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1. 发明申请

US20090165913A1 AMINO ALKOXY-MODIFIED SILSESQUIOXANE ADHESIVES FOR IMPROVED METAL ADHESION AND METAL ADHESION RETENTION TO CURED RUBBER 有权
标题翻译：用于改进金属粘合剂和金属粘合剂固化橡胶的AMINO ALKOXY改性SILSESQUIOXANE粘合剂
公开(公告)号：US20090165913A1
公开(公告)日：2009-07-02
申请号：US12347086
申请日：2008-12-31
申请人： William L. Hergenrother , Walter Tomaszewski , Ashley Hilton , Michael Hayes , James H. Pawlow , Terrence E. Hogan
发明人： William L. Hergenrother , Walter Tomaszewski , Ashley Hilton , Michael Hayes , James H. Pawlow , Terrence E. Hogan
IPC分类号： B60C9/00 , C08G77/26 , B32B15/02 , B32B15/085
CPC分类号： C08K7/06 , B29C66/71 , B29C66/74283 , B29D30/38 , B29D2030/383 , B29D2030/483 , B60C1/00 , B60C2009/0014 , B60C2009/0021 , C08G77/26 , C08G77/28 , C08L21/00 , C09D183/08 , C09J183/08 , D07B1/0666 , Y02P20/582 , Y10T428/31663 , B29K2021/00
摘要： Amino alkoxy-modified silsesquioxanes (amino AMS), and/or amino co-AMS compounds that also comprise a mercaptosilane or a blocked mercaptosilane, are excellent adhesives for coating plated or unplated metal wire for adherence of the wire to a rubber stock. The amino AMS and/or the amino/mercaptan co-AMS adhesives can be used with all types of rubber and there is no requirement for the use of special adhesive additives to the rubber vulcanizates, such as, but not limited to, cobalt, resins and high sulfur levels. In particular, the use of amino AMS and/or amino/mercaptan co-AMS compounds as adhesives for bonding wire to rubber also improves the adherence performance of the reinforcements to obtain sufficient bonding that is resistant to degradation over the course of time, especially resistance to thermal aging and/or thermo-oxidizing aging, in particular corrosion in the presence of water.
摘要翻译：还包含巯基硅烷或封端巯基硅烷的氨基烷氧基改性倍半硅氧烷（氨基AMS）和/或氨基共-MSMS化合物是用于涂覆电镀或未镀覆金属丝的优良粘合剂，用于将线粘附到橡胶原料上。氨基AMS和/或氨基/硫醇共-AMS粘合剂可以与所有类型的橡胶一起使用，并且不需要对橡胶硫化橡胶使用特殊的粘合剂添加剂，例如但不限于钴，树脂和高硫含量。特别地，使用氨基AMS和/或氨基/硫醇共-AMS化合物作为用于将线接合到橡胶上的粘合剂也提高了增强材料的粘附性能，以获得足够的粘合，其耐受在时间上的劣化，特别是电阻热老化和/或热氧化老化，特别是在水存在下的腐蚀。

