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1. 发明授权

US4035213A Soft textile coatings resembling napa leather 失效
标题翻译：柔软的纺织品涂料类似于napa皮革
公开(公告)号：US4035213A
公开(公告)日：1977-07-12
申请号：US637202
申请日：1975-12-03
申请人： Wilhelm Thoma , Josef Pedain , Jurgen Grammel , Antonio Aguado
发明人： Wilhelm Thoma , Josef Pedain , Jurgen Grammel , Antonio Aguado
IPC分类号： C08G18/00 , C08G18/10 , C08L75/00 , C09D175/04 , D06M15/423 , D06N3/14 , D06N7/04 , B32B27/12 , B32B27/40 , B32B27/42
CPC分类号： D06N3/148 , C08G18/10 , C09D175/04 , D06N3/143 , Y10S428/904 , Y10T428/31554 , Y10T428/31594
摘要： This invention relates to the coating of textile sheets with polyurethane pastes by the reversal process for producing very soft coating articles with a hand resembling that of napa leather. The particular properties of the coating are obtained by using bonding pastes which contain a mixture which can be cross-linked by the action of heat, consisting of polyurethane hydrazodicarbonamides and melamine-formaldehyde resins and/or urea-formaldehyde resins.
摘要翻译：本发明涉及通过反转方法对具有聚氨酯浆料的纺织品片材进行涂布，以用类似于napa皮革的手制造非常柔软的涂层制品。通过使用含有可通过热作用交联的混合物的粘结浆料获得涂层的特定性质，其由聚氨酯肼二酰胺和三聚氰胺 - 甲醛树脂和/或脲 - 甲醛树脂组成。

2. 发明授权

US4530990A Process for the preparation of viscosity stable polyurethane solutions 失效
标题翻译：制备粘度稳定的聚氨酯溶液的方法
公开(公告)号：US4530990A
公开(公告)日：1985-07-23
申请号：US433596
申请日：1982-10-08
申请人： Reinhard Halpaap , Josef Pedain , Wilhelm Thoma , Jurgen Grammel
发明人： Reinhard Halpaap , Josef Pedain , Wilhelm Thoma , Jurgen Grammel
IPC分类号： C08G18/00 , C08G18/10 , C08G18/65 , C08G2/28 , C08G18/08
CPC分类号： C08G18/10
摘要： A process is described for the preparation of predominantly linear polyurethane solutions which comprises(a) reacting(A) an organic diisocyanate or diisocyanate mixture optionally containing small portions of a triisocyanate with(B) one or more polyhydroxyl compounds which are predominantly bifunctional and generally have molecular weights of from about 400 to 5000 and(C) optionally one or more chain lengthening agents having at least two isocyanate reactive hydrogen atoms and molecular weights of from about 32 to 399, wherein the proportion of isocyanate groups to the number of isocyanate-reactive hydrogen atoms is in the range of from about 0.9:1 to 1:0.9, and(b) when the polyurethane formed has reached the required viscosity, adding a monofunctional, low molecular weight oxime having a molecular weight of from about 73 to 325, preferably butanone oxime, to the reaction mixture as chain breaking agent in a quantity equivalent to or in excess of the equivalents of unreacted isocyanate groups.The new chain breaking agents are simple compounds which effect rapid chain breaking and have no undesirable side effects as regards subsequent breakdown of the chains and even enable further synthesizing reactions to be carried out if desired, for example with diamines.
摘要翻译：描述了用于制备主要为线性聚氨酯溶液的方法，其包括（a）使（A）任选地含有少量三异氰酸酯的有机二异氰酸酯或二异氰酸酯混合物与（B）一种或多种主要是双官能的多羟基化合物反应，并且通常具有约400至5000的分子量和（C）任选的一种或多种具有至少两个异氰酸酯反应性氢原子和分子量为约32至399的链延长剂，其中异氰酸酯基团与异氰酸酯反应性数目的比例氢原子在约0.9:1至1:0.9的范围内，和（b）当所形成的聚氨酯达到所需粘度时，加入分子量为约73至325的单官能低分子量肟，优选丁酮肟作为断链剂的反应混合物，其量等于或超过未反应的异氰酸酯的当量 anate组。新的断链剂是简单的化合物，其能够快速断链，并且对链的随后分解没有不期望的副作用，并且甚至能够进一步合成反应，如果需要，例如用二胺进行。

