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1. 发明授权

US06682784B2 Liquid crystal compositions and liquid crystal display devices 有权
标题翻译：液晶组合物和液晶显示装置
公开(公告)号：US06682784B2
公开(公告)日：2004-01-27
申请号：US10101114
申请日：2002-03-20
申请人： Yasuhiro Kubo , Kanetsugu Terashima
发明人： Yasuhiro Kubo , Kanetsugu Terashima
IPC分类号： C09K1930
CPC分类号： C09K19/46 , C09K19/42 , C09K2019/3009 , C09K2019/301 , C09K2019/3016 , C09K2019/3083 , C09K2019/309 , C09K2019/3092 , Y10T428/10
摘要： Liquid crystal compositions having board nematic phase range, low viscosity, low threshold voltage and large pre-tilt angle, while meeting the general properties required for AM-LCD. The compositions contain at least one of the compounds of the formulas (I-1) to (I-3), at least one of the compounds of the formulas (II-1) to (II-4), at least one of the compounds of the formulas (III-1) and (III-2), at least one of the compounds of the formulas (IV-1) to (IV-3), and optionally at least one of the compounds of the formulas (V-1) and (V-2), as described in the specification.
摘要翻译：具有板向列相范围，低粘度，低阈值电压和大预倾角的液晶组合物，同时满足AM-LCD所需的一般特性。所述组合物含有至少一种式（I-1）至（I-3）的化合物，至少一种式（II-1）至（II-4）的化合物，至少一种式式（Ⅳ-1）至（Ⅳ-3）的化合物中的至少一种，和任选的至少一种式（Ⅴ-Ⅴ）化合物，式 -1）和（V-2），如说明书中所述。

2. 发明授权

US06844032B2 Liquid crystal compounds having bis(trifluoromethyl) phenyl rings, liquid crystal compositions and liquid crystal display devices 有权
标题翻译：具有双（三氟甲基）苯环，液晶组合物和液晶显示装置的液晶化合物
公开(公告)号：US06844032B2
公开(公告)日：2005-01-18
申请号：US10108712
申请日：2002-03-29
申请人： Kazutoshi Miyazawa , Takashi Kato , Yasuhiro Kubo , Kanetsugu Terashima
发明人： Kazutoshi Miyazawa , Takashi Kato , Yasuhiro Kubo , Kanetsugu Terashima
IPC分类号： G02F1/13 , C07C43/225 , C07C69/753 , C07D213/30 , C07D237/08 , C07D239/26 , C07D319/06 , C09K19/04 , C09K19/12 , C09K19/14 , C09K19/20 , C09K19/30 , C09K19/34 , C07D213/78 , C07D239/02
CPC分类号： C09K19/0403 , C09K2019/0407 , Y10T428/10
摘要： The compound (1) having 2,3-bis(trifluoromethyl)-1,4-phenylene is stable chemically and has excellent miscibility with other liquid crystal compounds, large and negative dielectric anisotropy and proper optical anisotropy. A liquid crystal composition comprising the compound has large specific resistance and a large voltage holding ratio, and that the composition is useful for a liquid crystal display element. The compound (1) is represented by formula (1): RaA1—Z1)m—(A2—Z2n—A3—Z3—A4—Rb (1) wherein Ra and Rb independently are alkyl having 1 to 20 carbons, any —CH2— in the alkyl may be replaced by —O—, —S—, —CH═CH—, or —C≡C—, and any hydrogen may be replaced by halogen; A1, A2, A3, and A4 independently are 1,4-cyclohexylene, 1,4-cyclohexenylene, 1,3-dioxane-2,5-diyl, 1,4-phenylene, pyridine-2,5-diyl, pyrimidine-2,5-diyl, pyridazine-3,6-diyl, or 2,3-bis(trifluoromethyl)-1,4-phenylene, any hydrogen in these rings may be replaced by halogen, and at least one of A1, A2, A3, and A4 is 2,3-bis(trifluoromethyl)-1,4-phenylene; Z1, Z2 and Z3 independently are a single bond, —(CH2)2—, —(CF2)2—, —COO—, —OCO—, —CH2O—, —OCH2—, —CF2O—, —OCF2—, —CH═CH—, —CF═CF—, —C≡C—, —(CH2)4—, —(CH2)3O—, or —O(CH2)3—; m and n independently are 0 or 1.
摘要翻译：具有2,3-双（三氟甲基）-1,4-亚苯基的化合物（1）化学稳定且与其它液晶化合物具有优异的混溶性，具有大的和负的介电各向异性和适当的光学各向异性。包含该化合物的液晶组合物具有大的电阻率和较大的电压保持率，并且该组合物可用于液晶显示元件。化合物（1）由式（1）表示：其中R a和R b独立地是具有1至20个碳的烷基，该烷基中的任何-CH 2 - 可以被-O - ， - S - ， - CH = CH- ，或-C = C-，并且任何氢可以被卤素取代; A1，A2，A3和A4独立地为1,4-亚环己基，1,4-亚环己烯基，1,3-二恶烷-2,5-二基，1,4-亚苯基，吡啶-2,5-二基， 2,5-二基，哒嗪-3,6-二基或2,3-双（三氟甲基）-1,4-亚苯基，这些环中的任何氢可以被卤素取代，并且至少一个A1，A2， A3和A4是2,3-双（三氟甲基）-1,4-亚苯基; Z 1，Z 2和Z 3独立地是单键， - （CH 2）2 - ， - （CF 2）2 - ， - COO - ， - OCO - ， - CH 2 O - ， - OCH 2 - ， - CH = CH-，-CF = CF-，-C = C - ， - （CH 2）4 - ， - （CH 2）3 O-或-O（CH 2） m和n独立地为0或1。

