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    • 2. 发明授权
    • Measurement of isotope ratios in complex matrices
    • 复杂基质中同位素比的测量
    • US09128076B2
    • 2015-09-08
    • US13641658
    • 2011-01-06
    • William A. LambertiHubert E. KingWilliam C. HornMindy M. ZimmerGordon MacleodRobert J. PottorfLeonard J. Srnka
    • William A. LambertiHubert E. KingWilliam C. HornMindy M. ZimmerGordon MacleodRobert J. PottorfLeonard J. Srnka
    • G01N33/24
    • G01N33/241
    • The present techniques are directed to a method for microprobe analyses of isotope ratios in inhomogeneous matrices. The method includes selecting matrix standards that have matrices that resemble a target matrix. A bulk isotope analysis is run on each of the matrix standards to determine a bulk isotope ratio value. A microprobe analysis is run on each of the matrix standards to determine a microprobe isotope ratio values for each of the plurality of matrix standards. Spurious values are eliminated from the microprobe isotope ratio values. The microprobe isotope ratio values are averaged for each of the matrix standards to create an average microprobe isotope ratio value associated with each of the matrix standards. The bulk isotope ratio value for each of matrix standards is plotted against the average microprobe isotope ratio value associated with each of the matrix standards to create a matrix corrected calibration curve.
    • 本技术涉及用于非均匀基质中同位素比率的微探针分析方法。 该方法包括选择具有类似于目标矩阵的矩阵的矩阵标准。 在每个矩阵标准上进行体同位素分析以确定体积同位素比值。 在每个矩阵标准上进行微探针分析以确定多个矩阵标准中的每一个的微探针同位素比值。 从微探针同位素比值中消除杂散值。 对于每个矩阵标准物对微探针同位素比值进行平均,以产生与每个矩阵标准相关联的平均微探针同位素比值。 将每个矩阵标准品的体同位素比值相对于与每个矩阵标准相关联的平均微探针同位素比值进行绘图,以创建矩阵校正曲线。