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1. 发明申请

US20100217040A1 2, 2', 6, 6'- TETRASUBSTITUTED AMINOPHOSPHINE LIGAND AND ITS SYNTHESIS METHOD 有权
标题翻译： 2，2'，6,6'-四唑基氨基磷酰胺配体及其合成方法
公开(公告)号：US20100217040A1
公开(公告)日：2010-08-26
申请号：US12377000
申请日：2007-08-10
申请人： Wanbin Zhang , Fang Xie , Fang Fang
发明人： Wanbin Zhang , Fang Xie , Fang Fang
IPC分类号： C07F9/50
CPC分类号： C07F9/46
摘要： The present invention relates to a 2,2′,6,6′-tetrasubstituted aminophosphine ligand and its synthesis method. The structure of the ligand is shown as below. Its synthesis method comprises: Step (1) coupling 2,6-dinitrochlorobenzene as the starting material to obtain 2,2′,6,6′-tetranitrobiphenyl; Step (2): hydrogenating the 2,2′,6,6′-tetranitrobiphenyl with Pd/C to obtain 2,2′,6,6′-tetraminobiphenyl; Step (3): reacting the 2,2′,6,6′-tetraminobiphenyl with a phosphine halide to obtain the 2,2′,6,6′-tetrasubstituted aminophosphine ligand. The ligand of the present invention is an achiral compound, and its preparation method is simple. The ligand can be converted to a chiral bimetallic catalyst with single configuration eventually through introduction of external chirality. Moreover, the ligand can be used in various asymmetric reaction catalyzed by metals with high reactivity and stereoselectivity.
摘要翻译：本发明涉及2,2'，6,6'-四取代氨基膦配体及其合成方法。配体的结构如下所示。其合成方法包括：步骤（1）以2,6-二硝基氯苯为原料，得到2,2'，6,6'-四硝基联苯; 步骤（2）：用Pd / C氢化2,2'，6,6'-四硝基二苯并得到2,2'，6,6'-四氨基联苯; 步骤（3）：使2,2'，6,6'-四磺酰联苯与卤化膦反应，得到2,2'，6,6'-四取代氨基膦配体。本发明的配体是非手性化合物，其制备方法简单。最终可以通过引入外部手性将配体转化为具有单一配置的手性双金属催化剂。此外，配体可用于由具有高反应性和立体选择性的金属催化的各种不对称反应中。

2. 发明授权

US08729303B2 2,2′,6,6′-tetrasubstituted aminophosphine ligand and its synthesis method 有权
标题翻译： 2,2'，6,6'-四取代氨基膦配体及其合成方法
公开(公告)号：US08729303B2
公开(公告)日：2014-05-20
申请号：US12377000
申请日：2007-08-10
申请人： Wanbin Zhang , Fang Xie , Fang Fang
发明人： Wanbin Zhang , Fang Xie , Fang Fang
IPC分类号： C07F9/02
CPC分类号： C07F9/46
摘要： The present invention relates to a 2,2′,6,6′-tetrasubstituted aminophosphine ligand and its synthesis method. The structure of the ligand is shown as below. Its synthesis method comprises: Step (1) coupling 2,6-dinitrochlorobenzene as the starting material to obtain 2,2′,6,6′-tetranitrobiphenyl; Step (2): hydrogenating the 2,2′,6,6′-tetranitrobiphenyl with Pd/C to obtain 2,2′,6,6′-tetraminobiphenyl; Step (3): reacting the 2,2′,6,6′-tetraminobiphenyl with a phosphine halide to obtain the 2,2′,6,6′-tetrasubstituted aminophosphine ligand. The ligand of the present invention is an achiral compound, and its preparation method is simple. The ligand can be converted to a chiral bimetallic catalyst with single configuration eventually through introduction of external chirality. Moreover, the ligand can be used in various asymmetric reaction catalyzed by metals with high reactivity and stereoselectivity.
摘要翻译：本发明涉及2,2'，6,6'-四取代氨基膦配体及其合成方法。配体的结构如下所示。其合成方法包括：步骤（1）以2,6-二硝基氯苯为原料，得到2,2'，6,6'-四硝基联苯; 步骤（2）：用Pd / C氢化2,2'，6,6'-四硝基二苯并得到2,2'，6,6'-四氨基联苯; 步骤（3）：使2,2'，6,6'-四磺酰联苯与卤化膦反应，得到2,2'，6,6'-四取代氨基膦配体。本发明的配体是非手性化合物，其制备方法简单。最终可以通过引入外部手性将配体转化为具有单一配置的手性双金属催化剂。此外，配体可用于由具有高反应性和立体选择性的金属催化的各种不对称反应中。