2. 发明授权

US08642691B2 Amino alkoxy-modified silsesquioxane adhesives for improved metal adhesion and metal adhesion retention to cured rubber 有权
标题翻译：氨基烷氧基改性的倍半硅氧烷粘合剂，用于改善金属粘附和金属粘附保持固化橡胶
公开(公告)号：US08642691B2
公开(公告)日：2014-02-04
申请号：US13174129
申请日：2011-06-30
申请人： William L. Hergenrother , Walter Tomaszewski , Ashley Hilton , Michael Hayes , James H. Pawlow , Terrence E. Hogan , Zhong-Ren Chen
发明人： William L. Hergenrother , Walter Tomaszewski , Ashley Hilton , Michael Hayes , James H. Pawlow , Terrence E. Hogan , Zhong-Ren Chen
IPC分类号： C08K3/08 , B60C1/00
CPC分类号： C08K3/08 , C08G77/26 , C08K5/544 , C09J183/08 , C08L21/00
摘要： Amino alkoxy-modified silsesquioxanes (amino AMS), and/or amino co-AMS compounds that also comprise a mercaptosilane or a blocked mercaptosilane, are excellent adhesives for coating plated or unplated metal wire for adherence of the wire to a rubber stock. The amino AMS and/or the amino/mercaptan co-AMS adhesives can be used with all types of rubber and there is no requirement for the use of special adhesive additives to the rubber vulcanizates, such as, but not limited to, cobalt, resins and high sulfur levels. In particular, the use of amino AMS and/or amino/mercaptan co-AMS compounds as adhesives for bonding wire to rubber also improves the adherence performance of the reinforcements to obtain sufficient bonding that is resistant to degradation over the course of time, especially resistance to thermal aging and/or thermo-oxidizing aging, in particular corrosion in the presence of water. Vulcanized rubber compositions that contain an amino AMS and/or amino/mercaptan co-AMS compound also have improved adhesion to embedded uncoated steel after humidity aging compared with vulcanized rubber compositions not containing the amino alkoxy-modified silsesquioxane.
摘要翻译：还包含巯基硅烷或封端巯基硅烷的氨基烷氧基改性倍半硅氧烷（氨基AMS）和/或氨基辅AMS化合物是用于涂覆电镀或未镀覆金属丝的优良粘合剂，用于将线粘附到橡胶原料上。氨基AMS和/或氨基/硫醇共-AMS粘合剂可以与所有类型的橡胶一起使用，并且不需要对橡胶硫化橡胶使用特殊的粘合剂添加剂，例如但不限于钴，树脂和高硫含量。特别地，使用氨基AMS和/或氨基/硫醇共-AMS化合物作为用于将线接合到橡胶上的粘合剂也提高了增强材料的粘附性能，以获得足够的粘合，其耐受在时间上的劣化，特别是电阻热老化和/或热氧化老化，特别是在水存在下的腐蚀。与不含氨基烷氧基改性的倍半硅氧烷的硫化橡胶组合物相比，含有氨基AMS和/或氨基/硫醇共-AMS化合物的硫化橡胶组合物在湿度老化后也具有改善的对包埋未涂层钢的粘附性。

3. 发明申请

US20120077922A1 Amino Alkoxy-Modified Silsesquioxane Adhesives For Improved Metal Adhesion And Metal Adhesion Retention To Cured Rubber 有权
标题翻译：用于改善金属粘附性和固化橡胶金属粘附保持性的氨基烷氧基改性倍半硅氧烷粘合剂
公开(公告)号：US20120077922A1
公开(公告)日：2012-03-29
申请号：US13174129
申请日：2011-06-30
申请人： William L. Hergenrother , Walter Tomaszewski , Ashley Hilton , Michael Hayes , James H. Pawlow , Terrence E. Hogan , Zhong-Ren Chen
发明人： William L. Hergenrother , Walter Tomaszewski , Ashley Hilton , Michael Hayes , James H. Pawlow , Terrence E. Hogan , Zhong-Ren Chen
IPC分类号： C08K3/08
CPC分类号： C08K3/08 , C08G77/26 , C08K5/544 , C09J183/08 , C08L21/00
摘要： Amino alkoxy-modified silsesquioxanes (amino AMS), and/or amino co-AMS compounds that also comprise a mercaptosilane or a blocked mercaptosilane, are excellent adhesives for coating plated or unplated metal wire for adherence of the wire to a rubber stock. The amino AMS and/or the amino/mercaptan co-AMS adhesives can be used with all types of rubber and there is no requirement for the use of special adhesive additives to the rubber vulcanizates, such as, but not limited to, cobalt, resins and high sulfur levels. In particular, the use of amino AMS and/or amino/mercaptan co-AMS compounds as adhesives for bonding wire to rubber also improves the adherence performance of the reinforcements to obtain sufficient bonding that is resistant to degradation over the course of time, especially resistance to thermal aging and/or thermo-oxidizing aging, in particular corrosion in the presence of water. Vulcanized rubber compositions that contain an amino AMS and/or amino/mercaptan co-AMS compound also have improved adhesion to embedded uncoated steel after humidity aging compared with vulcanized rubber compositions not containing the amino alkoxy-modified silsesquioxane.
摘要翻译：还包含巯基硅烷或封端巯基硅烷的氨基烷氧基改性倍半硅氧烷（氨基AMS）和/或氨基共-MSMS化合物是用于涂覆电镀或未镀覆金属丝的优良粘合剂，用于将线粘附到橡胶原料上。氨基AMS和/或氨基/硫醇共-AMS粘合剂可以与所有类型的橡胶一起使用，并且不需要对橡胶硫化橡胶使用特殊的粘合剂添加剂，例如但不限于钴，树脂和高硫含量。特别地，使用氨基AMS和/或氨基/硫醇共-AMS化合物作为用于将线接合到橡胶上的粘合剂也提高了增强材料的粘附性能，以获得足够的粘合，其耐受在时间上的劣化，特别是电阻热老化和/或热氧化老化，特别是在水存在下的腐蚀。与不含氨基烷氧基改性的倍半硅氧烷的硫化橡胶组合物相比，含有氨基AMS和/或氨基/硫醇共-AMS化合物的硫化橡胶组合物在湿度老化后也具有改善的对包埋未涂层钢的粘附性。