3. 发明授权

US4401801A Coating and dressing agents for leather and leather substitutes based on polyurethane urea coating compounds 失效
标题翻译：基于聚氨酯脲涂料的皮革和皮革替代品的涂层和改性剂
公开(公告)号：US4401801A
公开(公告)日：1983-08-30
申请号：US408371
申请日：1982-08-16
申请人： Josef Pedain , Wilhelm Thoma , Jurgen Grammel , Walter Schroer
发明人： Josef Pedain , Wilhelm Thoma , Jurgen Grammel , Walter Schroer
IPC分类号： C08G18/12 , C08G18/40 , C08G18/42 , C08G18/75 , C14C11/00 , D06N3/14 , C08G18/65
CPC分类号： D06N3/14 , C08G18/12 , C08G18/4018 , C08G18/4202 , C08G18/75 , C14C11/006
摘要： This invention relates to coating agents and dressing agents for leather and leather substitutes with improved resistance to plasticizer migration, greater hardness and folding strength, a dry hand and resistance to aqueous alcoholic solutions, based on linear or only slightly branched thermoplastic polyurethane ureas built up from the following components(A) at least two macrodiols in a molar ratio of from about 1:6 to 6:1, one of which macrodiols(1) has an average molecular weight of from about 254 to 650 and contains at least one benzene, cyclohexane or cyclohexene ring, while(2) the second macrodiol has an average molecular weight in the range of from about 1200 to 3000 but has at least three times the molecular weight of A/l, and which contain(B) from about 0.5 to 11 mol of chain lengthening agent per mol of macrodiol mixture, at least about 50 mol % of the chain lengthening agents used being aliphatic and/or cycloaliphatic diamines and/or hydrazine,and in which(C) the diisocyanates used are cycloaliphatic diisocyanates, up to about 50 mol % of which may be replaced by aliphatic and/or aromatic diisocyanates.
摘要翻译：本发明涉及用于皮革和皮革代用品的涂料和改性剂，其具有改善的耐增塑剂迁移性，更高的硬度和折叠强度，干手和耐醇水溶液，基于线性或仅轻微分支的热塑性聚氨酯脲，其由以下组分（A）至少两种摩尔比为约1:6至6:1的大分子二醇，其中一个大分子二醇（1）的平均分子量为约254至650，并含有至少一个苯，环己烷或环己烯环，而（2）第二大二茂醇的平均分子量为约1200-3000，但具有至少三倍于A / l的分子量，并且含有（B）约0.5至每摩尔大分子二醇混合物使用11摩尔的链延长剂，至少约50摩尔％的使用的链增长剂是脂族和/或脂环族二胺和/或肼，其中（C）二异氰酸酯使用的氰酸酯是脂环族二异氰酸酯，其中最多约50mol％可以被脂族和/或芳族二异氰酸酯代替。

4. 发明授权

US4829122A Process for the preparation of aqueous polyurethane dispersions and solutions 失效
标题翻译：制备水性聚氨酯分散体和溶液的方法
公开(公告)号：US4829122A
公开(公告)日：1989-05-09
申请号：US19902
申请日：1987-02-27
申请人： Josef Pedain , Klaus Nachtkamp , Klaus Noll , Jurgen Grammel
发明人： Josef Pedain , Klaus Nachtkamp , Klaus Noll , Jurgen Grammel
IPC分类号： C08G18/00 , C03C25/00 , C08G18/08 , C08G18/10
CPC分类号： C08G18/0804 , C03C25/00 , C08G18/10 , Y10T428/31551
摘要： The present invention therefore relates to a process for the preparation of aqueous solutions or dispersions of polyurethane-polyureas by the reaction in the aqueous phase of prepolymers which contain chemically built-in hydrophilic groups and/or external emulsifiers which are not bound chemically as well as at least two free isocyanate groups with organic compounds containing at least two primary and/or secondary amino groups, characterized in that the isocyanate prepolymer which has been hydrophilically modified and/or contains an external emulsifier is mixed, in the absence of water, with compounds containing at the most one free primary or secondary amino group and at least one blocked group which releases a free primary or secondary amino group in the presence of water and a total of at least two at least partially blocked primary and/or secondary amino groups, and the mixture is subsequently mixed with water.The invention also relates to the dispersions or solutions obtained by this process and to their use for coating flexible and rigid substrates.
摘要翻译：因此，本发明涉及一种制备聚氨酯 - 聚脲的水溶液或分散体的方法，所述水溶液或分散体是通过在水相中含有化学内置的亲水基团的预聚物和/或外部乳化剂的反应制成的，至少两个含有至少两个伯和/或仲氨基的有机化合物的游离异氰酸酯基团，其特征在于，在没有水的情况下将已经亲水改性和/或含有外部乳化剂的异氰酸酯预聚物与化合物含有最多一个游离的伯或仲氨基和至少一个在水存在下释放游离的伯或仲氨基并且总共至少两个至少部分封闭的伯和/或仲氨基的封闭基团，随后将混合物与水混合。本发明还涉及通过该方法获得的分散体或溶液及其用于涂覆柔性和刚性基材的用途。

