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1. 发明授权

US06489499B1 Siloxane modified carboxylic acid substituted amines and salts thereof 有权
标题翻译：硅烷改性的羧酸取代的胺及其盐
公开(公告)号：US06489499B1
公开(公告)日：2002-12-03
申请号：US10096047
申请日：2002-03-11
申请人： Wayne King , John H. MacMillan , Michael J. Telepchak
发明人： Wayne King , John H. MacMillan , Michael J. Telepchak
IPC分类号： C07F710
CPC分类号： C07F7/1804
摘要： Novel compounds comprising siloxane modified carboxylic acid substituted amines and salts thereof are provided. The compounds according to the invention provide many of the desirable properties of ethylenediamine tetraacetic acid and its salts in a stationary phase. A process for synthesis of the compounds according to the invention are also provided.
摘要翻译：提供了包含硅氧烷改性的羧酸取代的胺及其盐的新型化合物。根据本发明的化合物在固定相中提供了乙二胺四乙酸及其盐的许多所需性质。还提供了合成本发明化合物的方法。

2. 发明授权

US06589799B2 Supported aldehydic silanes and method of manufacture 有权
公开(公告)号：US06589799B2
公开(公告)日：2003-07-08
申请号：US09847212
申请日：2001-05-02
申请人： Ann N. Coyne , John H. MacMillan , Michael J. Telepchak
发明人： Ann N. Coyne , John H. MacMillan , Michael J. Telepchak
IPC分类号： G01N33552
CPC分类号： C12N11/06 , C12N11/14
摘要： A method for producing a derivatized aldehydic support matrix material includes activating surface hydroxyl groups on the support matrix material and reacting the activated hydroxyl groups with an aldehydic alkoxy silane. The derivatized aldehydic support matrix material produced is useful for immobilizing bio-molecules in biological applications.

3. 发明授权

US06177583B1 Method for the preparation of aminopropyl or aminoalkyl functional polyalkyl or aryl siloxanes 有权
标题翻译：氨基丙基或氨基烷基官能化聚烷基或芳基硅氧烷的制备方法
公开(公告)号：US06177583B1
公开(公告)日：2001-01-23
申请号：US09385286
申请日：1999-08-30
申请人： Marla Marzinke , John H. MacMillan , Thomas F. August , Michael J. Telepchak
发明人： Marla Marzinke , John H. MacMillan , Thomas F. August , Michael J. Telepchak
IPC分类号： C02F210
CPC分类号： C08G77/388
摘要： A new method for the preparation of aminopropyl terminated or internal functionalized polyalkyl or aryl siloxanes is described. The method involves readily available commercial starting materials and proceeds under mild conditions in high yield. Purification is facilitated over present commercial procedures and a wider variety of internal functionalized siloxanes may be prepared. The method involves hydrosilation of commercially availably alkyl or aryl functional hydrosilicones with allyl amine or other alkenyl or arenyl amine in the presence of platinum (0) divinyltetramethylsiloxane or platinum (0) cyclovinyl complexes.
摘要翻译：描述了制备氨基丙基封端或内部官能化聚烷基或芳基硅氧烷的新方法。该方法涉及易于获得的商业起始材料，并且在温和条件下以高产率进行。在目前的商业程序中促进了纯化，并且可以制备更多种类的内部官能化硅氧烷。该方法包括在铂（0）二乙烯基四甲基硅氧烷或铂（0）环乙烯基络合物的存在下，使用烯丙基胺或其它烯基或异戊基胺在商业上有用的烷基或芳基官能水合硅氧烷进行氢化硅烷化。

4. 发明授权

US07045365B2 Supported aldehydic silanes and method of manufacture 有权
公开(公告)号：US07045365B2
公开(公告)日：2006-05-16
申请号：US10438432
申请日：2003-05-15
申请人： Ann N. Coyne , John H. MacMillan , Michael J. Telepchak
发明人： Ann N. Coyne , John H. MacMillan , Michael J. Telepchak
IPC分类号： G01N33/552 , G01N33/553 , G01N33/545 , G01N33/548 , C07K17/08 , C07K17/10 , C07K17/14
CPC分类号： C12N11/06 , C12N11/14
摘要： A method for producing a derivatized aldehydic support matrix material includes activating surface hydroxyl groups on the support matrix material and reacting the activated hydroxyl groups with an aldehydic alkoxy silane. The derivatized aldehydic support matrix material produced is useful for immobilizing bio-molecules in biological applications.

5. 发明授权

US07666686B2 Method for sample preparation by solid phase extraction 有权
标题翻译：固相萃取法制备样品
公开(公告)号：US07666686B2
公开(公告)日：2010-02-23
申请号：US11434270
申请日：2006-05-15
申请人： Donald L. Shelly, Jr. , Phillip Spraker , William L. Ozanich, Jr. , Michael J. Telepchak
发明人： Donald L. Shelly, Jr. , Phillip Spraker , William L. Ozanich, Jr. , Michael J. Telepchak
IPC分类号： G01N1/18
CPC分类号： G01N1/405 , B01D2253/106 , B01D2257/80 , B01J20/103 , B01J20/20 , B01J20/28052 , B01J20/3242 , Y10T436/25375 , Y10T436/255 , Y10T436/25875
摘要： An method for sample preparation using solid phase extraction. Using an apparatus comprising a SPE cartridge and a sorbent-containing gas filter which contains a sorbent and is detachably connected to the SPE cartridge the gas used to dry the SPE cartridge is purified by passage through the gas filter, thereby preventing contamination of the SPE sorbent by airborne contaminants.
摘要翻译：使用固相萃取的样品制备方法。使用包含SPE盒和含吸附剂的气体过滤器的装置，其包含吸附剂并且可拆卸地连接到SPE筒，用于干燥SPE筒的气体通过气体过滤器被净化，从而防止SPE吸附剂的污染由空气污染物。