4. 发明授权

US08513371B2 Amino alkoxy-modified silsesquioxanes and method of preparation 有权
标题翻译：氨基烷氧基改性倍半硅氧烷及其制备方法
公开(公告)号：US08513371B2
公开(公告)日：2013-08-20
申请号：US12346994
申请日：2008-12-31
申请人： William L. Hergenrother , Ashley Hilton , Michael Hayes , Walter Tomaszewski , James H. Pawlow , Terrence E. Hogan
发明人： William L. Hergenrother , Ashley Hilton , Michael Hayes , Walter Tomaszewski , James H. Pawlow , Terrence E. Hogan
IPC分类号： C08G77/26
CPC分类号： C08K5/544 , C08G77/26 , C08G77/28 , C08K5/548 , C09D183/08 , Y02T10/862 , Y10T152/10 , Y10T152/10495 , Y10T428/2991 , Y10T428/2995
摘要： An amino alkoxy-modified silsesquioxane (AMS) comprising one or more compounds selected from the group consisting of an amino AMS, an amino/mercaptan co-AMS, an amino/blocked mercaptan co-AMS, mixtures thereof, and a weak acid-neutralized solid or aqueous solution thereof, and a method of making the amino AMS, are presented. The compounds are useful in compounding, processing, cure and storage of silica-reinforced rubbers because they contain low levels of volatile organic compounds (VOC).
摘要翻译：包含一种或多种选自氨基AMS，氨基/硫醇共-AMS，氨基/封端的硫醇共-AMS，及其混合物和弱酸中和的氨基烷氧基改性倍半硅氧烷（AMS）提供其固体或水溶液，以及制备氨基AMS的方法。该化合物可用于二氧化硅增强橡胶的混合，加工，固化和储存，因为它们含有低水平的挥发性有机化合物（VOC）。

