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1. 发明申请

US20120100378A1 PAINT COATING SYSTEM AND METHOD OF PRODUCING MULTILAYERED PAINT COATING 审中-公开
标题翻译：涂料涂料体系和多层涂料涂料的制造方法
公开(公告)号：US20120100378A1
公开(公告)日：2012-04-26
申请号：US13380304
申请日：2010-06-24
申请人： Walter H. Ohrbom , Gregory G. Menovcik , Patrick J. Mormile , Donald H. Campbell , David Cranfill
发明人： Walter H. Ohrbom , Gregory G. Menovcik , Patrick J. Mormile , Donald H. Campbell , David Cranfill
IPC分类号： B32B27/36 , B05D3/02 , B32B27/38
CPC分类号： B05D1/36 , B05D7/52 , C09D4/00 , Y10T428/31507 , Y10T428/31515 , Y10T428/31536
摘要： A paint coating system comprises a substrate and a first paint layer disposed on the substrate. The first paint layer is formed from a first composition comprising either a first decomplexing agent or a first organoborane complex. The paint coating system further comprises a second paint layer disposed on the first paint layer. The second paint layer is formed from a second composition comprising the other of the first decomplexing agent and the first organoborane complex. At least one of the first and second compositions further comprises a radical polymerizable compound. A method of producing a multilayered paint coating includes the steps of providing the substrate, applying a first paint layer on the substrate, applying a second paint layer on the first paint layer, and curing the at least one of the first and second paint layers.
摘要翻译：涂料系统包括基材和设置在基材上的第一涂料层。第一涂料层由包含第一解络剂或第一有机硼烷络合物的第一组合物形成。涂料系统还包括设置在第一涂料层上的第二涂料层。第二涂层由第二组合物形成，第二组合物包含第一解络剂和第一有机硼烷络合物中的另一种。第一和第二组合物中的至少一种还包含自由基聚合性化合物。制造多层涂料涂料的方法包括以下步骤：提供基材，在基材上施加第一涂料层，在第一涂料层上施加第二涂料层，并固化第一和第二涂料层中的至少一个。

2. 发明授权

US08906507B2 Coating system for achieving excellent MVSS adhesion 有权
标题翻译：涂层系统可实现优异的MVSS粘附力
公开(公告)号：US08906507B2
公开(公告)日：2014-12-09
申请号：US12516836
申请日：2008-02-13
申请人： Donald H. Campbell , Gregory G. Menovcik , David J. Santure , Walter H. Ohrbom , Donald St. Aubin , Paul J. Harris
发明人： Donald H. Campbell , Gregory G. Menovcik , David J. Santure , Walter H. Ohrbom , Donald St. Aubin , Paul J. Harris
IPC分类号： B32B27/08 , B32B27/40 , C08G18/00 , B05D7/00 , C09D201/02
CPC分类号： B05D7/576 , B05D2202/15 , C09D201/025 , Y10T428/31551 , C08L2666/16
摘要： A coating system includes a clear coat layer and a sealant. The clear coat layer is formed from a clear coat composition that comprises a crosslinkable carbamate-functional resin and an aminoplast. Optionally, the coating system further includes a sub-clear coat layer. The sealant is bonded to the clear coat layer opposite the sub-clear coat layer. Optionally, the coating system further includes a tie coat layer and that is disposed between the sealant and the clear coat layer. An adhesion promoter is present in the clear coat composition in an amount of less than or equal to about 3% by weight based on the total weight of resin solids of the clear coat composition. Further, the adhesion promoter is present in at least one of the sub-clear coat composition and the tie coat composition in an amount sufficient to increase adhesion between the clear coat layer and the sealant.
摘要翻译：涂层系统包括透明涂层和密封剂。透明涂层由透明涂层组合物形成，该组合物包含可交联的氨基甲酸酯官能树脂和氨基塑料。任选地，涂层系统还包括副透明涂层。密封剂粘合到与透明涂层相对的透明涂层。任选地，涂层系统还包括粘结涂层，并且设置在密封剂和透明涂层之间。基于透明涂料组合物的树脂固体的总重量，粘合促进剂以小于或等于约3重量％的量存在于透明涂料组合物中。此外，粘合促进剂以足以增加透明涂层和密封剂之间的粘合力的量存在于至少一种亚透明涂料组合物和粘合涂层组合物中。

