C07D309/12 , C07F3/06 , C07C229/08 , C07C67/03
CPC分类号： C07D211/46 , B01J31/2239 , B01J2231/349 , B01J2531/0219 , B01J2531/26 , C07B41/12 , C07C53/18 , C07C67/03 , C07C67/08 , C07C269/06 , C07C2601/14 , C07D263/12 , C07D309/12 , C07F3/003 , C07C69/612 , C07C271/22
摘要： Disclosed is a novel zinc cluster compound represented by general formula (1): Zn4O (OCOR)6 (RCOOH)n, wherein R represents an alkyl group which has 1 to 4 carbon atoms and may be substituted with a halogen atom, and n represents 0.1 to 1, and also disclosed are a method for producing the compound and a reaction using the compound.
摘要翻译：公开了由通式（1）表示的新型锌簇化合物：Zn 4 O（OCOR）6（RCOOH）n，其中R表示具有1至4个碳原子并可被卤素原子取代的烷基，n表示 0.1〜1，也公开了使用该化合物的化合物的制造方法和反应。

2. 发明申请

US20120172601A1 ZINC CLUSTER 有权
标题翻译： ZINC集群
公开(公告)号：US20120172601A1
公开(公告)日：2012-07-05
申请号：US13395312
申请日：2010-05-31
申请人： Yoshimasa Matsushima , Hideki Nara , Takahiro Fujiwara
发明人： Yoshimasa Matsushima , Hideki Nara , Takahiro Fujiwara
IPC分类号： C07F3/06 , C07C67/08 , C07F7/18 , C07C229/34 , C07D211/46 , C07D263/12 , C07C67/03
CPC分类号： C07D211/46 , B01J31/2239 , B01J2231/349 , B01J2531/0219 , B01J2531/26 , C07B41/12 , C07C53/18 , C07C67/03 , C07C67/08 , C07C269/06 , C07C2601/14 , C07D263/12 , C07D309/12 , C07F3/003 , C07C69/612 , C07C271/22
摘要： Disclosed is a novel zinc cluster compound represented by general formula (1): Zn4O (OCOR)6 (RCOOH)n, wherein R represents an alkyl group which has 1 to 4 carbon atoms and may be substituted with a halogen atom, and n represents 0.1 to 1, and also disclosed are a method for producing the compound and a reaction using the compound.
摘要翻译：公开了由通式（1）表示的新型锌簇化合物：Zn 4 O（OCOR）6（RCOOH）n，其中R表示具有1至4个碳原子并可被卤素原子取代的烷基，n表示 0.1〜1，也公开了使用该化合物的化合物的制造方法和反应。

3. 发明授权

US07880025B2 Ruthenium silyl-arene complex , and method for production thereof 有权
标题翻译：钌甲硅烷基芳烃络合物及其制备方法
公开(公告)号：US07880025B2
公开(公告)日：2011-02-01
申请号：US12782153
申请日：2010-05-18
申请人： Taichiro Touge , Hideki Nara , Takahiro Fujiwara
发明人： Taichiro Touge , Hideki Nara , Takahiro Fujiwara
IPC分类号： C07F15/00 , B01J31/00
CPC分类号： C07F15/0046 , C07F17/02
摘要： The present invention is to provide a ruthenium complex having a novel arene moiety, which has improved solubility in various solvents, and a method for production thereof.The present invention relates to a novel ruthenium complex having an arene moiety, which has a trisubstituted silyl group introduced to the arene moiety, and a method for production thereof.
摘要翻译：本发明提供一种具有新的芳族部分的钌配合物及其制备方法，其在各种溶剂中的溶解度提高。本发明涉及一种具有引入到芳族部分的三取代甲硅烷基的具有芳烃部分的新型钌络合物及其制备方法。

