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1. 发明申请

US20060178525A1 Method for the continuous production of a compound that carries at least two functional groups 有权
公开(公告)号：US20060178525A1
公开(公告)日：2006-08-10
申请号：US10560740
申请日：2004-06-11
申请人： Wolfram Stuer , Jens Scheidel , Hartwig Voss , Peter Bassler , Michael Roper
发明人： Wolfram Stuer , Jens Scheidel , Hartwig Voss , Peter Bassler , Michael Roper
IPC分类号： C07C67/04
CPC分类号： C07C51/36 , C07C51/353 , C07C51/47 , C07C67/303 , C07C67/347 , C07C67/56 , C07C57/13 , C07C55/14 , C07C69/44 , C07C69/593
摘要： A process for continuously preparing a compound which bears at least two functional groups which are each independently selected from the group consisting of nitrile group, carboxylic acid group, carboxylic ester group and carboxamide group, comprising the steps of a) adding two terminal olefins which bear the functional groups required to prepare the compound as per a1) containing at least two functional groups, in the presence of a compound as per a3) which is suitable as a catalyst for this addition and is homogeneous with respect to the reaction mixture to obtain a mixture comprising a1) a compound which is obtained by monoaddition of the two terminal olefins mentioned and bears at least two functional groups which are each independently selected from the group consisting of nitrile group, carboxylic acid group, carboxylic ester group and carboxamide group, a2) a compound which is obtained by polyaddition of the two terminal olefins mentioned and a3) the compound which is suitable as a catalyst for this addition and is homogeneous with respect to the reaction mixture, b) distilling the mixture obtained in step a) to obtain b1) the compound which is obtained by monoaddition of the two terminal olefins mentioned and bears at least two functional groups which are each independently selected from the group consisting of nitrile group, carboxylic acid group, carboxylic ester group and carboxamide group, as the top product and b2) a mixture comprising b2a) a compound which is obtained by monoaddition of the two terminal olefins mentioned and bears at least two functional groups which are each independently selected from the group consisting of nitrile group, carboxylic acid group, carboxylic ester group and carboxamide group, b2b) a compound which is obtained by polyaddition of the two terminal olefins mentioned and b2c) the compound which is suitable as a catalyst for this addition and is homogeneous with respect to the reaction mixture, c) separating the entire mixture obtained in step b2) or a portion thereof by means of a semipermeable membrane to obtain a permeate and a retentate, in such a way that the weight ratio of component b2b) to component b2c) in the mixture b2) fed in step c) is smaller than in the retentate, d) recycling the permeate obtained in step b2) partly or fully into step a) and e) recycling the portion of the mixture obtained in step b2) which has not been separated in c) partly or fully into step a).

2. 发明申请

US20070034576A1 Method for separating a homogeneous catalyst 审中-公开
标题翻译：分离均相催化剂的方法
公开(公告)号：US20070034576A1
公开(公告)日：2007-02-15
申请号：US10561613
申请日：2004-06-11
申请人： Wolfram Stuer , Jens Scheidel , Hartwig Voss , Peter Bassler , Michael Roper
发明人： Wolfram Stuer , Jens Scheidel , Hartwig Voss , Peter Bassler , Michael Roper
IPC分类号： B01D61/00
CPC分类号： C07F15/0073 , C07F15/008
摘要： A process for separating a mixture comprising a) a monoolefinically unsaturated compound which is obtainable by adding two terminal olefins which bear the functional groups required to prepare the monoolefinically unsaturated compound containing at least two functional groups, or a saturated compound obtained by hydrogenating such a compound, b) a compound which is obtainable by adding more than two of the terminal olefins mentioned in a) or a compound obtained by hydrogenating such a compound, and c) a compound which contains a transition metal, is homogeneous with respect to the mixture and is suitable as a catalyst for preparing a monoolefinically unsaturated compound by adding two terminal olefins which bear the functional groups required to prepare the monoolefinically unsaturated compound containing at least two functional groups, by means of a semipermeable membrane to obtain a permeate and a retentate in such a way that the weight ratio of component b) to component c) in the mixture fed to the semipermeable membrane is smaller than in the retentate.
摘要翻译：一种分离混合物的方法，该混合物包含a）单烯属不饱和化合物，其可以通过加入含有制备含有至少两个官能团的单烯属不饱和化合物所需的官能团的二末端烯烃，或通过氢化这种化合物获得的饱和化合物 b）通过添加a）中所述的两种以上的末端烯烃或通过氢化这种化合物得到的化合物得到的化合物，和c）含有过渡金属的化合物相对于混合物是均匀的，通过加入具有制备含有至少两个官能团的单烯属不饱和化合物所需的官能团的二末端烯烃，通过半透膜以制备单烯属不饱和化合物，以获得渗透物和渗余物组分b）与组分c）的重量比在mi中的方式进料到半透膜的切口小于滞留物中的孔。

