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1. 发明授权

US3948872A Polymerization process for producing low cis-configuration homopolymers 失效
标题翻译：用于生产低顺式构型均聚物的聚合方法
公开(公告)号：US3948872A
公开(公告)日：1976-04-06
申请号：US109684
申请日：1971-01-25
申请人： William J. Trepka , Ralph C. Farrar
发明人： William J. Trepka , Ralph C. Farrar
IPC分类号： C08F136/04 , C08F136/06
CPC分类号： C08F136/04
摘要： A polymerization process for preparing homopolymers of conjugated dienes having decreased cis-content resulting from the use of organolithium compounds as initiators wherein 1,2-dialkoxybenzene is introduced in a quantity sufficient to decrease the cis-content of the homopolymers formed.
摘要翻译：用于制备由使用有机锂化合物作为引发剂而导致的顺式含量降低的共聚二烯的均聚物的聚合方法，其中引入1,2-二烷氧基苯的量足以降低所形成的均聚物的顺式含量。

2. 发明授权

US5705569A Block copolymers of monovinylarenes and conjugated dienes and preparation thereof 失效
标题翻译：单乙烯基芳烃和共轭二烯的嵌段共聚物及其制备
公开(公告)号：US5705569A
公开(公告)日：1998-01-06
申请号：US651082
申请日：1996-05-22
申请人： George A. Moczygemba , Larry L. Nash , William J. Trepka , Craig D. DePorter , Nathan E. Stacy , Ralph C. Farrar , Charles M. Selman
发明人： George A. Moczygemba , Larry L. Nash , William J. Trepka , Craig D. DePorter , Nathan E. Stacy , Ralph C. Farrar , Charles M. Selman
IPC分类号： C08F297/04 , C08L53/02
CPC分类号： C08F297/044
摘要： A method for preparing resinous polymodal monovinylarene-conjugated diene block copolymers and polymers produced thereby are provided. The method comprises sequentially contacting under polymerization conditions: (a) a monovinylarene monomer and initiator; (b) initiator and a monovinylarene monomer; (c) a sequence of at least two charges selected from the group consisting of (i) initiator and a monovtnylarene monomer, (ii) a mixture of monovtnylarene monomer and conjugated diene monomor, (iii) a conjugated diene monomer, (iv) a monovinylarene monomer; (d) a coupling agent; wherein the sequence of at least two charges in step (c) can be made in any order. In a preferred embodiment, at least three Initiator charges are provided. In another preferred embodiment, at least three monovinylarene charges precede the first charge containing conjugated diene. In another preferred embodiment, at least four monovinylarene charges precede the first charge containing conjugated diene.
摘要翻译：提供了一种制备树脂多聚单乙烯基芳烃 - 共轭二烯嵌段共聚物和由此制备的聚合物的方法。该方法包括在聚合条件下依次接触：（a）单乙烯基芳烃单体和引发剂; （b）引发剂和单乙烯基芳烃单体; （c）选自（i）引发剂和单甲苯基芳烃单体的至少两种电荷的序列，（ii）单甲苯基芳烃单体和共轭二烯单体的混合物，（iii）共轭二烯单体，（iv）单乙烯基芳烃单体; （d）偶联剂; 其中步骤（c）中的至少两个电荷的顺序可以以任何顺序制成。在优选实施方案中，提供至少三种引发剂电荷。在另一个优选实施方案中，至少三种单乙烯基芳烃电荷位于含有共轭二烯的第一电荷之前。在另一个优选的实施方案中，至少四种单乙烯基芳烃电荷位于含有共轭二烯的第一电荷之前。