4. 发明申请

US20100298588A1 RUTHENIUM SILYL-ARENE COMPLEX , AND METHOD FOR PRODUCTION THEREOF 有权
标题翻译：镧系复合物及其生产方法
公开(公告)号：US20100298588A1
公开(公告)日：2010-11-25
申请号：US12782153
申请日：2010-05-18
申请人： Taichiro Touge , Hideki Nara , Takahiro Fujiwara
发明人： Taichiro Touge , Hideki Nara , Takahiro Fujiwara
IPC分类号： C07F7/08
CPC分类号： C07F15/0046 , C07F17/02
摘要： The present invention is to provide a ruthenium complex having a novel arene moiety, which has improved solubility in various solvents, and a method for production thereof.The present invention relates to a novel ruthenium complex having an arene moiety, which has a trisubstituted silyl group introduced to the arene moiety, and a method for production thereof.
摘要翻译：本发明提供一种具有新的芳族部分的钌配合物及其制备方法，其在各种溶剂中的溶解度提高。本发明涉及一种具有引入到芳族部分的三取代甲硅烷基的具有芳烃部分的新型钌络合物及其制备方法。

5. 发明授权

US07964744B2 Method for producing a ruthenium complex 有权
标题翻译：钌络合物的制造方法
公开(公告)号：US07964744B2
公开(公告)日：2011-06-21
申请号：US12540794
申请日：2009-08-13
申请人： Hideki Nara , Noboru Sayo , Takahiro Fujiwara
发明人： Hideki Nara , Noboru Sayo , Takahiro Fujiwara
IPC分类号： C07F15/00
CPC分类号： C07F15/0053
摘要： Provided is a method for producing a ruthenium complex comprises the step of reacting a ruthenium compound represented by general formula (1): [RuX(L)(PP)]X (1), wherein Ru represents a ruthenium atom; X represents a halogen atom; L represents an arene; and PP represents an optically active bisphosphine, with a carboxylate salt represented by general formula (2): R1CO2M (2), wherein M represents a monovalent cation; and R1 represents a group selected from the group consisting of alkyl groups, haloalkyl groups, phenyl groups optionally having a substituent(s), 1-aminoalkyl groups and 1-amino-1-phenylalkyl groups, to produce a ruthenium complex represented by general formula (3): Ru(OCOR1)2(PP) (3), wherein R1 represents the group selected from the group consisting of alkyl groups, haloalkyl groups, phenyl groups optionally having a substituent(s), 1-aminoalkyl groups and 1-amino-1-phenylalkyl groups; and PP represents the optically active bisphosphine.
摘要翻译：提供一种制备钌络合物的方法，包括使通式（1）表示的钌化合物：[RuX（L）（PP）] X（1），其中Ru表示钌原子; X表示卤原子; L代表芳烃; 和PP代表光学活性双膦，与通式（2）表示的羧酸盐：R1CO2M（2），其中M表示一价阳离子; 并且R 1表示选自烷基，卤代烷基，任选具有取代基的苯基，1-氨基烷基和1-氨基-1-苯基烷基的基团，以制备由通式（3）：Ru（OCOR1）2（PP）（3），其中R1表示选自烷基，卤代烷基，任选具有取代基的苯基，1-氨基烷基和1- 氨基-1-苯基烷基; PP代表光学活性双膦。

6. 发明授权

US08658815B2 Method for producing ruthenium complex 有权
标题翻译：钌络合物的制备方法
公开(公告)号：US08658815B2
公开(公告)日：2014-02-25
申请号：US13138709
申请日：2010-03-18
申请人： Takahiro Fujiwara , Hideki Nara
发明人： Takahiro Fujiwara , Hideki Nara
IPC分类号： C07F15/00
CPC分类号： C07F15/0046 , C07F17/02
摘要： The present invention provides a method for inexpensively producing di-μ-chloro-bis[chloro(η6-1-isopropyl-4-methylbenzene)ruthenium (II)] complex used as a catalyst raw material for a hydrogenation or metathesis polymerization reaction at a high yield. In the present invention, the above-described problem can be solved by reacting ruthenium chloride or a hydrate thereof with γ-terpinene in a solvent. In particular, by using an alcohol having a boiling point of 100° C. or higher as a solvent, the yield of the above-described complex can be increased.
摘要翻译：本发明提供了一种低成本生产用作氢化或易位聚合反应的催化剂原料的二氯氯 - 双[氯（eta6-1-异丙基-4-甲苯）钌（II）]络合物的方法，高产。在本发明中，上述问题可以通过使氯化钌或其水合物与γ-萜品烯在溶剂中反应来解决。特别是通过使用沸点为100℃以上的醇作为溶剂，可以提高上述络合物的收率。