3. 发明申请

US20070037999A1 Method for isolating a homogeneous catalyst containing rhodium 审中-公开
标题翻译：用于分离含铑的均相催化剂的方法
公开(公告)号：US20070037999A1
公开(公告)日：2007-02-15
申请号：US10561611
申请日：2004-06-19
申请人： Wolfram Stuer , Jens Scheidel , Peter Bassler , Michael Roper
发明人： Wolfram Stuer , Jens Scheidel , Peter Bassler , Michael Roper
IPC分类号： C07C69/52 , C07C69/34 , C07C253/30 , C07C231/14
CPC分类号： C07C67/54 , C07C51/44 , C07C231/24 , C07C253/32 , C07C253/34 , C07C255/08 , C07C255/03 , C07C255/20
摘要： A process for removing a compound which bears at least two functional groups which are each independently selected from the group consisting of nitrile group, carboxylic acid group, carboxylic ester group and carboxamide group, from a mixture which comprises a compound which bears at least two functional groups which are each independently selected from the group consisting of nitrile group, carboxylic acid group, carboxylic ester group and carboxamide group, and a compound which is homogeneous with respect to the mixture and contains rhodium, by distillation.
摘要翻译：从包含至少两个官能团的化合物的混合物的混合物中除去至少两个各自独立地选自腈基，羧酸基，羧酸酯基和羧酰胺基的官能团的化合物的方法，各自独立地选自腈基，羧酸基，羧酸酯基和羧酰胺基的基团，和通过蒸馏相对于混合物均匀并含有铑的化合物。

4. 发明申请

US20060014988A1 Method for the production of 1,6-hexanediol 失效
标题翻译： 1,6-己二醇生产方法
公开(公告)号：US20060014988A1
公开(公告)日：2006-01-19
申请号：US10537829
申请日：2003-12-03
申请人： Rolf-Hartmuth Fischer , Thomas Krug , Andrea Haunert , Michael Roper , Tilman Sirch , Wolfram Stuer
发明人： Rolf-Hartmuth Fischer , Thomas Krug , Andrea Haunert , Michael Roper , Tilman Sirch , Wolfram Stuer
IPC分类号： C07C35/08
CPC分类号： C07C29/177 , C07C31/20
摘要： The present invention provides a process for preparing 1,6-hexanediol having a purity of ≧99.5% by weight by catalytically dimerizing acrylic esters and catalytically hydrogenating the hexenedioic diesters obtained in this way to 1,6-hexanediol by a) dimerizing C1- to C8-acrylic esters in the presence of at least one rhodium compound to give mixtures of predominantly 2- and 3-hexenedioic diesters, b) hydrogenating the resulting dimerizing effluent in the presence of chromium-free catalysts comprising predominantly copper as the hydrogenation component and c) purifying the crude 1,6-hexanediol obtained in this way by fractional distillation.
摘要翻译：本发明提供了一种通过催化二聚丙烯酸酯制备纯度> 99.5％（重量）的1,6-己二醇的方法，并将以这种方式获得的己二酸二酯催化氢化，在至少一种铑化合物的存在下加入到C 8 - 丙烯酸酯中，得到主要为2-和3-己烯二酸二酯的混合物，b）将得到的二聚流出物在主要含有铜作为氢化组分的无铬催化剂的存在下，和c）通过分馏纯化以这种方式得到的粗制1,6-己二醇。