3. 发明申请

US20100183882A1 Coating System For Achieving Excellent MVSS Adhesion 有权
标题翻译：涂层体系可实现优异的MVSS粘合力
公开(公告)号：US20100183882A1
公开(公告)日：2010-07-22
申请号：US12516836
申请日：2008-02-13
申请人： Donald H. Campbell , Gregory G. Menovcik , David J. Santure , Walter H. Ohrbom , Donald St. Aubin , Paul J. Harris
发明人： Donald H. Campbell , Gregory G. Menovcik , David J. Santure , Walter H. Ohrbom , Donald St. Aubin , Paul J. Harris
IPC分类号： B32B27/08 , B32B27/40 , B05D1/36
CPC分类号： B05D7/576 , B05D2202/15 , C09D201/025 , Y10T428/31551 , C08L2666/16
摘要： A coating system includes a clear coat layer and a sealant. The clear coat layer is formed from a clear coat composition that comprises a crosslinkable carbamate-functional resin and an aminoplast. Optionally, the coating system further includes a sub-clear coat layer that is formed from a sub-clear coat composition. The sealant is bonded to the clear coat layer opposite the sub-clear coat layer. Optionally, the coating system further includes a tie coat layer that is formed from a tie coat composition and that is disposed between the sealant and the clear coat layer. An adhesion promoter is present in the clear coat composition in an amount of less than or equal to about 3% by weight based on the total weight of resin solids of the clear coat composition. Further, the adhesion promoter is present in at least one of the sub-clear coat composition and the tie coat composition in an amount sufficient to increase adhesion between the clear coat layer and the sealant.
摘要翻译：涂层系统包括透明涂层和密封剂。透明涂层由透明涂层组合物形成，该组合物包含可交联的氨基甲酸酯官能树脂和氨基塑料。任选地，涂层系统还包括由亚透明涂层组合物形成的副透明涂层。密封剂粘合到与透明涂层相对的透明涂层上。任选地，涂层系统还包括由粘结涂层组合物形成并且设置在密封剂和透明涂层之间的粘结涂层。基于透明涂料组合物的树脂固体的总重量，粘合促进剂以小于或等于约3重量％的量存在于透明涂料组合物中。此外，粘合促进剂以足以增加透明涂层和密封剂之间的粘合力的量存在于至少一种亚透明涂料组合物和粘合涂层组合物中。

4. 发明授权

US08653183B2 Method of curing a coating composition comprising a radical curable compound and an organoborane-amine complex 有权
标题翻译：固化包含自由基固化性化合物和有机硼烷 - 胺络合物的涂料组合物的方法
公开(公告)号：US08653183B2
公开(公告)日：2014-02-18
申请号：US13380255
申请日：2010-06-22
申请人： Keith E. Gutowski , Walter H. Ohrbom , David Cranfill , Donald H. Campbell
发明人： Keith E. Gutowski , Walter H. Ohrbom , David Cranfill , Donald H. Campbell
IPC分类号： C09D7/12 , B05D7/24 , B05D3/10 , C09D4/02 , C09D133/08
CPC分类号： C09D133/08 , C08J3/24 , C08K5/55 , C09D4/00
摘要： A method of curing a coating composition and a method of forming a cured coating on an automobile component are provided. The coating composition comprises a radical polymerizable compound and an organoborane-amine complex having an organoborane initiator, an amine blocking agent, and water. The method of curing the coating composition comprises the steps of combining the organoborane-amine complex, the radical polymerizable compound, and water to form the coating composition. Carbon dioxide is introduced into the coating composition or into a composition including at least one of the organoborane-amine complex, the radical polymerizable compound, and water prior to forming the coating composition. Carbonic acid is formed in situ within the coating composition through reaction of the water and carbon dioxide. The organoborane-amine complex is decomplexed with the carbonic acid thereby separating the organoborane initiator and the amine blocking agent. The radical polymerizable compound is polymerized using the organoborane initiator in the presence of oxygen.
摘要翻译：提供固化涂料组合物的方法和在汽车部件上形成固化涂层的方法。涂料组合物包含可自由基聚合的化合物和具有有机硼烷引发剂，胺封闭剂和水的有机硼烷 - 胺络合物。固化涂料组合物的方法包括将有机硼烷 - 胺络合物，可自由基聚合的化合物和水组合以形成涂料组合物的步骤。在形成涂料组合物之前，将二氧化碳引入涂料组合物或包含至少一种有机硼烷 - 胺络合物，可自由基聚合的化合物和水的组合物。碳酸通过水和二氧化碳的反应在涂料组合物中原位形成。有机硼烷 - 胺络合物与碳酸分解，从而分离有机硼烷引发剂和胺封闭剂。使用有机硼烷引发剂在氧的存在下使自由基聚合性化合物聚合。