7. 发明申请

US20100076210A1 METHOD FOR PRODUCING A RUTHENIUM COMPLEX 有权
标题翻译：生产金属复合材料的方法
公开(公告)号：US20100076210A1
公开(公告)日：2010-03-25
申请号：US12540794
申请日：2009-08-13
申请人： Hideki Nara , Noboru Sayo , Takahiro Fujiwara
发明人： Hideki Nara , Noboru Sayo , Takahiro Fujiwara
IPC分类号： C07F15/00
CPC分类号： C07F15/0053
摘要： Provided is a method for producing a ruthenium complex comprises the step of reacting a ruthenium compound represented by general formula (1): [RuX(L)(PP)]X (1), wherein Ru represents a ruthenium atom; X represents a halogen atom; L represents an arene; and PP represents an optically active bisphosphine, with a carboxylate salt represented by general formula (2): R1CO2M (2), wherein M represents a monovalent cation; and R1 represents a group selected from the group consisting of alkyl groups, haloalkyl groups, phenyl groups optionally having a substituent(s), 1-aminoalkyl groups and 1-amino-1-phenylalkyl groups, to produce a ruthenium complex represented by general formula (3): Ru(OCOR1)2(PP) (3), wherein R1 represents the group selected from the group consisting of alkyl groups, haloalkyl groups, phenyl groups optionally having a substituent(s), 1-aminoalkyl groups and 1-amino-1-phenylalkyl groups; and PP represents the optically active bisphosphine.
摘要翻译：提供一种制备钌络合物的方法，包括使通式（1）表示的钌化合物：[RuX（L）（PP）] X（1），其中Ru表示钌原子; X表示卤原子; L代表芳烃; 和PP代表光学活性双膦，与通式（2）表示的羧酸盐：R1CO2M（2），其中M表示一价阳离子; 并且R 1表示选自烷基，卤代烷基，任选具有取代基的苯基，1-氨基烷基和1-氨基-1-苯基烷基的基团，以制备由通式（3）：Ru（OCOR1）2（PP）（3），其中R1表示选自烷基，卤代烷基，任选具有取代基的苯基，1-氨基烷基和1- 氨基-1-苯基烷基; PP代表光学活性双膦。

8. 发明申请

US20120016148A1 METHOD FOR PRODUCING RUTHENIUM COMPLEX 有权
标题翻译：生产金属复合材料的方法
公开(公告)号：US20120016148A1
公开(公告)日：2012-01-19
申请号：US13138709
申请日：2010-03-18
申请人： Takahiro Fujiwara , Hideki Nara
发明人： Takahiro Fujiwara , Hideki Nara
IPC分类号： C07F15/00
CPC分类号： C07F15/0046 , C07F17/02
摘要： The present invention provides a method for inexpensively producing di-μ-chloro-bis[chloro(η6-1-isopropyl-4-methylbenzene)ruthenium (II)] complex used as a catalyst raw material for a hydrogenation or metathesis polymerization reaction at a high yield. In the present invention, the above-described problem can be solved by reacting ruthenium chloride or a hydrate thereof with γ-terpinene in a solvent. In particular, by using an alcohol having a boiling point of 100° C. or higher as a solvent, the yield of the above-described complex can be increased.
摘要翻译：本发明提供了一种廉价生产用作氢化或易位聚合反应的催化剂原料的二 - 氯 - 双[氯（＆eegr; 6-1-异丙基-4-甲苯）钌（II）]络合物的方法以高产量。在本发明中，上述问题可以通过使氯化钌或其水合物与γ-萜品烯在溶剂中反应来解决。特别是通过使用沸点为100℃以上的醇作为溶剂，可以提高上述络合物的收率。