3. 发明授权

US06641872B2 Liquid crystal composition and liquid crystal display element 有权
标题翻译：液晶组成和液晶显示元件
公开(公告)号：US06641872B2
公开(公告)日：2003-11-04
申请号：US09985812
申请日：2001-11-06
申请人： Yasuhiro Kubo , Kanetsugu Terashima
发明人： Yasuhiro Kubo , Kanetsugu Terashima
IPC分类号： C09K1934
CPC分类号： C09K19/42 , C09K19/3402 , C09K19/46 , C09K2019/3422 , Y10T428/10
摘要： A liquid crystal composition comprising component I consisting of at least one compound represented by formula (I) and component II consisting at least one compound selected from a group of compounds represented by formulas (II-1) to (II-7): wherein each symbol in the formulas (I) to (II-7) is represented in the specification.
摘要翻译：一种液晶组合物，其包含由至少一种由式（I）表示的化合物和组分II组成的组分，所述组分由至少一种选自式（II-1）至（II-7）表示的化合物的化合物组成：其中每个式（I）〜（II-7）中的符号在说明书中表示。

4. 发明授权

US06703083B2 Silicon compound, liquid crystal composition and liquid crystal display 失效
标题翻译：硅化合物，液晶组合物和液晶显示器
公开(公告)号：US06703083B2
公开(公告)日：2004-03-09
申请号：US10084854
申请日：2002-02-28
申请人： Takashi Kato , Yasuyuki Koizumi , Yasuhiro Kubo , Kanetsugu Terashima
发明人： Takashi Kato , Yasuyuki Koizumi , Yasuhiro Kubo , Kanetsugu Terashima
IPC分类号： C09K1934
CPC分类号： C07F7/0896 , C09K19/406 , Y10T428/10
摘要： Silicon compounds having a low viscosity and a low threshold voltage and improved mutual solubility, a liquid crystal composition comprising the same and a liquid crystal display using the liquid crystal composition. The silicon compound is represented by formula (1): wherein Y1 is, for example, alkylene having 1 to 10 carbon atoms, Y2 is, for example, hydrogen, halogen, —CN, —C≡C—CN, or alkyl having 1 to 10 carbon atoms; A1, A2, A3, and A4 each are, for example, independently 1,4-cyclohexylene, 1,4-cyclohexenylene, 1,4-phenylene, or 1,4-phenylene; Z1, Z2 and Z3 each are independently a single bond, —(CH2)2—, —OCH2—, —CH2O—, —CH═CH—, —C≡C—, —(CH2)4—, —O(CH2)3—, —(CH2)3O—, —COO—, —OCO—, —OCF2—, or —CF2O—; and p and q each are independently 0 or 1.
