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1. 发明申请

US20060116523A1 Silver-containing catalysts for the reaction of substrates with c-c-double bonds 审中-公开
标题翻译：含有底物与c-c-双键反应的含银催化剂
公开(公告)号：US20060116523A1
公开(公告)日：2006-06-01
申请号：US10541561
申请日：2004-01-09
申请人： Wolfram Stichert , Jens Klein , Stephan Schunk , Dirk Demuth , Andreas Sundermann , Ewald Gallei , Harmut Hibst , Sebastian Storck
发明人： Wolfram Stichert , Jens Klein , Stephan Schunk , Dirk Demuth , Andreas Sundermann , Ewald Gallei , Harmut Hibst , Sebastian Storck
IPC分类号： C07D301/10 , B01J23/50 , B01J23/48
CPC分类号： B01J23/66 , B01J21/04 , B01J23/50 , B01J37/0203 , B01J37/16 , C07D301/10 , C07D303/04
摘要： The present invention relates to a silver-containing catalyst system, which can be applied for the reaction of substrates with at least one C—C-double bond with at least one oxygen-containing or oxygen-supplying component with formation of at least one epoxide. The silver-containing catalyst according to the invention is characterized in that its activity as well as its selectivity is significantly increased with respect to the target product compared with the silver-containing catalysts of the state of the art, as a consequence of the process for the manufacture according to the invention, in which the synthesis of a silver-amine complex is carried out in absence of light and at temperatures below room temperature.
摘要翻译：本发明涉及一种含银催化剂体系，其可以应用于具有至少一个C-C-双键的底物与至少一种含氧或供氧组分的反应，形成至少一种环氧化物。根据本发明的含银催化剂的特征在于，与现有技术的含银催化剂相比，其活性及其选择性相对于目标产物显着增加，这是由于根据本发明的制造，其中银 - 胺络合物的合成在不存在光和低于室温的温度下进行。

2. 发明授权

US07071363B2 Structured catalyst bed 失效
标题翻译：结构催化剂床
公开(公告)号：US07071363B2
公开(公告)日：2006-07-04
申请号：US10617859
申请日：2003-07-14
申请人： Hartmut Hibst , Sebastian Storck , Dirk Demuth , Wolfram Stichert , Jens Klein , Stephan A. Schunk , Andreas Sundermann
发明人： Hartmut Hibst , Sebastian Storck , Dirk Demuth , Wolfram Stichert , Jens Klein , Stephan A. Schunk , Andreas Sundermann
IPC分类号： C07C45/00 , B01J23/48 , B01J23/50
CPC分类号： C07C45/34 , B01J8/0453 , B01J23/002 , B01J23/50 , B01J23/66 , B01J23/8885 , B01J27/1806 , B01J35/0006 , B01J2208/025 , B01J2523/00 , C07C45/58 , C07C47/21 , B01J2523/18 , B01J2523/31 , B01J2523/13 , B01J2523/41 , B01J2523/54 , B01J2523/68 , B01J2523/69 , B01J2523/842 , B01J2523/845 , B01J2523/11 , B01J2523/51
摘要： The invention relates to a novel structured catalyst bed which optionally comprises at least one part bed comprising at least one catalytically active mixture of oxides of the main group metals and transition metals and additionally comprises at least one catalytically active part bed comprising at least silver, at least one alkali metal and a porous support material and finally and necessarily at least one catalytically active part bed comprising at least one alkali metal phosphate and at least one sheet silicate.
摘要翻译：本发明涉及一种新颖的结构化催化剂床，其任选地包含至少一部分床，其包含至少一种主要金属和过渡金属的氧化物的催化活性混合物，并且还包含至少一种至少包含银的催化活性部分床，至少一种碱金属和多孔载体材料，最后并且必需至少一种包含至少一种碱金属磷酸盐和至少一种片状硅酸盐的催化活性部分床。