3. 发明授权

US5436298A Block copolymers of monovinylarenes and conjugated dienes and preparation thereof 失效
标题翻译：单乙烯基芳烃和共轭二烯的嵌段共聚物及其制备
公开(公告)号：US5436298A
公开(公告)日：1995-07-25
申请号：US308240
申请日：1994-09-19
申请人： George A. Moczygemba , Larry L. Nash , William J. Trepka , Craig D. DePorter , Nathan E. Stacy , Ralph C. Farrar , Charles M. Selman
发明人： George A. Moczygemba , Larry L. Nash , William J. Trepka , Craig D. DePorter , Nathan E. Stacy , Ralph C. Farrar , Charles M. Selman
IPC分类号： C08F297/04
CPC分类号： C08F297/044
摘要： A method for preparing resinous polymodal monovinylarene-conjugated diene block copolymers and polymers produced thereby are provided. The method comprises sequentially contacting under polymerization conditions:(a) a monovinylarene monomer and initiator;(b) initiator and a monovinylarene monomer;(c) a sequence of at least two charges selected from the group consisting of (i) initiator and a monovinylarene monomer, (ii) a mixture of monovinylarene monomer and conjugated diene monomer, (iii) a conjugated diene monomer, (iv) a monovinylarene monomer;(d) s coupling agent;wherein the sequence of at least two charges in step (c) can be made in any order. In a preferred embodiment, at least three initiator charges are provided. In another preferred embodiment, at east three monovinylarene charges precede the first charge containing conjugated diene. In another preferred embodiment, at least four monovinylarene charges precede the first charge containing conjugated diene.
摘要翻译：提供了一种制备树脂多聚单乙烯基芳烃 - 共轭二烯嵌段共聚物和由此制备的聚合物的方法。该方法包括在聚合条件下依次接触：（a）单乙烯基芳烃单体和引发剂; （b）引发剂和单乙烯基芳烃单体; （c）选自（i）引发剂和单乙烯基芳烃单体的至少两种电荷的序列，（ii）单乙烯基芳烃单体和共轭二烯单体的混合物，（iii）共轭二烯单体，（iv）单乙烯基芳烃单体; （d）偶联剂; 其中步骤（c）中的至少两个电荷的顺序可以以任何顺序制成。在优选的实施方案中，提供至少三种引发剂电荷。在另一个优选的实施方案中，在东部三乙烯基芳烃电荷位于含有共轭二烯的第一电荷之前。在另一个优选的实施方案中，至少四种单乙烯基芳烃电荷位于含有共轭二烯的第一电荷之前。

4. 发明授权

US4250270A Solution polymerization with molecular sieve purification of recycled solvent 失效
标题翻译：溶液聚合用分子筛纯化回收溶剂
公开(公告)号：US4250270A
公开(公告)日：1981-02-10
申请号：US81949
申请日：1979-10-04
申请人： Ralph C. Farrar
发明人： Ralph C. Farrar
IPC分类号： C08F2/06 , C08F36/04 , C08G81/02
CPC分类号： C08G81/022 , C08F36/04
摘要： In the solution polymerization process wherein monomers comprising at least one conjugated diene are polymerized followed by coupling with a polyfunctional coupling agent which results in some alkyl chloride formation and solvent recovered from said polymerization is used in a subsequent solution polymerization process, the improvement comprising contacting said solvent with a molecular sieve to remove alkyl chloride therefrom before said solvent is used in said subsequent polymerization.
摘要翻译：在溶液聚合过程中，其中包含至少一个共轭二烯的单体聚合，然后与导致一些烷基氯形成的多官能偶联剂偶联，并且从所述聚合反应回收的溶剂用于随后的溶液聚合过程中，改进包括使所述溶剂用分子筛除去其中的所述溶剂，然后在所述后续聚合中使用所述溶剂。

5. 发明授权

US4145498A Addition of coupling agent during organolithium initiated polymerizations 失效
标题翻译：在有机锂引发聚合过程中加入偶联剂
公开(公告)号：US4145498A
公开(公告)日：1979-03-20
申请号：US762691
申请日：1977-01-26
申请人： Ralph C. Farrar
发明人： Ralph C. Farrar
IPC分类号： C08C19/44 , C08F12/02 , C08F36/04 , C08F4/08 , C08F4/16 , C08F36/06 , C08F36/08
CPC分类号： C08F36/04 , C08C19/44 , C08F12/02 , Y10S526/919
摘要： Continuous or incremental addition of a coupling agent, such as silicon tetrachloride, during the polymerization step of organolithium initiated polymerization processes results in polymers of improved processability, as well as other improved properties such as high green strength, low die swell, and minimal shrinkage on extrusion.
摘要翻译：在有机锂引发的聚合方法的聚合步骤期间连续或递增地加入偶联剂，例如四氯化硅，导致聚合物具有改进的加工性能，以及其它改进的性能，例如高生坯强度，低模量膨胀和最小收缩率挤压。

6. 发明授权

US4377666A Age-resistant polymers containing chemically bound antioxidant functional groups 失效
标题翻译：含有化学结合的抗氧化剂官能团的抗老化聚合物
公开(公告)号：US4377666A
公开(公告)日：1983-03-22
申请号：US293737
申请日：1981-08-17
申请人： Ralph C. Farrar
发明人： Ralph C. Farrar
IPC分类号： C08C19/44 , C08F8/00 , C08F8/32
CPC分类号： C08C19/44
摘要： Conjugated diene homo- or copolymers having chemically bound antioxidant functional groups are prepared by the reaction of polymer-alkali metal with certain antioxidants containing a functional group reactable polymer-alkali metal, providing both coupling and bound anti-oxidant groups. These polymers having antioxidant functional groups chemically attached into the polymer chain have better aging stability than similar polymers containing non-bound antioxidants.
摘要翻译：具有化学结合的抗氧化剂官能团的共轭二烯均聚物或共聚物通过聚合物 - 碱金属与含有官能团可反应聚合物 - 碱金属的某些抗氧化剂的反应制备，提供偶联和结合的抗氧化剂基团。具有化学连接到聚合物链中的抗氧化官能团的这些聚合物具有比含有非结合抗氧化剂的类似聚合物更好的时效稳定性。