3. 发明申请

US20110160474A1 C2-SYMMETRICAL RUTHENOCENE DIPHOSPHINE LIGANDS ONLY WITH SURFACE CHIRALITY AND THEIR MANUFACTURE 失效
标题翻译： C2-对称二硫代磷酸酯配体仅具有表面光洁度及其制造
公开(公告)号：US20110160474A1
公开(公告)日：2011-06-30
申请号：US12303767
申请日：2007-06-08
申请人： Wanbin Zhang , Fang Xie , Delong Liu , Li Luo , Genghong Hua , Jian Shang
发明人： Wanbin Zhang , Fang Xie , Delong Liu , Li Luo , Genghong Hua , Jian Shang
IPC分类号： C07F17/02
CPC分类号： C07F17/02 , B01J31/2295 , B01J31/24 , B01J31/2409 , B01J2531/0205 , B01J2531/0263 , B01J2531/821
摘要： The invention affords C2-symmetrical ruthenocene diphosphine ligands with surface chirality and their manufacture. The present invention uses (S)—(S)-1,1′-2(diphenylphosphino)-2,2′-2[(S)-4-isopropyloxazolinyl]ruthenocene as raw material and the product is prepared through two or three steps of reaction. At the action of trifluoroacetic acid, (S)—(S)-1,1′-2(diphenylphosphino)-2,2′-2[(S)-4-isopropyloxazolinyl]ruthenocene first removes oxazoline and gets ester amides compound which then carries out ester exchange or reduction alkylation and gets the product of ruthenocene diphosphine ligand with surface chirality. The ligands prepared with the structure as follows from the invention can be used in all kinds of metallic catalysis asymmetric reaction and has good reaction activity and stereoselectivity, wherein R is methyl or ethyl, R1 is linear or branched alkyl, cycloalkyl, alkoxy, aryl, aralkyl and alkyl amino.
摘要翻译：本发明提供具有表面手性及其制造的C2对称的二茂铁二膦配体。本发明使用（S） - （S）-1,1'-2（二苯基膦基）-2,2'-2 [（S）-4-异丙唑恶唑啉基] rut烯为原料，通过2或3 反应步骤。在三氟乙酸的作用下，（S） - （S）-1,1'-2（二苯基膦基）-2,2'-2 [（S）-4-异丙基恶唑啉基] rut hen ene首先除去恶唑啉并得到酯酰胺化合物，然后进行酯交换或还原烷基化，得到具有表面手性的钌基二膦配体的产物。由本发明制备的具有如下结构的配位体可用于各种金属催化不对称反应，具有良好的反应活性和立体选择性，其中R为甲基或乙基，R 1为直链或支链烷基，环烷基，烷氧基，芳基，芳烷基和烷基氨基。