5. 发明授权

US08794282B2 Amino alkoxy-modified silsesquioxane adhesives for improved metal adhesion and metal adhesion retention to cured rubber 有权
标题翻译：氨基烷氧基改性的倍半硅氧烷粘合剂，用于改善金属粘附和金属粘附保持固化橡胶
公开(公告)号：US08794282B2
公开(公告)日：2014-08-05
申请号：US12347086
申请日：2008-12-31
申请人： William L. Hergenrother , Walter Tomaszewski , Ashley Hilton , Michael Hayes , James H. Pawlow , Terrence E. Hogan
发明人： William L. Hergenrother , Walter Tomaszewski , Ashley Hilton , Michael Hayes , James H. Pawlow , Terrence E. Hogan
IPC分类号： C08G77/28 , C08L21/00 , B60C1/00
CPC分类号： C08K7/06 , B29C66/71 , B29C66/74283 , B29D30/38 , B29D2030/383 , B29D2030/483 , B60C1/00 , B60C2009/0014 , B60C2009/0021 , C08G77/26 , C08G77/28 , C08L21/00 , C09D183/08 , C09J183/08 , D07B1/0666 , Y02P20/582 , Y10T428/31663 , B29K2021/00
摘要： Amino alkoxy-modified silsesquioxanes (amino AMS), and/or amino co-AMS compounds that also comprise a mercaptosilane or a blocked mercaptosilane, are excellent adhesives for coating plated or unplated metal wire for adherence of the wire to a rubber stock. The amino AMS and/or the amino/mercaptan co-AMS adhesives can be used with all types of rubber and there is no requirement for the use of special adhesive additives to the rubber vulcanizates, such as, but not limited to, cobalt, resins and high sulfur levels. In particular, the use of amino AMS and/or amino/mercaptan co-AMS compounds as adhesives for bonding wire to rubber also improves the adherence performance of the reinforcements to obtain sufficient bonding that is resistant to degradation over the course of time, especially resistance to thermal aging and/or thermo-oxidizing aging, in particular corrosion in the presence of water.
摘要翻译：还包含巯基硅烷或封端巯基硅烷的氨基烷氧基改性倍半硅氧烷（氨基AMS）和/或氨基辅AMS化合物是用于涂覆电镀或未镀覆金属丝的优良粘合剂，用于将线粘附到橡胶原料上。氨基AMS和/或氨基/硫醇共-AMS粘合剂可以与所有类型的橡胶一起使用，并且不需要对橡胶硫化橡胶使用特殊的粘合剂添加剂，例如但不限于钴，树脂和高硫含量。特别地，使用氨基AMS和/或氨基/硫醇共-AMS化合物作为用于将线接合到橡胶上的粘合剂也提高了增强材料的粘附性能，以获得足够的粘合，其耐受在时间上的劣化，特别是电阻热老化和/或热氧化老化，特别是在水存在下的腐蚀。

6. 发明申请

US20090203929A1 AMINO ALKOXY-MODIFIED SILSESQUIOXANES AND METHOD OF PREPARATION 有权
标题翻译：氨基改性硅烷氧化物及其制备方法
公开(公告)号：US20090203929A1
公开(公告)日：2009-08-13
申请号：US12346994
申请日：2008-12-31
申请人： William L. Hergenrother , Ashley Hilton , Michael Hayes , Walter Tomaszewski , James H. Pawlow , Terrence E. Hogan
发明人： William L. Hergenrother , Ashley Hilton , Michael Hayes , Walter Tomaszewski , James H. Pawlow , Terrence E. Hogan
IPC分类号： C07F7/02
CPC分类号： C08K5/544 , C08G77/26 , C08G77/28 , C08K5/548 , C09D183/08 , Y02T10/862 , Y10T152/10 , Y10T152/10495 , Y10T428/2991 , Y10T428/2995
摘要： An amino alkoxy-modified silsesquioxane (AMS) comprising one or more compounds selected from the group consisting of an amino AMS, an amino/mercaptan co-AMS, an amino/blocked mercaptan co-AMS, mixtures thereof, and a weak acid-neutralized solid or aqueous solution thereof, and a method of making the amino AMS, are presented. The compounds are useful in compounding, processing, cure and storage of silica-reinforced rubbers because they contain low levels of volatile organic compounds (VOC).
摘要翻译：包含一种或多种选自氨基AMS，氨基/硫醇共-AMS，氨基/封端的硫醇共-AMS，及其混合物和弱酸中和的氨基烷氧基改性倍半硅氧烷（AMS）提供其固体或水溶液，以及制备氨基AMS的方法。该化合物可用于二氧化硅增强橡胶的混合，加工，固化和储存，因为它们含有低水平的挥发性有机化合物（VOC）。