5. 发明申请

US20070083066A1 Method for the production of 1,7-octadiene and use thereof 审中-公开
标题翻译： 1,7-辛二烯的制备方法及其用途
公开(公告)号：US20070083066A1
公开(公告)日：2007-04-12
申请号：US10572077
申请日：2004-09-17
申请人： Volker Bohm , Michael Roper , Jurgen Stephan , Regina Benfer , Markus Schubert , Jorn Karl , Klaus Ebel , Oliver Lober , Martin Volland
发明人： Volker Bohm , Michael Roper , Jurgen Stephan , Regina Benfer , Markus Schubert , Jorn Karl , Klaus Ebel , Oliver Lober , Martin Volland
IPC分类号： C07C45/68 , C07C45/49 , C07C5/08
CPC分类号： C07C49/587 , C07C6/06 , C07C45/50 , C07C45/62 , C07C45/73 , C07C49/385 , C07C2521/04 , C07C2523/20 , C07C2523/28 , C07C2523/30 , C07C2523/36 , C07C2523/74 , C07C11/12 , C07C47/12 , C07C49/12
摘要： The invention relates to a method for the production of 1,7 octadiene by reacting metathesis of cyclohexene with ethylene. The invention also relates to the production of 1,10-decandiol by hydroformulating 1,7 octadiene produced according to said method. The invention further relates to a method for the production of muscone or olefinically unsaturated analogs thereof using 1,10 decandiol which is obtainable in said manner.
摘要翻译：本发明涉及通过使环己烯的复分解与乙烯反应制备1,7辛二烯的方法。本发明还涉及通过根据所述方法制备的1,7辛二烯加氢制备1,10-癸二醇。本发明还涉及使用可以所述方式获得的1,10-癸二醇生产肌醇或其烯属不饱和类似物的方法。

6. 发明申请

US20050143598A1 Method for producing methyl formate 失效
标题翻译：甲酸甲酯的生产方法
公开(公告)号：US20050143598A1
公开(公告)日：2005-06-30
申请号：US10511088
申请日：2003-04-15
申请人： Christoph Adami , Michael Slany , Jorn Karl , Gerd Kaibel , Martin Schafer , Peter Zehner , Michael Roper
发明人： Christoph Adami , Michael Slany , Jorn Karl , Gerd Kaibel , Martin Schafer , Peter Zehner , Michael Roper
IPC分类号： C07C67/36
CPC分类号： C07C67/36 , C07C69/06
摘要： The invention relates to a process for the preparation of methyl formate by reacting methanol with carbon monoxide at a pressure of from 0.5 to 10 MPa abs. and a temperature of from 50 to 150° C. in the presence of a metal alkoxide as catalyst in a reactor, in which a gas stream is withdrawn from the reactor, entrained methyl formate is removed from this gas stream by condensation, and all or some of the remaining gas stream is returned to the reactor as circulating-gas stream and a mean gas superficial velocity of from 1 to 20 cm/s is set in at least one region of the reactor in which the gas flows essentially in one direction.
摘要翻译：本发明涉及一种通过使甲醇与一氧化碳在0.5至10MPa abs的压力下反应制备甲酸甲酯的方法。在反应器中从作为催化剂的金属醇盐存在下的温度为50-150℃，其中将气流从反应器中排出，夹带的甲酸甲酯通过冷凝从该气流中除去，全部或一些剩余的气流作为循环气体流返回到反应器，并且在反应器的至少一个区域中设置1至20cm / s的平均气体空气速度，其中气体基本上在一个方向上流动。