摘要翻译：具有低粘度和低阈值电压和改善的互溶性的硅化合物，包含该硅化合物的液晶组合物和使用该液晶组合物的液晶显示器。硅化合物由式（1）表示：其中Y 1为例如具有1至10个碳原子的亚烷基，Y 2为例如氢，卤素，-CN，-C = C- CN或具有1至10个碳原子的烷基; A 1，A 2，A 3和A 4各自独立地为1,4-亚环己基，1,4-亚环己烯基，1,4-亚苯基或1,4-亚环己基，亚苯基; Z 1，Z 2和Z 3各自独立地为单键， - （CH 2）2 - ， - OCH 2 - ， - CH 2 O - ， - CH = CH - ， - C = CH2）4-，-O（CH2）3 - ， - （CH2）3O-，-COO-，-OCO-，-OCF2-或-CF2O-; p和q各自独立地为0或1。

5. 发明授权

US07563492B2 Liquid crystal composition and liquid crystal display device 有权
标题翻译：液晶组成和液晶显示装置
公开(公告)号：US07563492B2
公开(公告)日：2009-07-21
申请号：US11598633
申请日：2006-11-14
申请人： Motoki Yanai , Hiroaki Kawashukuda , Shuichi Goto , Yasuhiro Kubo
发明人： Motoki Yanai , Hiroaki Kawashukuda , Shuichi Goto , Yasuhiro Kubo
IPC分类号： C09K19/34 , C09K19/30 , C09K19/12
CPC分类号： C09K19/44 , C09K19/3458 , C09K19/3469 , C09K19/42 , C09K2019/0448 , C09K2019/0451 , C09K2019/123 , C09K2019/3004 , C09K2019/301 , C09K2019/3016 , Y10T428/1036
摘要： A liquid crystal composition having a nematic phase that includes three components, wherein the first component is at least one compound selected from the group of compounds represented by formula (1), the second component is at least one compound selected from the group of compounds represented by formulas (2-1) to (2-3), and the third component is at least one compound selected from the group of compounds represented by formula (3): wherein R1, R2 and R4 are each independently alkyl having 1 to 12 carbons or alkenyl having 2 to 12 carbons; R3 is fluorine, alkyl having 1 to 12 carbons or alkenyl having 2 to 12 carbons; R5 is fluorine, chlorine, alkyl having 1 to 12 carbons or alkenyl having 2 to 12 carbons; R6 is alkenyl having 2 to 12 carbons; Y1 is fluorine, chlorine or trifluoromethoxy; X1, X2, X3 and X4 are each independently hydrogen or fluorine; and one of X5 and X6 is fluorine, and the other is hydrogen.
摘要翻译：一种液晶组合物，其具有向列相，其包含三种成分，其中所述第一成分为选自式（1）所示的化合物的族群中的至少一种化合物，所述第二成分为选自所述化合物组中的至少一种化合物由式（2-1）〜（2-3）表示的化合物，第三成分为选自式（3）所示的化合物中的至少一种化合物：式中，R 1，R 2和R 4各自独立地为具有1〜12的烷基碳或碳数2〜12的烯基; R3是氟，具有1至12个碳的烷基或具有2至12个碳的烯基; R5是氟，氯，具有1至12个碳的烷基或具有2至12个碳的烯基; R6为碳数2〜12的烯基; Y1是氟，氯或三氟甲氧基; X1，X2，X3和X4各自独立地为氢或氟; X5和X6之一是氟，另一个是氢。