7. 发明申请

US20120252979A1 Process for Producing Blends of Syndiotactic, 1,2-Polybutadiene and Rubbery Elastomers 审中-公开
标题翻译：制备间同立构1,2-二丁二烯和橡胶弹性体共混物的方法
公开(公告)号：US20120252979A1
公开(公告)日：2012-10-04
申请号：US13305219
申请日：2011-11-28
申请人： Christine Rademacher , Steven Luo , Zhong-Ren Chen , Walter Tomaszewski , Edward Kelley
发明人： Christine Rademacher , Steven Luo , Zhong-Ren Chen , Walter Tomaszewski , Edward Kelley
IPC分类号： C08L9/00 , C08L7/00
CPC分类号： C09D151/003 , C08F236/06 , C08F255/06 , C08F279/02 , C08F287/00 , C08L7/00 , C08L9/00 , C08L23/16 , C08L51/006 , C08L51/04 , C08L2312/00 , C08L2666/02 , C09J151/003 , Y10T152/10495 , C08F4/70 , C08L2666/06 , C08L2666/08 , C08L2666/04
摘要： Blends of syndiotactic 1,2-polybutadiene and rubbery elastomers are prepared by a process that comprises polymerizing 1,3-butadiene monomer into syndiotactic 1,2-polybutadiene within a rubber cement of an elastomeric terpolymer by using a chromium-based, molybdenum-based, or iron-based catalyst composition. Polymer composition comprising the blend with improved properties is also provided.
摘要翻译：间同立构1,2-聚丁二烯和橡胶状弹性体的共混物是通过一种方法制备的，该方法包括通过使用基于铬的钼基，将1,3-丁二烯单体聚合成弹性体三元共聚物的橡胶胶泥内的间同立构1,2-聚丁二烯，或铁基催化剂组合物。还提供了包含具有改进性质的共混物的聚合物组合物。

8. 发明申请

US20090032162A1 BELT ASSEMBLIES AND PNEUMATIC TIRES INCLUDING THE SAME 审中-公开
标题翻译：皮带组装和气动轮胎，包括它们
公开(公告)号：US20090032162A1
公开(公告)日：2009-02-05
申请号：US12184794
申请日：2008-08-01
申请人： Xiao-Dong Pan , Walter Tomaszewski , Edward D. Kelly
发明人： Xiao-Dong Pan , Walter Tomaszewski , Edward D. Kelly
IPC分类号： B60C9/18 , C08K5/13
CPC分类号： C08K5/55 , B60C9/2006 , C08K5/0025 , C08K5/098 , C08K5/13 , C08K5/34922 , Y10T152/1081 , C08L21/00
摘要： A pneumatic tire comprising a carcass, a tread assembly, a sidewall assembly, and a belt assembly, where the belt assembly includes at least one reinforcing element disposed within a matrix, where the matrix is a vulcanizate prepared from a skim stock prepared by combining an elastomer, a filler, a curative, a methylene donor, and a phenol derivative.
摘要翻译：一种包括胎体，胎面组件，侧壁组件和带组件的充气轮胎，其中所述带组件包括设置在基质内的至少一个增强元件，其中所述基质是由通过组合弹性体，填料，固化剂，亚甲基供体和苯酚衍生物。