5. 发明授权

US4269748A Process for the preparation of aqueous polyurethane dispersions and solutions 失效
标题翻译：制备水性聚氨酯分散体和溶液的方法
公开(公告)号：US4269748A
公开(公告)日：1981-05-26
申请号：US17017
申请日：1979-03-02
申请人： Klaus Nachtkamp , Josef Pedain , Jurgen Grammel
发明人： Klaus Nachtkamp , Josef Pedain , Jurgen Grammel
IPC分类号： C08G18/00 , C08G18/08 , C08G18/10 , C08G18/28 , C08G18/32 , C08J3/02 , C08L75/12
CPC分类号： C08G18/283 , C08G18/0804 , C08G18/10 , Y10T428/31551
摘要： The present invention relates to a process for the preparation of aqueous solutions or dispersions of polyurethanes, in which process prepolymers which have at least two free isocyanate groups and contain chemically-fixed hydrophilic groups and/or external emulsifiers which are not chemically fixed are reacted with chain lengthening agents in the aqueous phase, characterized in that the isocyanate prepolymer which is hydrophilically modified and/or contains an external emulsifier is mixed with chain lengthening agents selected from the group consisting of azines and hydrazones in the absence of water and the mixture obtained is then mixed with water. The present invention also relates to the dispersions or solutions which can be obtained by this process. Lastly, this invention relates to the use of the dispersions or solutions which can be obtained by this process for coating flexible substrates.
摘要翻译：本发明涉及一种制备聚氨酯水溶液或分散体的方法，其中具有至少两个游离异氰酸酯基并含有化学上固定的亲水基团的工艺预聚物和/或未化学固定的外部乳化剂与在水相中的链延长剂，其特征在于将亲水改性和/或含有外部乳化剂的异氰酸酯预聚物与不含水的吖嗪和腙类的链增长剂混合，得到的混合物为然后与水混合。本发明还涉及可以通过该方法获得的分散体或溶液。最后，本发明涉及通过该方法可以获得的用于涂覆柔性基材的分散体或溶液的用途。

6. 发明授权

US5252671A Coating compositions for coatings that are permeable to water vapor and a process for their preparation 失效
标题翻译：可渗透水蒸气的涂料涂料组合物及其制备方法
公开(公告)号：US5252671A
公开(公告)日：1993-10-12
申请号：US887213
申请日：1992-05-21
申请人： Josef Pedain , Klaus Noll , Wilhelm Thoma , Detlef-Ingo Schutze
发明人： Josef Pedain , Klaus Noll , Wilhelm Thoma , Detlef-Ingo Schutze
IPC分类号： C14C11/00 , C08L75/00 , C09D133/04 , C09D175/00 , C09D175/04 , D06M15/564 , D06N3/04 , D06N3/14 , C08F8/30
CPC分类号： D06N3/14 , C09D133/04 , C09D175/04 , C08L75/00 , Y10S528/904
摘要： The present invention relates to coating compositions containing(A) 70 to 98% by weight, based on the sum of components (A) and (B), of(a) isocyanate-free polymers of ethylenically unsaturated monomers and/or polyurethanes or blocked isocyanate prepolymers, and(b) optional organic solvents, wherein component (A) contains no significant quantities of groups capable of reacting with component (B) or starting materials thereof and has a viscosity (at 23.degree. C.) of 2000 to 100,000 mPa.s;(B) 2 to 30% by weight, based on the sum of components (A) and (B), of a polyaddition product prepared in and dispersed in component (A), wherein the polyaddition product is a polyurethane, polyurethane urea, polyurea, or mixture thereof, containing ionic groups and/or potentially ionic groups in a quantity corresponding to from 0.5 to 20 milliequivalents per 100 g of component (B) but containing substantially no free isocyanate, hydroxyl, or amino groups: and(C) optional cross-linking agents;in which component (B) is formed in situ in component (A).
摘要翻译：本发明涉及涂料组合物，其包含（A）70至98重量％，基于组分（A）和（B）的总和，（a）烯属不饱和单体和/或聚氨酯或封闭的无异氰酸酯的聚合物异氰酸酯预聚物和（b）任选的有机溶剂，其中组分（A）不含有显着量的能够与组分（B）或其原料反应的基团，并且具有2000至100,000mPa的粘度（在23℃） .s; （B）基于组分（A）和（B）的总和，制备和分散在组分（A）中的加聚产物的2-30重量％，其中所述加聚产物是聚氨酯，聚氨酯脲，聚脲或其混合物，其含有相对于每100g组分（B）0.5至20毫当量但基本上不含游离异氰酸酯，羟基或氨基的量的离子基团和/或潜在的离子基团：和（C）任选的交联剂; 其中组分（B）在组分（A）中原位形成。