7. 发明授权

US07606221B2 Network communications having endpoint device with automatic connection to iPBX 有权
标题翻译：具有自动连接到iPBX的端点设备的网络通信
公开(公告)号：US07606221B2
公开(公告)日：2009-10-20
申请号：US10996657
申请日：2004-11-24
申请人： Fredric Artru , Andy Huckridge , Marc Petit-Hugenin , Jean-Hugues Robert , Michael Roper , Philip Bednarz
发明人： Fredric Artru , Andy Huckridge , Marc Petit-Hugenin , Jean-Hugues Robert , Michael Roper , Philip Bednarz
IPC分类号： H04L12/66
CPC分类号： G06F21/10
摘要： A telephony communications approach implements an autodiscover feature that enables an endpoint device to automatically locate and establish communication with a desirable server in a web of interconnected servers. In one specific example implementation, the endpoint device is an internet-type telephone communicating with a remotely-located server in an internet-based private branch exchange. Various packet-communicating endpoint devices are adapted to communicate with the internet-based private branch exchange by adapting each to automatically broadcast its identity and, in response to receiving an assignment for the appropriated iPBX, establish communication with the internet-based private branch exchange from other packet-based servers. Other aspects of the invention are directed to approaches for distinguishing the desired internet-based private branch exchange from the other packet-based servers and implementations for assigning the appropriate iPBX.
摘要翻译：电话通信方法实现自动发现功能，其使端点设备能够自动定位并建立与互连服务器的网络中期望的服务器的通信。在一个具体示例实现中，端点设备是在基于因特网的专用小交换机中与位于远程的服务器通信的互联网型电话。各种分组通信端点设备适于通过适应每个分组通信端点设备来自动广播其身份，并且响应于接收到专用iPBX的分配来建立与基于因特网的专用小交换机的通信其他基于包的服务器。本发明的其它方面涉及用于将期望的基于互联网的私人分支交换与其他基于分组的服务器区分开来的方法以及用于分配适当的iPBX的实施方式。

8. 发明申请

US20050010067A1 Preparation for production of formic acid formates 失效
标题翻译：甲酸甲酸盐的制备
公开(公告)号：US20050010067A1
公开(公告)日：2005-01-13
申请号：US10494701
申请日：2002-10-29
申请人： Michael Slany , Martin Schafer , Jorn Karl , Michael Roper
发明人： Michael Slany , Martin Schafer , Jorn Karl , Michael Roper
IPC分类号： A23K1/16 , C07C27/02 , C07C51/09 , C07C51/41 , C07C53/02 , C07C53/06
CPC分类号： C07C51/09 , C07C53/08
摘要： A process is described for preparing acid formates in which methyl formate is reacted with water and a basic compound having a pKa of the conjugate acid of the corresponding dissociation state of ≧3 measured at 25° C. in aqueous solution, the methanol formed is separated off and, optionally, the desired acid content is set by adding formic acid.
摘要翻译：描述了一种制备酸甲酯的方法，其中甲酸甲酯与水反应，并且在25℃下在水溶液中测定的具有相应解离状态为> = 3的共轭酸的pKa的碱性化合物形成的甲醇为分离出来，任选地，通过加入甲酸来设定所需的酸含量。