9. 发明授权

US08067503B2 Process for producing blends of syndiotactic, 1,2-polybutadiene and rubbery elastomers 有权
标题翻译：制备间同立构，1,2-聚丁二烯和橡胶弹性体的共混物的方法
公开(公告)号：US08067503B2
公开(公告)日：2011-11-29
申请号：US11625976
申请日：2007-01-23
申请人： Christine Rademacher , Steven Luo , Zhong-Ren Chen , Walter Tomaszewski , Edward Kelley
发明人： Christine Rademacher , Steven Luo , Zhong-Ren Chen , Walter Tomaszewski , Edward Kelley
IPC分类号： B60C1/00
CPC分类号： C09D151/003 , C08F236/06 , C08F255/06 , C08F279/02 , C08F287/00 , C08L7/00 , C08L9/00 , C08L23/16 , C08L51/006 , C08L51/04 , C08L2312/00 , C08L2666/02 , C09J151/003 , Y10T152/10495 , C08F4/70 , C08L2666/06 , C08L2666/08 , C08L2666/04
摘要： Blends of syndiotactic 1,2-polybutadiene and rubbery elastomers are prepared by a process that comprises polymerizing 1,3-butadiene monomer into syndiotactic 1,2-polybutadiene within a rubber cement of an elastomeric terpolymer by using a chromium-based, molybdenum-based, or iron-based catalyst composition. Polymer composition comprising the blend with improved properties is also provided.
摘要翻译：间同立构1,2-聚丁二烯和橡胶状弹性体的共混物是通过一种方法制备的，该方法包括通过使用基于铬的钼基，将1,3-丁二烯单体聚合成弹性体三元共聚物的橡胶胶泥内的间同立构1,2-聚丁二烯，或铁基催化剂组合物。还提供了包含具有改进性质的共混物的聚合物组合物。

10. 发明授权

US5350470A Method of forming tire bead assembly 失效
标题翻译：形成轮胎胎圈组件的方法
公开(公告)号：US5350470A
公开(公告)日：1994-09-27
申请号：US159419
申请日：1993-11-30
申请人： Virgil D. Mochel , Walter Tomaszewski , Georg G. A. Bohm
发明人： Virgil D. Mochel , Walter Tomaszewski , Georg G. A. Bohm
IPC分类号： B29D30/18 , B29D30/32 , B29D30/48 , B60C15/06
CPC分类号： B29D30/48 , B60C15/06 , B29D2030/482
摘要： A method of forming a bead assembly for use in a pneumatic tire includes extruding a strip of green elastomeric material onto a split or pair of steel supporting guide ring where the ends of the extruded strip are cut at a bias angle and then spliced together to form an annular elastomeric member. The extruded strip and formed annular member has a pair of tapered longitudinal end members joined by a central recess. An annular tire bead is placed in radial alignment about the central recess of the annular member. Next, a segmented mandrel carrying inflatable turnup bladders is expanded outwardly, afterwhich the split guide ring is axially withdrawn. The mandrel and bladders then provide the support for the elastomeric member previously provided by the split annular ring, and traps the bead within the central recess. The two longitudinal end members of the extruded strip are then turned up about the bead by inflating the bladders to form the bead assembly, afterwhich the assembly is placed in a shaping mold. If desired, an annular strip of reinforcing material may be placed concentrically about the bead before the end members are turned up about the bead, to provide internal reinforcement for the bead assembly.
摘要翻译：一种形成用于充气轮胎的胎圈组件的方法包括将绿色弹性体材料条挤出到分开或一对钢支撑导向环上，其中挤压条的端部以偏压角切割，然后拼接在一起形成环形弹性构件。挤出的条带和成形的环形构件具有通过中心凹部连接的一对锥形纵向端部构件。环形轮胎胎圈围绕环形构件的中心凹槽放置成径向对准。接下来，承载充气翻转气囊的分段心轴向外扩张，之后分离导向环被轴向拉出。然后心轴和气囊为先前由分割的环形环提供的弹性体构件提供支撑，并将胎圈收集在中心凹部内。然后通过使气囊膨胀以形成胎圈组件，然后将组件放置在成型模具中，将挤出的带材的两个纵向端部构件围绕胎圈卷起。如果需要，在端部构件围绕胎圈卷起之前，增强材料的环形带可以围绕胎圈同心地放置，以为胎圈组件提供内部加强。

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