6. 发明授权

US06827876B2 Difluoromethyl ether derivative and process for producing the same 有权
标题翻译：二氟甲基醚衍生物及其制备方法
公开(公告)号：US06827876B2
公开(公告)日：2004-12-07
申请号：US10463598
申请日：2003-06-18
申请人： Tomoyuki Kondo , Kouki Sagou , Shuichi Matsui , Hiroyuki Takeuchi , Yasuhiro Kubo , Etsuo Nakagawa
发明人： Tomoyuki Kondo , Kouki Sagou , Shuichi Matsui , Hiroyuki Takeuchi , Yasuhiro Kubo , Etsuo Nakagawa
IPC分类号： C09K1906
CPC分类号： C09K19/3066 , C09K19/20 , C09K19/3402 , C09K19/3458 , C09K19/3469 , C09K19/3491 , C09K19/42 , C09K2019/0466 , C09K2019/3422 , Y10T428/10
摘要： A liquid crystalline compound represented by Formula (1c′): wherein R1 and R2, rings A1, A2, A3, A4 and A5, Z1, Z2, Z3 and Z4, Y1, Y2, Y3 and Y4, and k, l, m and n are as defined in the specification. Also provided is a liquid crystal composition containing at least one of these liquid crystalline compounds.
摘要翻译：由式（1c'）表示的液晶化合物：其中R 1和R 2分别为环A 1，A 2，A 3，A 4和A 5，Z Z 1，Z 2，Z 3和Z 4，Y 1，Y 2，Y 3和Y 4，k，l，m和n如上所定义在规范中。还提供含有这些液晶化合物中的至少一种的液晶组合物。

7. 发明授权

US06649227B2 Difluorovinyl compound, liquid crystal composition and liquid crystal display 有权
标题翻译：二氟乙烯基化合物，液晶组合物和液晶显示
公开(公告)号：US06649227B2
公开(公告)日：2003-11-18
申请号：US09899169
申请日：2001-07-06
申请人： Takashi Kato , Shuichi Matsui , Hiroyuki Takeuchi , Yasuhiro Kubo , Etsuo Nakagawa
发明人： Takashi Kato , Shuichi Matsui , Hiroyuki Takeuchi , Yasuhiro Kubo , Etsuo Nakagawa
IPC分类号： C09K1934
CPC分类号： C07C49/753 , C07C49/687 , C07C49/693 , C07C49/697 , C07D319/06 , C09K19/04 , C09K19/3402 , C09K19/42 , C09K19/44 , C09K19/46 , C09K2019/0448 , C09K2019/0451 , C09K2019/3422 , Y10T428/10
摘要： Provided are liquid crystalline compounds having a wide liquid crystal phase temperature range, low viscosity, a large elastic constant ratio K33/K11 and excellent solubility at low temperature, a liquid crystal composition using the same and a liquid crystal display. Preferred compounds are difluorovinyl compounds represented by Formula (1): wherein Y1, represents H or a straight chain or branched alkyl group having 1 to 10 carbon atoms, and optional —CH2— in the above alkyl group may be replaced by —O— or —CH═CH—, but —O— is not adjacent to each other, and at least one H in Y1 may be substituted with halogen or a cyano group: A1, A2, A3 and A4 each independently represent 1,4-cyclohexylene in which optional —CH2— which is not adjacent to each other may be replaced by —O—, 1,4-phenylene in which optional H may be substituted with halogen, and a single bond, in which at least two of A1, A2, A3 and A4 have the ring structure described above, and at least one of them is 1,4-cyclohexylene in which —CH2— is replaced by —O—; Z1, Z2 and Z3 each independently represent a single bond, —(CH2)2—, —CH═CH—, —(CH2)4—, —O(CH2)3— or —(CH2)3O—; n represents 0 or an integer of 1 to 10, provided that when any of A1, A2, A3 and A4 is 1,4-phenylene, Z1, Z2 and Z3 are single bonds, and among them, when A1 is 1,3-dioxane-2,5-diyl and A2 is 1,4-phenylene and when A3 is 1,4-cyclohexylene and A4 is a single bond, Y1 is H, and n is not 0.
摘要翻译：本发明提供具有宽液晶相温度范围，低粘度，大弹性常数比K33 / K11和低温溶解度优异的液晶化合物，使用该液晶组合物的液晶组合物和液晶显示器。优选的化合物是由式（1）表示的二氟乙烯基化合物：其中Y 1表示H或具有1至10个碳原子的直链或支链烷基，并且上述烷基中任选的-CH 2 - 可以被 - O-或-CH = CH-，但-O-不彼此相邻，并且Y 1中的至少一个H可以被卤素或氰基取代：A 1，A 2， A 3和A 4各自独立地表示1,4-亚环己基，其中不相邻的任选的-CH 2可以被-O-，1,4-亚苯基代替，其中任选的H可以被取代具有卤素和单键，其中A 1，A 2，A 3和A 4中的至少两个具有上述环结构，并且它们中的至少一个为1,4 - 环己烯，其中-CH 2 - 被-O-取代; Z 1，Z 2和Z 3各自独立地表示单键， - （CH 2）2 - ， - CH = CH - ， - （CH 2）4 - ， - O（CH 2）3 - （CH2）3O-; n表示0或1〜10的整数，条件是当A 1，A 2，A 3和A 4中的任何一个为1,4-亚苯基时，Z 1，Z 2 且Z 3为单键，其中A 1为1,3-二恶烷-2,5-二基，A 2为1,4-亚苯基，当A 3为1时，，4-环亚己基和A 4为单键，Y 1为H，n为0。