6. 发明授权

US6156431A Extraction material comprising treated silica and method for determination of gamma-hydroxybutyrate 有权
标题翻译：包含处理过的二氧化硅的提取材料和γ-羟基丁酸酯的测定方法
公开(公告)号：US6156431A
公开(公告)日：2000-12-05
申请号：US224691
申请日：1999-01-04
申请人： Chester J. Kitchen , Thomas F. August , William L. Ozanich , Michael J. Telepchak
发明人： Chester J. Kitchen , Thomas F. August , William L. Ozanich , Michael J. Telepchak
IPC分类号： B01J20/10 , B01J20/32 , B32B5/16 , B01D24/00 , B01D39/06
CPC分类号： B01J20/103 , B01J20/28004 , B01J20/283 , B01J20/286 , B01J20/3204 , B01J20/3257 , B01J20/3261 , B01J2220/54 , B01J2220/58 , B01J2220/62 , Y10T428/2995
摘要： A treated silica composition particularly useful for solid phase extraction in chemical analysis, the silica having both phenyl and propylsulfonic acid functional groups; a cartridge for extraction which comprises the treated silica; a column for extraction which comprises the treated silica; and a method for solid phase extraction which uses the silica composition. A method for analysis of gamma hydroxybutyric acid is also disclosed which uses the treated silica.
摘要翻译：在化学分析中特别可用于固相萃取的经处理的二氧化硅组合物，具有苯基和丙磺酸官能团的二氧化硅; 用于提取的筒，其包含处理过的二氧化硅; 用于提取的柱，其包含处理过的二氧化硅; 以及使用二氧化硅组合物的固相萃取方法。还公开了用于分析γ-羟基丁酸的方法，其使用经处理的二氧化硅。

7. 发明授权

US07438862B2 Apparatus for simultaneous processing of multiple samples 有权
标题翻译：用于同时处理多个样品的装置
公开(公告)号：US07438862B2
公开(公告)日：2008-10-21
申请号：US10222192
申请日：2002-08-16
申请人： Ann N. Coyne , Michael J. Telepchak , Philip Spraker , Jay Hardee , John A. D'Asaro
发明人： Ann N. Coyne , Michael J. Telepchak , Philip Spraker , Jay Hardee , John A. D'Asaro
IPC分类号： B01L3/00
CPC分类号： B01L3/5025 , B01J2219/00274 , B01L3/50255 , B01L2200/141 , B01L2400/049
摘要： An apparatus is provided for simultaneous processing of multiple fluid samples. The apparatus comprises a multiple well plate for holding a plurality of sample reservoirs for simultaneous processing of multiple samples. The wells are configured in the plate in staggered rows. The well plate is dimensioned to be compatible with a vacuum manifold or positive pressure system either as a stand-alone unit or in conjunction with a separate fluid handling system. The apparatus may further comprise a sample collection plate having the same number of wells as the multiple well plate. The wells in the samples collection plate are arranged in the same staggered configuration as the wells in the well plate and are sized for holding sample collection vials. When the well plate and sample collection plate are assembled in a manifold, the vials in the sample collection plated are aligned directly beneath the sample exits of corresponding sample reservoirs in the well plate.
摘要翻译：提供了用于同时处理多个流体样品的装置。该装置包括用于保持多个样品储存器以用于多个样品的同时处理的多孔板。井在板中以交错排列配置。孔板的尺寸设计为与真空歧管或正压系统兼容，作为独立单元或与单独的流体处理系统结合。该装置还可以包括具有与多孔板相同数量的孔的样品收集板。样品收集板中的孔以与孔板中的孔相同的交错构型布置，并且尺寸适于保持样品采集瓶。当孔板和样品收集板组装在歧管中时，电镀样品中的小瓶直接对准孔板中相应样品储存器的样品出口的正下方。

8. 发明授权

US06530288B1 Microcolumn for use in sample extraction 有权
标题翻译：用于样品提取的微柱
公开(公告)号：US06530288B1
公开(公告)日：2003-03-11
申请号：US09599680
申请日：2000-06-22
申请人： Thomas F. August , Michael J. Telepchak
发明人： Thomas F. August , Michael J. Telepchak
IPC分类号： G01N100
CPC分类号： G01N1/405 , G01N30/6004
摘要： A housing is described for use in preparing a sample for chemical analysis, the housing having a sample entrance, a sample exit, and a passageway therebetween; the housing further comprising at least three ridges, the ridges integral with the housing, depending into the passageway, and defining a supporting profile for holding a sorbent retaining member.
摘要翻译：描述了用于制备用于化学分析的样品的壳体，所述壳体具有样品入口，样品出口及其间的通路; 所述壳体还包括至少三个脊部，所述脊部与所述壳体一体形成，所述脊部与所述通道一体，并且限定用于保持吸附剂保持构件的支撑轮廓。

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