7. 发明授权

US4894428A Process for coating substrates with polyurethane ureas 失效
标题翻译：用聚氨酯脲涂层基材的方法
公开(公告)号：US4894428A
公开(公告)日：1990-01-16
申请号：US292698
申请日：1989-01-03
申请人： Wilhelm Thoma , Josef Pedain , Waldemar Kling
发明人： Wilhelm Thoma , Josef Pedain , Waldemar Kling
IPC分类号： B32B27/12 , C08G18/10 , C08G18/12 , C08G18/40 , C08G18/65 , C08G18/80 , C09D175/00 , C09D175/04 , D06M15/564 , D06N3/14
CPC分类号： D06N3/14 , C08G18/10 , C08G18/12 , C08G18/4018 , Y10T428/31551 , Y10T428/31591 , Y10T442/2566
摘要： The present invention is directed to a process for coating substrates with polyurethane ureas which is characterized in that a substrate is coated with a product, which has been obtained by the reation of (A) a prepolymer based on an aromatic polyisocyanate containing on average two ketoxime-blocked NCO groups and having an average molecular weight of about 500 to 15,000 with (B) a chain-extending agent corresponding to the formulaH.sub.2 N--R'--NH.sub.2in which R' is an aliphatic or cycloaliphatic radical, in the presence of solvents at temperatures above 50.degree. C. and at an equivalent ratio of blocked NCO groups to NH.sub.2 groups of 1.43 to 1.02, wherein after about 40 to 90% of the available amino groups have reacted, the reaction is completed with crosslinking at temperatures above 120.degree. C.The present invention is also directed to the coated substrates produced by this process.
摘要翻译：本发明涉及一种用聚氨酯脲涂覆基材的方法，其特征在于基材涂覆有产品，该产品是通过（A）基于芳族多异氰酸酯的预聚物（其平均包含平均两个酮肟）（B）相应于式H2N-R'-NH2的增链剂，其中R'是脂族或脂环族基团，在溶剂存在下，具有约500至15,000的平均分子量在高于50℃的温度下，封闭的NCO基团与NH 2基团的当量比为1.43至1.02，其中约40至90％的可用氨基已经反应后，反应在120℃以上的温度下进行交联本发明还涉及通过该方法制备的涂覆基材。

8. 发明授权

US4308184A Heat cross linkable polyurethane coating compositions 失效
标题翻译：热交联聚氨酯涂料组合物
公开(公告)号：US4308184A
公开(公告)日：1981-12-29
申请号：US25152
申请日：1979-03-29
申请人： Wilhelm Thoma , Gerhard Berndt , Josef Pedain , Walter Schroer , Waldemar Kling
发明人： Wilhelm Thoma , Gerhard Berndt , Josef Pedain , Walter Schroer , Waldemar Kling
IPC分类号： C09D175/04 , D06N3/14 , C08L75/04
CPC分类号： D06N3/142 , C09D175/04 , Y10S428/904 , Y10T428/31591
摘要： The present disclosure is concerned with solvent free or very low solvent coating compositions suitable for use on flexible sheet form substrates particularly textile substrates. The composition comprises a urethane group-containing prepolymer with OH or CONH.sub.2 terminal groups mixed with a urea or melamine formaldehyde resin and a stable aqueous polymer dispersion or solution. The composition may also contain small amounts of an organic solvent. The coating can be applied to the substrate by direct or reverse coating techniques.
摘要翻译：本公开涉及适用于柔性片状基材，特别是纺织品基材的无溶剂或非常低溶剂涂料组合物。该组合物包含与尿素或三聚氰胺甲醛树脂混合的OH或CONH 2端基和稳定的含水聚合物分散体或溶液的含氨基甲酸酯基的预聚物。组合物还可以含有少量的有机溶剂。可以通过直接或反向涂布技术将涂层施加到基底上。