8. 发明授权

US06500503B2 Cyclohexane derivatives, liquid crystal compositions comprising the same and liquid crystal display devices 有权
标题翻译：环己烷衍生物，含有它们的液晶组合物和液晶显示装置
公开(公告)号：US06500503B2
公开(公告)日：2002-12-31
申请号：US09842254
申请日：2001-04-26
申请人： Koichi Shibata , Shuichi Matsui , Hiroyuki Tekeuchi , Katsuyuki Kawano , Yasuhiro Kubo , Etsuo Nakagawa
发明人： Koichi Shibata , Shuichi Matsui , Hiroyuki Tekeuchi , Katsuyuki Kawano , Yasuhiro Kubo , Etsuo Nakagawa
IPC分类号： C09K1930
CPC分类号： C07D239/26 , C07C17/16 , C07C17/18 , C07C17/2635 , C07C25/18 , C07C25/24 , C07C45/29 , C07C45/513 , C07C255/50 , C07C255/54 , C07C2601/14 , C07D319/06 , C07D339/08 , C09K19/3001 , C09K19/3028 , C09K19/3402 , C09K19/42 , C09K19/44 , C09K19/46 , C09K2019/0448 , C09K2019/0451 , C09K2019/3422 , Y10T428/10 , C07C22/08 , C07C49/813 , C07C47/24
摘要： Liquid crystalline compounds are disclosed which have large dielectric anisotropy and relatively low viscosity, and which are represented by formula (1) wherein R1 represents hydrogen or C1-C15 alkyl in which one or more non-adjacent methylene may be replaced by oxygen, sulfur or —CH═CH— and one or more hydrogen may be replaced by halogen; R2 represents hydrogen, cyano, halogen or C1-C15 alkyl in which one or more non-adjacent methylene may be replaced by oxygen, sulfur or —CH═CH— and one or more hydrogen may be replaced by halogen; L represents halogen or hydrogen; A1, A2, A4 and A5 each independently represent trans-1,4-cyclohexylene or 1,4-phenylene, one or more —CH2— in the trans-1,4-cyclohexylene may be replaced by oxygen or sulfur, one or more ═CH— in the 1,4-phenylene may be replaced by nitrogen, and one or more hydrogen in the 1,4-phenylene ring may be replaced by halogen; A3represents trans-1,4-cyclohexylene in which one or more —CH2— may be replaced by oxygen or sulfur; Z1,Z2,Z3 and Z4 each independently represent —COO—, —OCO—, —CH2CH2—, —(CH2)4—, —CH2O —, —OCH2—, —CF2O—, —OCF2— or a single bond; Q represents —CF2CH2— or —CH2CF2—; and k, l, m and n each independently represent 0 or 1 with the condition of k+l+m+n≦2. Further, liquid crystal compositions comprising at least one liquid crystalline compound of formula (1) and liquid crystal display devices composed of the compositions are disclosed.
摘要翻译：公开了具有大介电各向异性和相对低粘度的液晶化合物，其由式（1）表示，其中R 1表示氢或C 1 -C 15烷基，其中一个或多个不相邻的亚甲基可被氧，硫或 -CH = CH-，一个或多个氢可被卤素取代; R 2表示氢，氰基，卤素或C 1 -C 15烷基，其中一个或多个不相邻的亚甲基可被氧，硫或-CH = CH-代替，并且一个或多个氢可被卤素取代; L表示卤素或氢; A1，A2，A4和A5各自独立地表示反式-1,4-亚环己基或1,4-亚苯基，反式-1,4-亚环己基中的一个或多个-CH 2 - 可被氧或硫代替，一个或多个 = 1,4-亚苯基中的CH-可以被氮代替，1,4-亚苯基环中的一个或多个氢可被卤素取代; A3表示反式-1,4-亚环己基，其中一个或多个-CH 2 - 可被氧或硫取代; Z 1，Z 2，Z 3和Z 4各自独立地表示-COO - ， - OCO - ， - CH 2 CH 2 - ， - （CH 2）4 - ， - CH 2 O - ， - OCH 2 - ， - CF 2 O-，-OCF 2-或单键; Q表示-CF 2 CH 2 - 或-CH 2 CF 2 - ; 并且k，l，m和n各自独立地表示0或1，条件为k + 1 + m + n <= 2。此外，公开了包含至少一种式（1）的液晶化合物和由该组合物组成的液晶显示装置的液晶组合物。