3. 发明申请

US20070167318A1 Catalytically active composition and the use thereof in dehydration methods 失效
标题翻译：催化活性组合物及其在脱水方法中的应用
公开(公告)号：US20070167318A1
公开(公告)日：2007-07-19
申请号：US10587191
申请日：2005-01-28
申请人： Christian Walsdorff , Thorsten Johann , Beatrice Rossler , Hartmut Hibst , Joaquim Teles , Sebastian Storck , Jens Klein
发明人： Christian Walsdorff , Thorsten Johann , Beatrice Rossler , Hartmut Hibst , Joaquim Teles , Sebastian Storck , Jens Klein
IPC分类号： B01J23/00
CPC分类号： C07C45/65 , B01J23/6445 , B01J23/6447 , B01J23/6522 , B01J23/681 , B01J23/8973 , B01J35/008 , B01J37/0201 , B01J37/0221 , B01J37/03 , C07C47/21 , C07C49/603
摘要： The present invention relates to a catalytically active composition comprising as active component Pd and Bi and at least one element selected from the group (a) consisting of Rh, Au, Sb, V, Cr, W, Mn, Fe, Co, Ni, Na, Cs and Ba, or Pd, Rh and Bi and optionally an element selected from the group (a′) consisting of Au, Sb, V, Cr, W, Mn, Fe, Co, Ni, Pt, Cu, Ag, Na, Cs, Mg, Ca and Ba. The present invention further provides a process for dehydrogenating hydrocarbons, preferably oxo-functionalized hydrocarbons such as cyclopentanone, cyclohexanone and isovaleraldehyde, using the catalytically active composition.
摘要翻译：本发明涉及包含作为活性成分Pd和Bi的至少一种元素的催化活性组合物和选自由Rh，Au，Sb，V，Cr，W，Mn，Fe，Co，Ni组成的组（a）中的至少一种元素， Na，Cs和Ba或Pd，Rh和Bi以及任选的选自Au，Sb，V，Cr，W，Mn，Fe，Co，Ni，Pt，Cu，Ag， Na，Cs，Mg，Ca和Ba。本发明还提供了一种使用催化活性组合物使烃优选氧化官能化烃如环戊酮，环己酮和异戊醛脱氢的方法。

4. 发明授权

US07495132B2 Catalytically active composition and the use thereof in dehydration methods 失效
标题翻译：催化活性组合物及其在脱水方法中的应用
公开(公告)号：US07495132B2
公开(公告)日：2009-02-24
申请号：US10587191
申请日：2005-01-28
申请人： Christian Walsdorff , Thorsten Johann , Beatrice Roessler , Hartmut Hibst , Joaquim Henrique Teles , Sebastian Storck , Jens Klein
发明人： Christian Walsdorff , Thorsten Johann , Beatrice Roessler , Hartmut Hibst , Joaquim Henrique Teles , Sebastian Storck , Jens Klein
IPC分类号： C07C45/65 , B01J23/42
CPC分类号： C07C45/65 , B01J23/6445 , B01J23/6447 , B01J23/6522 , B01J23/681 , B01J23/8973 , B01J35/008 , B01J37/0201 , B01J37/0221 , B01J37/03 , C07C47/21 , C07C49/603
摘要： The present invention relates to a catalytically active composition comprising as active component Pd and Bi and at least one element selected from the group (a) consisting of Rh, Au, Sb, V, Cr, W, Mn, Fe, Co, Ni, Na, Cs and Ba, or Pd, Rh and Bi and optionally an element selected from the group (a′) consisting of Au, Sb, V, Cr, W, Mn, Fe, Co, Ni, Pt, Cu, Ag, Na, Cs, Mg, Ca and Ba. The present invention further provides a process for dehydrogenating hydrocarbons, preferably oxo-functionalized hydrocarbons such as cyclopentanone, cyclohexanone and isovaleraldehyde, using the catalytically active composition.
摘要翻译：本发明涉及包含作为活性成分Pd和Bi的至少一种元素的催化活性组合物和选自由Rh，Au，Sb，V，Cr，W，Mn，Fe，Co，Ni组成的组（a）中的至少一种元素， Na，Cs和Ba或Pd，Rh和Bi以及任选的选自Au，Sb，V，Cr，W，Mn，Fe，Co，Ni，Pt，Cu，Ag， Na，Cs，Mg，Ca和Ba。本发明还提供了一种使用催化活性组合物使烃优选氧化官能化烃如环戊酮，环己酮和异戊醛脱氢的方法。