9. 发明授权

US4876302A Polyurethane dispersions and the use thereof as finishing agents 失效
标题翻译：聚氨酯分散体及其作为整理剂的用途
公开(公告)号：US4876302A
公开(公告)日：1989-10-24
申请号：US284970
申请日：1988-12-15
申请人： Klaus Noll , Wilhelm Thoma , Klaus Nachtkamp , Walter Schroer , Josef Pedain
发明人： Klaus Noll , Wilhelm Thoma , Klaus Nachtkamp , Walter Schroer , Josef Pedain
IPC分类号： C08L75/04 , C08G18/00 , C08G18/08 , C08G18/12 , C08G18/66 , C08G18/72 , C08G18/73 , C08G18/75 , C08J7/04 , C08L75/00 , C09D175/00 , C09D175/04 , C09D175/06 , C09D175/12
CPC分类号： C09D175/06 , C08G18/0819 , C08G18/12 , C08G18/6644 , C08G18/6659 , C08G18/722 , C08J7/047 , C08J2475/00
摘要： The present invention is directed to aqueous coating compositions suitable for use as coating and finishing agents for surface coatings, preferably PVC or polyurethane coatings, based on sedimentation-stable polyurethane dispersions having a solids content of about 10-70% by weight wherein the polyurethane-urea solids material is based on polyester diols, low molecular weight diols and optionally triols, chemically incorporated hydrophilic groups, specific mixtures of diisocyanates and polyamine chain extenders having an average functionality of greater than 2 and wherein the aqueous preparations additionally contain alkoxylated dimethyl-polysiloxanes and water-soluble polyethylene oxides. The present invention is also directed to a process for applying top coats and finishes to surface coatings, preferably PVC or polyurethane surface coatings, wherein the above-described aqueous coating and finishing agents are used as the top coat and the coatings are cured at about 70.degree.-170.degree. C.
摘要翻译：本发明涉及适用于基于沉积稳定的聚氨酯分散体的表面涂层（优选PVC或聚氨酯涂层）的涂层和整理剂的水性涂料组合物，其中固体含量为约10-70％（重量），其中聚氨酯 - 脲固体材料基于聚酯二醇，低分子量二醇和任选的三醇，化学引入的亲水基团，二异氰酸酯的特定混合物和平均官能度大于2的多胺扩链剂，其中所述水性制剂另外含有烷氧基化二甲基 - 聚硅氧烷，水溶性聚环氧乙烷。本发明还涉及一种将表面涂层和表面涂层施用于表面涂层，优选PVC或聚氨酯表面涂层的方法，其中上述水性涂料和整理剂用作顶涂层，并且涂层在约70℃下固化 DEG-170℃

10. 发明授权

US4743470A Spreading pastes containing polyurethane plastics and a process for the production of polyurethane coatings permeable to water vapor 失效
标题翻译：散布含有聚氨酯塑料的糊状物以及生产可渗透水蒸汽的聚氨酯涂料的方法
公开(公告)号：US4743470A
公开(公告)日：1988-05-10
申请号：US829892
申请日：1986-02-18
申请人： Klaus Nachtkamp , Wilhelm Thoma , Josef Pedain , Walter Schroer , Rolf Langel
发明人： Klaus Nachtkamp , Wilhelm Thoma , Josef Pedain , Walter Schroer , Rolf Langel
IPC分类号： C08J7/04 , C08G18/00 , C08G18/04 , C08G18/08 , C08G18/38 , C08G18/40 , C08G18/42 , C08G18/48 , C08G18/61 , C08L75/00 , C09D175/00 , C09D175/04 , C14C11/00 , D06M13/02 , D06M13/224 , D06M13/325 , D06M13/338 , D06M15/256 , D06M15/263 , D06M15/507 , D06M15/53 , D06M15/564 , D06M15/568 , D06M15/576 , D06M15/61 , D06M15/643 , D06N3/14 , D06M15/572 , D06M15/653
CPC分类号： D06N3/142 , C08G18/3861 , C08G18/4018 , C08G18/4202 , C08G18/4211 , C08G18/4879 , C08G18/61 , C09D175/04 , C14C11/006 , D06N3/14 , D06N3/141 , Y10T428/31558 , Y10T442/2861 , Y10T442/2893
摘要： This invention relates to spreading pastes containing polyurethanes which are prepared from special synthesis components selected from the group of silicone resins, polyethers or polyesters containing aromatic segments or perfluorocarbon resins. The spreading pastes also contain organic solvents and optionally non-solvents for the polyurethanes so that when the coatings are used to coat textile substrates according to the direct or transfer process, the coatings may be cured based on the principle of evaporation coagulation.
摘要翻译：本发明涉及由含有聚硅氧烷树脂，聚醚或含有芳族链段或全氟化碳树脂的聚酯组成的特殊合成成分制备的含有聚氨酯的铺展浆料。铺展的糊料还含有有机溶剂和任选的用于聚氨酯的非溶剂，使得当根据直接或转移过程将涂层用于涂覆织物基材时，可以基于蒸发凝结原理固化涂层。

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