5. 发明申请

US20120116013A1 METHOD OF CURING A COATING COMPOSITION COMPRISING A RADICAL CURABLE COMPOUND AND AN ORGANOBORANE-AMINE COMPLEX 有权
标题翻译：固化包含耐光固化性化合物的涂料组合物和有机硼 - 胺复合物的方法
公开(公告)号：US20120116013A1
公开(公告)日：2012-05-10
申请号：US13380255
申请日：2010-06-22
申请人： Keith E. Gutowski , Walter H. Ohrbom , David Cranfill , Donald H. Campbell
发明人： Keith E. Gutowski , Walter H. Ohrbom , David Cranfill , Donald H. Campbell
IPC分类号： C09D7/12 , B05D7/24 , B05D3/10 , C09D4/02 , C09D133/08
CPC分类号： C09D133/08 , C08J3/24 , C08K5/55 , C09D4/00
摘要： A method of curing a coating composition and a method of forming a cured coating on an automobile component are provided. The coating composition comprises a radical polymerizable compound and an organoborane-amine complex having an organoborane initiator, an amine blocking agent, and water. The method of curing the coating composition comprises the steps of combining the organoborane-amine complex, the radical polymerizable compound, and water to form the coating composition. Carbon dioxide is introduced into the coating composition or into a composition including at least one of the organoborane-amine complex, the radical polymerizable compound, and water prior to forming the coating composition. Carbonic acid is formed in situ within the coating composition through reaction of the water and carbon dioxide. The organoborane-amine complex is de-complexed with the carbonic acid thereby separating the organoborane initiator and the amine blocking agent. The radical polymerizable compound is polymerized using the organoborane initiator in the presence of oxygen.
摘要翻译：提供固化涂料组合物的方法和在汽车部件上形成固化涂层的方法。涂料组合物包含可自由基聚合的化合物和具有有机硼烷引发剂，胺封闭剂和水的有机硼烷 - 胺络合物。固化涂料组合物的方法包括将有机硼烷 - 胺络合物，可自由基聚合的化合物和水组合以形成涂料组合物的步骤。在形成涂料组合物之前，将二氧化碳引入涂料组合物或包含至少一种有机硼烷 - 胺络合物，可自由基聚合的化合物和水的组合物。碳酸通过水和二氧化碳的反应在涂料组合物中原位形成。有机硼烷 - 胺络合物与碳酸脱配合，从而分离有机硼烷引发剂和胺封闭剂。使用有机硼烷引发剂在氧气存在下使自由基聚合性化合物聚合。

6. 发明授权

US06531560B1 Carbamate-functional resins having improved adhesion, method of making the same, and method of improving intercoat adhesion 有权
公开(公告)号：US06531560B1
公开(公告)日：2003-03-11
申请号：US09677063
申请日：2000-09-29
申请人： Donald H. Campbell , Walter H. Ohrbom , Joseph Borst , Michael A. Gessner , Donald L. St. Aubin , Marvin L. Green , Bruce E. Oermann
发明人： Donald H. Campbell , Walter H. Ohrbom , Joseph Borst , Michael A. Gessner , Donald L. St. Aubin , Marvin L. Green , Bruce E. Oermann
IPC分类号： C08F12602
CPC分类号： C08G18/8116 , C08F8/00 , C08F2800/20 , C08F2810/50 , C08G18/3823 , C09D201/025 , Y10T428/31551 , Y10T428/31573 , Y10T428/31645 , C08F2220/325 , C08F220/34 , C08F220/20 , C08F212/08
摘要： The invention provides carbamate-functional resins and coating compositions incorporating said resins that have improved adhesion with respect to subsequently applied films or coatings. More particularly, the invention relates to carbamate-functional addition polymers having at least 250 grams of polymer per carbamate group which are made with less than 35 percent by weight of nonfunctional monomers, preferably with less than 20 percent by weight and most preferably from 0 to less than 10 percent by weight, based on the total weight of the polymer. The invention further provides a method of making a carbamate-functional polymer and carbamate-functional polymers made by the claimed method. Finally, the invention provides a method for improving the adhesion of a first coating composition to a subsequently applied material as well as a method of making a composite comprising a coated substrate, an adhesive composition, and a glass having at least one surface.