4. 发明授权

US08507705B2 C2-symmetrical ruthenocene diphosphine ligands only with surface chirality and their manufacture 失效
标题翻译： C2对称的二茂铁二膦配体仅具有表面手性及其制造
公开(公告)号：US08507705B2
公开(公告)日：2013-08-13
申请号：US12303767
申请日：2007-06-08
申请人： Wanbin Zhang , Fang Xie , Delong Liu , Li Luo , Genghong Hua , Jian Shang
发明人： Wanbin Zhang , Fang Xie , Delong Liu , Li Luo , Genghong Hua , Jian Shang
IPC分类号： C07F15/00
CPC分类号： C07F17/02 , B01J31/2295 , B01J31/24 , B01J31/2409 , B01J2531/0205 , B01J2531/0263 , B01J2531/821
摘要： The invention affords C2-symmetrical ruthenocene diphosphine ligands with surface chirality and their manufacture. The present invention uses (S)-(S)-1,1′-2(diphenylphosphino)-2,2′-2[(S)-4-isopropyloxazolinyl] ruthenocene as raw material and the product is prepared through two or three steps of reaction. At the action of trifluoroacetic acid, (S)-(S)-1,1′-2(diphenylphosphino)-2,2′-2[(S)-4-isopropyloxazolinyl] ruthenocene first removes oxazoline and gets ester amides compound which then carries out ester exchange or reduction alkylation and gets the product of ruthenocene diphosphine ligand with surface chirality. The ligands prepared with the structure as follows from the invention can be used in all kinds of metallic catalysis asymmetric reaction and has good reaction activity and stereoselectivity, wherein R is methyl or ethyl, R1 is linear or branched alkyl, cycloalkyl, alkoxy, aryl, aralkyl and alkyl amino.
摘要翻译：本发明提供具有表面手性及其制造的C2对称的二茂铁二膦配体。本发明使用（S） - （S）-1,1'-2（二苯基膦基）-2,2'-2 [（S）-4-异丙唑恶唑啉基] rut烯为原料，通过2或3 反应步骤。在三氟乙酸的作用下，（S） - （S）-1,1'-2（二苯基膦基）-2,2'-2 [（S）-4-异丙基恶唑啉基] rut hen ene首先除去恶唑啉并得到酯酰胺化合物，然后进行酯交换或还原烷基化，得到具有表面手性的钌基二膦配体的产物。由本发明制备的具有如下结构的配位体可用于各种金属催化不对称反应，具有良好的反应活性和立体选择性，其中R为甲基或乙基，R 1为直链或支链烷基，环烷基，烷氧基，芳基，芳烷基和烷基氨基。

5. 发明申请

US20120225637A1 Method, Mobile Terminal, Service Platform and System for Implementing Debit Card Service 有权
标题翻译：方法，移动终端，实施借记卡服务的服务平台和系统
公开(公告)号：US20120225637A1
公开(公告)日：2012-09-06
申请号：US13509054
申请日：2010-05-11
申请人： Fang Xie , Jianjun Yang , Sanping Zhang , Xuefeng Guo
发明人： Fang Xie , Jianjun Yang , Sanping Zhang , Xuefeng Guo
IPC分类号： H04W4/26 , H04W4/24
CPC分类号： H04L12/14 , H04M3/38 , H04M3/42195 , H04M15/06 , H04M17/02 , H04M17/30 , H04M17/301 , H04M17/303 , H04M2203/2011 , H04M2207/18 , H04W4/24
摘要： A method and system for implementing debit card service based on callback. The method is applied to a mobile terminal set with an automatic dialing function unit, automatic dialing function of the automatic dialing function unit is activated, and a number corresponding to the mobile terminal is bound with one debit card. The method includes the following steps: a preset callback access number is dialed before the called number by the automatic dialing function unit in the mobile terminal to connect the call to a debit card service platform when the mobile terminal calls the called number; the debit card service platform releases the call and calls back the mobile terminal; the called number is continued by the debit card service platform after the mobile terminal answers the callback; the debit card service based on callback is implemented.
摘要翻译：一种基于回调实现借记卡服务的方法和系统。该方法应用于具有自动拨号功能单元的移动终端，自动拨号功能单元的自动拨号功能被激活，并且与移动终端对应的号码与一张借记卡绑定。该方法包括以下步骤：通过移动终端中的自动拨号功能单元在被叫号码之前拨打预设的回拨接入号码，以便当移动终端呼叫被叫号码时将呼叫连接到借记卡服务平台; 借记卡服务平台释放呼叫并呼叫移动终端; 在移动终端应答回叫之后，由借记卡服务平台继续被叫号码; 基于回拨的借记卡服务被实现。