9. 发明授权

US07038087B2 Process for the production of optically active amino alcohols 失效
标题翻译：用于制备光学活性氨基醇的方法
公开(公告)号：US07038087B2
公开(公告)日：2006-05-02
申请号：US10656617
申请日：2003-09-04
申请人： Takahiro Fujiwara , Hideki Nara , Tsukasa Sotoguchi
发明人： Takahiro Fujiwara , Hideki Nara , Tsukasa Sotoguchi
IPC分类号： C07C209/16 , C07C209/46 , C07C209/56
CPC分类号： C07C269/00 , C07B2200/07 , C07C213/02 , C07C2601/08 , C07C2601/14 , Y02P20/55 , C07C215/44 , C07C271/24
摘要： An object of the present invention is to provide a process for the production of an optically active amino alcohol, particularly an optically active amino alcohol of a trans-form, being excellent in economy and efficiency, and suitable for industry using easily available and less expensive materials.The present invention relates to a process for the production of an optically active amino alcohol comprising the steps that an optically active hydroxy ester in a trans-form obtained by an asymmetric hydrogenation of an easily available β-keto ester is reacted with hydrazine, the resulting optically active hydrazinocarbonyl alcohol is subjected to a Curtius rearrangement in the presence of alcohol and protective group of amino group of the resulting optically active alkoxycarbonylamino alcohol is deprotected. As a result of the process for the production in accordance with the present invention, the objected substance is able to be prepared in a high optical purity and in a high yield.
摘要翻译：本发明的目的是提供一种制备光学活性氨基醇，特别是反式形式的光学活性氨基醇的方法，其经济性和效率优异，并且适用于易于获得和较便宜的工业应用材料本发明涉及一种制备光学活性氨基醇的方法，该方法包括以下步骤：通过易于获得的β-酮酯的不对称氢化获得的反式的光学活性羟基酯与肼反应，得到光学活性肼基羰基醇在醇的存在下进行Curtius重排，并将得到的光学活性烷氧基羰基氨基醇的保护基的氨基脱保护。作为根据本发明的生产方法的结果，可以以高光学纯度和高产率制备被
反应物质。

10. 发明申请

US20140051871A1 RUTHENIUM-DIAMINE COMPLEX AND METHOD FOR PRODUCING OPTICALLY ACTIVE COMPOUND 有权
标题翻译：十二烷基二胺复合物和生产光学活性化合物的方法
公开(公告)号：US20140051871A1
公开(公告)日：2014-02-20
申请号：US14114268
申请日：2012-05-02
申请人： Taichiro Touge , Tomohiko Hakamata , Hideki Nara
发明人： Taichiro Touge , Tomohiko Hakamata , Hideki Nara
IPC分类号： C07F15/00 , C07D311/22 , C07C209/52 , C07C29/143 , C07C41/26
CPC分类号： C07F15/0046 , B01J31/1805 , B01J31/2282 , B01J2231/643 , B01J2531/0205 , B01J2531/0216 , B01J2531/821 , C07B53/00 , C07B2200/07 , C07C29/143 , C07C41/26 , C07C209/52 , C07C2602/12 , C07D311/22 , C07C43/23 , C07C33/20 , C07C33/18 , C07C33/34 , C07C33/22 , C07C33/46 , C07C35/23
摘要： Provided is a ruthenium complex that is represented by general formula (1*) and is useful as an asymmetric reduction catalyst.(In the formula, * is an asymmetric carbon atom; R1 is an arenesulfonyl group, and the like; R2 and R3 are a phenyl group, and the like; R10 through R14 are selected from a hydrogen atom, C1-10 alkyl group, and the like, but R10 through R14 are not simultaneously hydrogen atoms; X is a halogen atom and the like; j and k are each either 0 or 1; and j+k is 0 or 2.)
摘要翻译：提供由通式（1 *）表示的钌络合物，可用作不对称还原催化剂。（式中，*为不对称碳原子，R1为芳烯磺酰基等，R2，R3为苯基等; R10〜R14选自氢原子，C1-10烷基，但R10至R14不同时为氢原子; X为卤素原子等; j和k各自为0或1; j + k为0或2.）

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