5. 发明申请

US20080064594A1 Titanium Dioxide Mixtures for Producing Catalysts 失效
标题翻译：用于生产催化剂的二氧化钛混合物
公开(公告)号：US20080064594A1
公开(公告)日：2008-03-13
申请号：US11719422
申请日：2005-04-11
申请人： Samuel Neto , Sebastian Storck , Jurgen Zuhlke , Frank Rosowski
发明人： Samuel Neto , Sebastian Storck , Jurgen Zuhlke , Frank Rosowski
IPC分类号： B01J21/00
CPC分类号： B01J21/063 , B01J23/002 , B01J23/22 , B01J35/0006 , B01J35/1014 , B01J37/0232 , B01J2523/00 , C07C51/265 , C07C51/313 , C07C63/16 , B01J2523/53 , B01J2523/55 , B01J2523/15 , B01J2523/47 , B01J2523/51
摘要： Catalytic titanium dioxide mixtures comprising: a first anatase titanium dioxide having a BET surface area greater than 15 m2/g and a hydrogen uptake for the reduction of Ti4+ to Ti of from 5 to 20 μmol/m2; and a second anatase titanium dioxide having a BET surface area less than or equal to 15 m2/g and a hydrogen uptake for the reduction of Ti4+ to Ti3+ of from 0.6 to 7 μmol/m2, processes for preparing catalysts containing the same, catalysts containing active compositions including such titanium dioxide mixtures on support materials, and catalyst systems using the same.
摘要翻译：催化二氧化钛混合物，其包含：具有大于15m 2 / g的BET表面积的第一锐钛矿二氧化钛和将Ti 4+还原成Ti的氢吸收为5至20mumol / m 2; 和具有小于或等于15m 2 / g的BET表面积的第二锐钛矿二氧化钛和用于还原Ti 4+的氢吸收 0.6〜7μmol/ m 2以上的3+以下，制备含有该催化剂的催化剂的方法，含有活性组合物的催化剂，包括载体材料上的这种二氧化钛混合物，以及使用相同。

6. 发明申请

US20070060758A1 Production of aldehydes, carboxylic acids and/or carboxylic acid anhydrides by means of catalysts containing vanadium oxide, titanium dioxide, and antimony oxide 有权
标题翻译：通过含有氧化钒，二氧化钛和氧化锑的催化剂生产醛，羧酸和/或羧酸酐
公开(公告)号：US20070060758A1
公开(公告)日：2007-03-15
申请号：US10557791
申请日：2004-05-21
申请人： Sebastian Storck , Jurgen Zuhlke , Samuel Neto , Frank Rosowski
发明人： Sebastian Storck , Jurgen Zuhlke , Samuel Neto , Frank Rosowski
IPC分类号： C07D307/89
CPC分类号： C07C51/265 , C07C51/313 , C07C63/16
摘要： A description is given of a process for preparing aldehydes, carboxylic acids and/or carboxylic anhydrides, in particular phthalic anhydride, in which a gaseous stream comprising an aromatic hydrocarbon and molecular oxygen is passed at elevated temperature over a bed of a first catalyst and a bed which is made up of a second catalyst having a higher activity than the first catalyst and is located downstream of the first catalyst in the flow direction of the gaseous stream, wherein the catalytically active composition of the first catalyst comprises at least vanadium oxide, titanium dioxide and antimony oxide and the ratio of vanadium, calculated as V2O5, to antimony, calculated as Sb2O3, in the first catalyst is from 3.5:1 to 5:1. The source of antimony oxide used for the first catalyst is preferably particulate antimony trioxide having a mean particle size of from 0.5 to 5 μm. The process allows the desired oxidation products to be obtained in high yield over longer periods of time.
摘要翻译：给出了制备醛，羧酸和/或羧酸酐，特别是邻苯二甲酸酐的方法的描述，其中包含芳族烃和分子氧的气流在升高的温度下通过第一催化剂的床和床，其由比第一催化剂高的活性的第二催化剂组成，并且位于气流的流动方向上位于第一催化剂的下游，其中第一催化剂的催化活性组合物至少包含氧化钒，钛二氧化锑和氧化锑，以V 2 O 5 5计算的钒与锑的比例计算为Sb 2 O 3 在第一催化剂中为3.5:1至5:1。用于第一催化剂的氧化锑的来源优选是平均粒径为0.5-5微米的颗粒状三氧化锑。该方法允许在较长时间内以高产率获得所需的氧化产物。