9. 发明授权

US06455852B2 Stable isotope measurement method and apparatus by spectroscopy 有权
公开(公告)号：US06455852B2
公开(公告)日：2002-09-24
申请号：US09929033
申请日：2001-08-15
申请人： Masaaki Mori , Yasuhiro Kubo , Kazunori Tsutsui
发明人： Masaaki Mori , Yasuhiro Kubo , Kazunori Tsutsui
IPC分类号： G01N2135
CPC分类号： G01N21/3504 , G01N33/0006
摘要： A test gas sample containing carbon dioxide 13CO2 as a component gas is introduced into a cell, then the absorbance of light transmitted therethrough at a wavelength suitable for the component gas 13CO2 is determined, and the concentration of the component gas is determined on the basis of a calibration curve prepared through measurement on test gas samples each containing the component gas in a known concentration. Further, the concentration of water vapor contained in the test gas sample is measured, and the concentration of the component gas in the test gas sample is corrected in accordance with the measured water vapor concentration on the basis of a correction curve prepared through measurement on the test gas samples each containing water vapor in a known concentration (FIG. 4). With the spectrometry, the concentration ratio of the component gas can precisely be determined and corrected by measuring the moisture content in the test gas sample.

10. 发明授权

US06325949B1 Liquid crystal composition and liquid crystal display element 有权
标题翻译：液晶组成和液晶显示元件
公开(公告)号：US06325949B1
公开(公告)日：2001-12-04
申请号：US09551641
申请日：2000-04-18
申请人： Fusayuki Takeshita , Etsuo Nakagawa , Yasuhiro Kubo
发明人： Fusayuki Takeshita , Etsuo Nakagawa , Yasuhiro Kubo
IPC分类号： C09K1930
摘要： The present invention provides a liquid crystal composition comprising a component A being at least one compound selected from the group of compounds represented by Formulas (1-1) and (1-2) described in the specification and a component B being at least one compound selected from the group of compounds represented by Formulas (2-1) and (2-2) described in the specification.
摘要翻译：本发明提供一种液晶组合物，其包含成分A为至少一种选自本说明书中所述的由式（1-1）和（1-2）表示的化合物的化合物，组分B为至少一种化合物选自由说明书中描述的式（2-1）和（2-2）表示的化合物组。

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