9. 发明授权

US5892125A Preparation of n-butyraldehyde and/or n-butanol 失效
标题翻译：正丁醛和/或正丁醇的制备
公开(公告)号：US5892125A
公开(公告)日：1999-04-06
申请号：US793480
申请日：1997-07-23
申请人： Jurgen Kanand , Michael Roper , Rocco Paciello , Alfred Thome
发明人： Jurgen Kanand , Michael Roper , Rocco Paciello , Alfred Thome
IPC分类号： C07C27/00 , C07B61/00 , C07C29/00 , C07C29/09 , C07C29/17 , C07C31/12 , C07C45/51 , C07C45/56 , C07C47/02 , C07D295/023
CPC分类号： C07D295/023 , C07C29/00 , C07C45/516 , C07C45/56 , C07C45/562
摘要： A process for the preparation of n-butyraldehyde and/or n-butanol, in whicha) 1,3-butadiene is caused to react with an amine of the formula IR.sup.1 R.sup.2 NH, I in which R.sup.1 and R.sup.2 independently denote hydrogen, optionally substituted aliphatic or cycloaliphatic radicals, or aryl or aralkyl radicals or are linked to form a bridging member which can contain hetero atoms, at elevated temperature and under superatmospheric pressure in the presence of a compound of a Group VIIIb element and in the presence of an alkali metal amide or a basic metal oxide to form a mixture of the adducts of the formulas II ##STR1## and III ##STR2## b) the adduct III is isomerized to the adduct II, c) the adduct II is isomerized in the presence of a homogeneous or heterogeneous transition metal element catalyst in the liquid phase or in the presence of a heterogeneous catalyst containing a transition metal element in the gaseous phase to form the enamine of the formula IV ##STR3## and d) n-butyraldehyde and/or n-butanol is/are produced from this enamine.
摘要翻译： PCT No.PCT / EP95 / 03358 Sec。 371日期1997年7月23日 102（e）日期1997年7月23日PCT 1995年8月24日PCT PCT。出版物WO96 / 07630 日期：1996年3月14日制备正丁醛和/或正丁醇的方法，其中a）使1,3-丁二烯与式ⅠR1R2NH，Ⅰ的胺反应，其中R1和R2独立地为表示氢，任选取代的脂族或脂环族基团，或芳基或芳烷基，或连接形成可含有杂原子的桥连构件，在高温和超大气压下，在VIIIb族元素的化合物存在下，存在碱金属酰胺或碱性金属氧化物以形成式II II和III III的加合物的混合物b）加合物III异构化为加合物II，c）加合物II为在均相或非均相过渡金属元素催化剂存在下在液相中或在气相中含有过渡金属元素的多相催化剂存在下异构化，形成式IV的烯胺IV和d）n -但从该烯胺产生乙醛和/或正丁醇。

10. 发明申请

US20080176782A1 Production of (Co)Surfactants by Reacting Polyols With Olefins 有权
标题翻译：通过与烯烃反应多元醇制备（Co）表面活性剂
公开(公告)号：US20080176782A1
公开(公告)日：2008-07-24
申请号：US11911028
申请日：2006-04-05
申请人： Jurgen Stephan , Michael Roper , Thomas Heidemann , Michael Triller , Jurgen Tropsch
发明人： Jurgen Stephan , Michael Roper , Thomas Heidemann , Michael Triller , Jurgen Tropsch
IPC分类号： C11D1/66 , C07C41/06 , C07C43/13
CPC分类号： C07C41/06 , C07C43/135 , C08G65/329 , C11D1/72 , C11D1/721 , C11D3/3707 , Y02P20/582
摘要： The present invention relates to a process for preparing polyol alkyl ethers by reacting compounds comprising at least three hydroxyl functionalities with olefins in the presence of acidic catalysts at temperatures of from 20 to 250° C. and pressures of from 0.5 to 10 bar, wherein the olefins correspond to the general formula (I) in which R1 is hydrogen and R2 is a linear or branched carbon radical having from 7 to 28 carbon atoms, or R1 and R2 are each linear or branched carbon radicals having from 1 to 27 carbon atoms, the sum of the carbon number of R1 and R2 being at most 28, to polyol alkyl ethers derived from compounds having at least three hydroxyl functionalities, not more than all but one hydroxyl functionality being replaced by a moiety of the general formula (VIII) to the use of these polyol alkyl ethers as surfactants and to laundry detergents and cleaning compositions comprising these polyol alkyl ethers.
摘要翻译：本发明涉及一种制备多元醇烷基醚的方法，该方法是在20至250℃的温度和0.5至10巴的压力下，在酸性催化剂存在下，使包含至少三个羟基官能团的化合物与烯烃反应，烯烃对应于其中R 1为氢且R 2为具有7至28个碳原子的直链或支链碳基团的通式（I），或R' SUP 1和R 2各自为具有1至27个碳原子的直链或支链碳原子，R 1和R 2的碳数之和至少28个的多元醇烷基醚衍生自具有至少三个羟基官能团的化合物，不超过一个羟基官能团，除了一个羟基官能团被通式（VIII）的部分替代为使用的这些多元醇烷基醚作为表面活性剂和洗涤剂和包含这些多元醇烷基醚的清洁组合物。

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