6. 发明申请

US20110072137A1 INTEGRATED APPLICATION ACCESS 有权
标题翻译：集成应用访问
公开(公告)号：US20110072137A1
公开(公告)日：2011-03-24
申请号：US12956617
申请日：2010-11-30
申请人： Marcial Montes de oca , Chi-Hwei Julie Lin , Manuel Ledesma , Yunyan Wang , Fang Xie , Tsehsin Jason Liu
发明人： Marcial Montes de oca , Chi-Hwei Julie Lin , Manuel Ledesma , Yunyan Wang , Fang Xie , Tsehsin Jason Liu
IPC分类号： G06F15/173
CPC分类号： H04L63/10 , G06F21/6218 , G06F2221/2141 , G06Q10/087
摘要： An integration portal provides a user with access to application entities of a plurality of remote applications. An authorization layer included in the integration portal includes a permission map indicating an association between the user and at least one of the application entities of the plurality of remote applications that the user is permitted to access. The authorization layer in the integration portal is synchronized with an authorization layer included in an application portal that provides the user with access to a subset of the remote applications, whereby the permission map is updated with information about at least one of the application entities that the user is permitted to access through the integration portal. Corresponding systems and methods are also disclosed.
摘要翻译：集成门户为用户提供对多个远程应用的应用实体的访问。包括在集成门户中的授权层包括许可图，其指示用户与用户被允许访问的多个远程应用中的至少一个应用实体之间的关联。集成门户中的授权层与包括在应用门户中的授权层同步，该授权层向用户提供对远程应用的一个子集的访问，由此权限映射被更新为关于至少一个应用实体的信息，允许用户通过集成门户访问。还公开了相应的系统和方法。

7. 发明申请

US20090325305A1 DETECTABLE THREADING INTERCALATOR 审中-公开
标题翻译：可检测的螺纹间隔器
公开(公告)号：US20090325305A1
公开(公告)日：2009-12-31
申请号：US12501319
申请日：2009-07-10
申请人： Zhiqiang Gao , Hong Xie , Fang Xie
发明人： Zhiqiang Gao , Hong Xie , Fang Xie
IPC分类号： G01N33/50 , C07F15/00 , C07H21/04
CPC分类号： C07D519/00 , C07F15/0053 , Y10T436/143333
摘要： A threading intercalator of general formula I: IG1-DG-IG2-(DG-IG3)n (I) wherein IG1, IG2, and IG3 are the same or different and represent an intercalating group comprising a planar polyaromatic group; wherein DG represents an electrochemical, a chemiluminescent, a catalytic or an electrochemiluminescent detectable group; and wherein n represents 0 or 1. This invention also relates to a process of detecting a double strand nucleic acid molecule using the threading intercalator.
摘要翻译：通式I的螺旋嵌入剂：IG1-DG-IG2-（DG-IG3）n（I）其中IG1，IG2和IG3相同或不同，表示包含平面多芳基的嵌入基团; 其中DG表示电化学，化学发光，催化或电化学发光可检测组; 并且其中n表示0或1.本发明还涉及使用穿线嵌入剂检测双链核酸分子的方法。

8. 发明授权

US07462720B2 Determination of nucleic acid using electrocatalytic intercalators 失效
标题翻译：使用电催化嵌入剂测定核酸
公开(公告)号：US07462720B2
公开(公告)日：2008-12-09
申请号：US10933023
申请日：2004-09-02
申请人： Fang Xie , Hong Xie , Zhiqiang Gao
发明人： Fang Xie , Hong Xie , Zhiqiang Gao
IPC分类号： C07F15/00 , C12Q1/68
CPC分类号： C07D471/06 , C07F15/0053 , C12Q1/6825 , C12Q2563/173
摘要： Compositions and methods for electrochemical detection of nucleic acid are disclosed. The compositions comprise electrocatalytic intercalators that bind to double-stranded nucleic acid and oxidize nucleic acid. Methods of detecting nucleic acid in a sample comprise forming double-stranded nucleic acid that is bound by electrocatalytic intercalators wherein the intercalators catalyze oxidation of the nucleic acid at the surface of an electrode.
摘要翻译：公开了用于核酸的电化学检测的组合物和方法。组合物包含结合双链核酸并氧化核酸的电催化嵌入剂。检测样品中核酸的方法包括形成由电催化嵌入剂结合的双链核酸，其中嵌入剂催化核酸在电极表面的氧化。