7. 发明授权

US07169732B2 Catalyst-precursor for the production of maleic acid anhydride and method for the production thereof 有权
标题翻译：用于生产马来酸酐的催化剂前体及其制备方法
公开(公告)号：US07169732B2
公开(公告)日：2007-01-30
申请号：US10507610
申请日：2003-03-12
申请人： Jens Weiguny , Sebastian Storck , Mark Duda , Cornelia Dobner
发明人： Jens Weiguny , Sebastian Storck , Mark Duda , Cornelia Dobner
IPC分类号： B01J27/18 , C07D307/60
CPC分类号： C07C51/252 , B01J23/002 , B01J27/198 , B01J35/002 , B01J35/1014 , B01J37/0018 , B01J37/031 , B01J2523/00 , C07C51/215 , C07C57/145 , B01J2523/51 , B01J2523/55
摘要： A process for preparing a vanadium, phosphorus, and oxygen catalyst precursor for preparing maleic anhydride by heterogeneously catalyzed gas-phase oxidation of a hydrocarbon having at least four carbon atoms, which comprises (a) reacting vanadium pentoxide with from 102 to 110% strength phosphoric acid in the presence of a primary or secondary, noncyclic or cyclic, unbranched or branched, saturated alcohol having from 3 to 6 carbon atoms in a temperature range from 80 to 160° C.; (b) isolating the precipitate formed; (c) setting an organic carbon content of ≦1.1% by weight in the isolated precipitate by heat treatment in a temperature range from 250 to 350° C., the heat-treated product, following the addition of 3.0% by weight of graphite, giving a powder X-ray diffraction diagram which in the 2θ region features a ratio of the height of the peak of any pyrophosphate phase present at 28.5° to the height of the peak due to the graphite at 26.6° of ≦0.1; and (d) shaping the heat-treated product obtained from step (c) into particles having an averaged diameter of at least 2 mm; a catalyst precursor obtainable from this process; a process for preparing a catalyst from the catalyst precursor; a catalyst obtainable from that process; and also a process for preparing maleic anhydride over that catalyst.
摘要翻译：一种制备用于通过异构催化气相氧化具有至少四个碳原子的烃来制备马来酸酐的钒，磷和氧催化剂前体的方法，其包括（a）使五氧化二钒与102-110％强度的磷酸在80至160℃的温度范围内在具有3至6个碳原子的伯或仲，非环或环状，无支链或支链的饱和醇存在下进行酸反应。（b）分离形成的沉淀物; （c）通过在250-350℃的温度范围内通过热处理将分离的沉淀物中的有机碳含量<= 1.1重量％设定为热处理产物，添加3.0重量％的石墨，给出粉末X射线衍射图，其在2θ区域的特征是存在于28.5°的任何焦磷酸盐相的峰的高度与由于石灰在26.6°<= 0.1处的峰的高度之比; 和（d）将由步骤（c）获得的热处理产物成型为具有至少2mm的平均直径的颗粒; 从该方法获得的催化剂前体; 从催化剂前体制备催化剂的方法; 可从该方法获得的催化剂; 以及在该催化剂上制备马来酸酐的方法。

8. 发明申请

US20060276661A1 Three-layered or four-layered catalyst systems for producing phthalic anhydride 有权
标题翻译：用于生产邻苯二甲酸酐的三层或四层催化剂体系
公开(公告)号：US20060276661A1
公开(公告)日：2006-12-07
申请号：US10557993
申请日：2004-05-15
申请人： Sebastian Storck , Jurgen Zuhike , Samuel Neto , Frank Rosowski
发明人： Sebastian Storck , Jurgen Zuhike , Samuel Neto , Frank Rosowski
IPC分类号： C07D307/89 , B01J21/00
CPC分类号： C07C51/313 , B01J23/002 , B01J23/22 , B01J27/198 , B01J35/0006 , B01J35/10 , B01J35/1009 , B01J35/1014 , B01J2523/00 , C07C51/265 , C07C63/16 , B01J2523/15 , B01J2523/47 , B01J2523/53 , B01J2523/55 , B01J2523/51
摘要： Catalyst systems for preparing phthalic anhydride by means of gas-phase oxidation of o-xylene and/or naphthalene, and a process for preparing phthalic anhydride using the catalyst systems.
摘要翻译：通过邻二甲苯和/或萘的气相氧化制备邻苯二甲酸酐的催化剂体系，以及使用催化剂体系制备邻苯二甲酸酐的方法。