7. 发明授权

US4020258A Addition of coupling agent during organolithium initiated polymerizations 失效
标题翻译：在有机锂引发聚合过程中加入偶联剂
公开(公告)号：US4020258A
公开(公告)日：1977-04-26
申请号：US447203
申请日：1974-03-01
申请人： Ralph C. Farrar
发明人： Ralph C. Farrar
IPC分类号： C08C19/44 , C08F12/02 , C08F36/04 , C08F4/08 , C08F4/16
CPC分类号： C08F36/04 , C08C19/44 , C08F12/02
摘要： Continuous or incremental addition of a coupling agent, such as silicon tetrachloride, during the polymerization step of organolithium initiated polymerization processes results in polymers of improved processability, as well as other improved properties such as high green strength, low die swell, and minimal shrinkage on extrusion.
摘要翻译：在有机锂引发的聚合方法的聚合步骤期间连续或递增地加入偶联剂，例如四氯化硅，导致聚合物具有改进的加工性能，以及其它改进的性能，例如高生坯强度，低模量膨胀和最小收缩率挤压。

8. 发明授权

US4414340A Thermosetting compositions 失效
标题翻译：热固性组合物
公开(公告)号：US4414340A
公开(公告)日：1983-11-08
申请号：US466691
申请日：1983-02-15
申请人： Guy Senatore , Ralph C. Farrar
发明人： Guy Senatore , Ralph C. Farrar
IPC分类号： C08C19/44 , C08K3/26 , C08K5/14 , C08L9/00 , C08L23/12 , C08L23/22 , C08K3/40 , C08K3/22
CPC分类号： C08K5/14 , C08C19/44 , C08L9/00 , C08K3/26 , C08L23/12 , C08L23/22
摘要： A thermosetting composition exhibiting improved physical properties and little or no blistering is provided consisting essentially of a CO.sub.2 or O.sub.2 terminated high vinyl alkadiene polymer, an inorganic filler, an organic peroxide compound, and a polyolefin modifier.
摘要翻译：提供基本上由CO 2或O 2封端的高乙烯基链二烯聚合物，无机填料，有机过氧化物化合物和聚烯烃改性剂组成的具有改善的物理性能和很少或不起泡的热固性组合物。

9. 发明授权

US4091198A Suppressing gel in the continuous solution polymerization of a conjugated diene with a monovinyl aromatic compound 失效
标题翻译：在共轭二烯与单乙烯基芳族化合物的连续溶液聚合中抑制凝胶
公开(公告)号：US4091198A
公开(公告)日：1978-05-23
申请号：US722195
申请日：1976-09-10
申请人： Richard L. Smith , Ralph C. Farrar , Daniel H. Willis
发明人： Richard L. Smith , Ralph C. Farrar , Daniel H. Willis
IPC分类号： C08F2/00 , C08F2/04 , C08F2/06 , C08F2/38 , C08F4/00 , C08F4/42 , C08F4/56 , C08F36/00 , C08F236/00 , C08F236/10 , C08F4/58
CPC分类号： C08F236/10
摘要： Gel formation in the first reactor means of a multireactor process is suppressed by the employment of a silicon halide in the first reactor means in an organolithium-initiated, solution-polymerized, randomized, conjugated diene/monovinyl-substituted aromatic compound copolymerization.
摘要翻译：通过在有机锂引发的，溶液聚合的，随机的，共轭二烯/单乙烯基取代的芳族化合物共聚合中的第一反应器装置中使用卤化硅来抑制多反应器方法的第一反应器装置中的凝胶形成。

10. 发明授权

US4311803A Continuous solution polymerization process 失效
标题翻译：连续溶液聚合工艺
公开(公告)号：US4311803A
公开(公告)日：1982-01-19
申请号：US181516
申请日：1980-08-26
申请人： Richard L. Smith , Ralph C. Farrar , Richard J. Sonnenfeld
发明人： Richard L. Smith , Ralph C. Farrar , Richard J. Sonnenfeld
IPC分类号： C08F36/04 , C08F8/00 , C08C19/00 , C08F8/42
CPC分类号： C08F36/04
摘要： A continuous solution polymerization process for polymerizing conjugated dienes alone or with a copolymerizable monovinylarene in the presence of a gel inhibitor employing a first stirred reactor in series with a following plug-flow tube reactor.
摘要翻译：一种用于在凝胶抑制剂存在下单独或与可共聚单乙烯基芳烃聚合的连续溶液聚合方法，该溶液采用第一搅拌反应器与下列活塞流反应器串联。

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