9. 发明授权

US06369517B2 Infrared inductive light switch using triac trigger-control and early-charging-peak current limiter with adjustable power consumption 失效
标题翻译：红外感应灯开关采用三端双向可控硅触发控制和早期充电峰值电流限制器，功耗可调
公开(公告)号：US06369517B2
公开(公告)日：2002-04-09
申请号：US09681273
申请日：2001-03-12
申请人： Qun Song , Jian Li , Fang Xie
发明人： Qun Song , Jian Li , Fang Xie
IPC分类号： G05F100
CPC分类号： H05B39/08 , H05B37/0209 , H05B37/0227 , Y02B20/44 , Y10T307/766
摘要： An electronic switch can replace a standard mechanical light switch for 110-240 volt alternating-current (A.C.) devices. A triac switches the A.C. current to an A.C. device such as a light. A rectifier bridge generates a direct-current (D.C.) voltage that is applied to a special current limiter. The special current limiter generates a large current peak at low voltages, but limits current at high voltages. The large current peak from the special current limiter charges a capacitor when voltage is low at the beginning of each A.C. half-cycle, before the triac turns on. The capacitor has enough charge to supply D.C. current to an Infrared detector and trigger control logic for the rest of the A.C. half-cycle. When the detector detects a person nearby, it signals the trigger control logic. The D.C. voltage from the rectifier bridge is filtered to generate a sync pulse to the trigger control logic when adds a phase delay to the sync pulse which triggers the triac.
摘要翻译：电子开关可以替代110-240伏交流（交流）装置的标准机械灯开关。三端双向可控硅开关将交流电流切换到交直流设备，如灯。整流桥产生施加到特殊限流器的直流（直流）电压。特殊电流限制器在低电压下产生大电流峰值，但限制高电压下的电流。在三端双向可控硅开关导通之前，每个交流电半周期的电压低电平时，特殊电流限制器的大电流峰值将对电容器充电。电容器具有足够的电荷，以将红外线检测器的电流提供给红外检测器，并触发交流半周期的其余部分的触发控制逻辑。当检测器检测到附近的人时，它会发出触发控制逻辑信号。当对触发三端双向可控硅开关元件的同步脉冲添加相位延迟时，来自整流桥的直流电压被滤波以产生到触发控制逻辑的同步脉冲。

10. 发明申请

US20150304825A1 SHORT MESSAGE SENDING METHOD, SHORT MESSAGE SERVICE CENTER AND GATEWAY 有权
标题翻译：短信息发送方式，短消息服务中心和网关
公开(公告)号：US20150304825A1
公开(公告)日：2015-10-22
申请号：US14233858
申请日：2012-05-23
申请人： Hao Wu , Fang Xie
发明人： Hao Wu , Fang Xie
IPC分类号： H04W4/14 , H04L12/58 , H04L12/741 , H04M1/725
CPC分类号： H04W4/14 , H04L45/74 , H04L51/06 , H04M1/72552 , H04W40/02 , H04W88/02 , H04W88/16 , H04W88/184
摘要： A short message sending method, a short message service center (SMS-SC) and a gateway are provided. The short message service center constructs a message body for bearing short message, includes routing information of the short message in this message body, and sends the message body to a short message mobile switching center gateway; after receiving the message body and determining that the message body includes the routing information of the short message, the short message mobile switching center gateway sends the short message to a core network service node according to the routing information. The SMS-SC sends the obtained routing information together with the short message to an SMS-GMSC, so that the SMS-GMSC does not need to request the routing information from an HSS or an HLR, which can reduce the interactive signaling, save the network resources, and optimize the system performance.
摘要翻译：提供短消息发送方法，短消息服务中心（SMS-SC）和网关。短消息服务中心构建用于承载短消息的消息体，包括短消息在该消息体中的路由信息，并将消息体发送到短消息移动交换中心网关; 在接收到消息体并确定消息体包括短消息的路由信息之后，短消息移动交换中心网关根据路由信息将短消息发送到核心网业务节点。 SMS-SC将获取的路由信息与短消息一起发送到SMS-GMSC，使得SMS-GMSC不需要从HSS或HLR请求路由信息，这可以减少交互信令，保存网络资源，优化系统性能。

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