9. 发明申请

US20050222435A1 Catalyst-precursor for the production of maleic acid anhydride and method for the production thereof 失效
标题翻译：用于生产马来酸酐的催化剂前体及其制备方法
公开(公告)号：US20050222435A1
公开(公告)日：2005-10-06
申请号：US10507609
申请日：2003-03-12
申请人： Jens Weiguny , Sebastian Storck , Mark Duda , Cornelia Dobner
发明人： Jens Weiguny , Sebastian Storck , Mark Duda , Cornelia Dobner
IPC分类号： C07D307/60 , B01J27/198 , B01J35/10 , B01J37/00 , B01J37/04 , B01J37/08 , C07B61/00 , C07C51/215 , C07C51/25 , C07D307/34
CPC分类号： C07C51/252 , B01J23/002 , B01J27/198 , B01J35/1014 , B01J35/1038 , B01J37/0009 , B01J37/009 , B01J37/08 , B01J2523/00 , C07C51/215 , C07C57/145 , B01J2523/51 , B01J2523/55
摘要： A process for preparing a vanadium, phosphorus, and oxygen catalyst precursor for preparing maleic anhydride by heterogeneously catalyzed gas-phase oxidation of a hydrocarbon having at least four carbon atoms, by reacting vanadium pentoxide (I) in the presence of a primary or secondary, noncyclic or cyclic, unbranched or branched, saturated alcohol having from 3 to 6 carbon atoms (II) with a pentavalent or trivalent phosphorus compound (III) in a temperature range from 80 to 160° C. with stirring and subsequently filtering the resultant suspension, in which (a) the way in which the phosphorus compound (III) and the vanadium pentoxide (I) are combined in the presence of the alcohol (II), (b) the action of a stirring power of from 0.01 to 0.6 W/kg suspension, and/or (c) the filtration at a temperature from 65° C. to 160° C. are used to set a filtration resistance αH·η of
摘要翻译：通过在一次或二次存在下使五氧化二钒（I）反应，通过使具有至少四个碳原子的烃的非均相催化气相氧化来制备用于制备马来酸酐的钒，磷和氧催化剂前体的方法，具有3至6个碳原子的非环状或环状，无支链或支链的饱和醇（II）与五价或三价磷化合物（III）在80至160℃的温度范围内搅拌并随后过滤得到的悬浮液，其中（a）在醇（II）的存在下将磷化合物（III）和五氧化二钒（I）组合的方式，（b）搅拌功率为0.01至0.6W / kg悬浮液，和/或（c）在65℃至160℃的温度下进行过滤，以设定过滤阻力<50％ / SUP> mPa.s / m 2; 从该方法获得的催化剂前体; 从催化剂前体制备催化剂的方法; 可从该方法获得的催化剂; 以及在该催化剂上制备马来酸酐的方法。

10. 发明授权

US07851398B2 Catalytic titanium dioxide mixtures, catalysts and catalyst systems containing the same, processes for making the same, and uses therefor 有权
标题翻译：催化二氧化钛混合物，催化剂和含有其的催化剂体系，其制备方法及其用途
公开(公告)号：US07851398B2
公开(公告)日：2010-12-14
申请号：US11719422
申请日：2005-11-16
申请人： Samuel Neto , Sebastian Storck , Jürgen Zühlke , Frank Rosowski
发明人： Samuel Neto , Sebastian Storck , Jürgen Zühlke , Frank Rosowski
IPC分类号： B01J27/198 , B01J21/06
CPC分类号： B01J21/063 , B01J23/002 , B01J23/22 , B01J35/0006 , B01J35/1014 , B01J37/0232 , B01J2523/00 , C07C51/265 , C07C51/313 , C07C63/16 , B01J2523/53 , B01J2523/55 , B01J2523/15 , B01J2523/47 , B01J2523/51
摘要： Catalytic titanium dioxide mixtures comprising: a first anatase titanium dioxide having a BET surface area greater than 15 m2/g and a hydrogen uptake for the reduction of Ti4+ to Ti3+ of from 5 to 20 μmol/m2; and a second anatase titanium dioxide having a BET surface area less than or equal to 15 m2/g and a hydrogen uptake for the reduction of Ti4+ to Ti3+ of from 0.6 to 7 μmol/m2, processes for preparing catalysts containing the same, catalysts containing active compositions including such titanium dioxide mixtures on support materials, and catalyst systems using the same.
摘要翻译：催化二氧化钛混合物，其包含：BET表面积大于15m 2 / g的第一锐钛型二氧化钛和用于还原Ti 4+至Ti 3+的氢吸收为5至20μmol/ m 2; 和BET表面积小于或等于15m 2 / g的第二锐钛矿型二氧化钛和用于还原Ti 4+至Ti 3+的氢吸收为0.6〜7μmol/ m 2，制备含有该催化剂的催化剂，含有包含载体材料上的这种二氧化钛混合物的活性组合物和使用其的催化剂体系。

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