7. 发明授权

US07989070B2 Coating composition for achieving excellent MVSS adhesion 有权
标题翻译：用于实现优异的MVSS粘附的涂料组合物
公开(公告)号：US07989070B2
公开(公告)日：2011-08-02
申请号：US11960815
申请日：2007-12-20
申请人： Donald H. Campbell , Gregory G. Menovcik , Timothy S. December
发明人： Donald H. Campbell , Gregory G. Menovcik , Timothy S. December
IPC分类号： C08G18/32
CPC分类号： C09D161/28 , C08G2190/00 , C08L61/28 , C08L75/04 , C09D175/04 , Y10T428/265 , Y10T428/31511 , Y10T428/31551 , Y10T428/31601 , Y10T428/31928 , C08L2666/20 , C08L2666/16
摘要： A coating composition comprises a crosslinkable carbamate-functional resin and an aminoplast. The aminoplast comprises the reaction product of an aldehyde and a melamine. The aminoplast has a content of imino groups of less than or equal to about 10%, a content of alkylol groups of at least about 7%, and a remainder of groups being alkoxyalkyl groups, all based on a total number of reactive sites present in the melamine prior to reaction. A coating system includes a clear coat layer that comprises the reaction product of the crosslinkable carbamate-functional resin and the aminoplast. Threshold adhesion strength, in accordance with MVSS standards, can be achieved between glass and the coating system when the crosslinkable carbamate-functional resin and the specific aminoplast set forth above are reacted to form the clear coat layer, while minimizing problems associated with high viscosity of aminoplasts having a high content of imino groups of greater than 10%.
摘要翻译：涂料组合物包含可交联的氨基甲酸酯官能树脂和氨基塑料。氨基塑料包括醛和三聚氰胺的反应产物。氨基塑料具有小于或等于约10％的亚氨基的含量，至少约7％的羟烷基的含量，剩余的基团是烷氧基烷基，全部基于存在于反应前的三聚氰胺。涂层系统包括透明涂层，其包含可交联的氨基甲酸酯官能树脂与氨基塑料的反应产物。当可交联的氨基甲酸酯官能树脂和上述特定的氨基塑料反应形成透明涂层时，玻璃和涂层体系之间可以实现根据MVSS标准的阈值粘附强度，同时最小化与高粘度具有大于10％的亚氨基的高含量的氨基塑料。

8. 发明申请

US20100104769A1 AUTOMOTIVE COATING SURFACE ENHANCEMENT USING A PLASMA TREATMENT TECHNIQUE 审中-公开
标题翻译：使用等离子体处理技术的汽车涂料表面增强
公开(公告)号：US20100104769A1
公开(公告)日：2010-04-29
申请号：US12257126
申请日：2008-10-23
申请人： John E. Boisseau , Donald H. Campbell , Paul Deskovitz , Patrick J. Mormile
发明人： John E. Boisseau , Donald H. Campbell , Paul Deskovitz , Patrick J. Mormile
IPC分类号： H05H1/24 , A61N5/00
CPC分类号： B05D7/14 , B05D1/62 , B05D3/148 , B05D7/53
摘要： A technique of treating an automotive coating to modify surface-specific physical properties thereof while retaining bulk physical properties of the automotive coating includes the step of generating a plasma discharge in a plasma generating assembly. The automotive coating is treated with the plasma discharge. The automotive coating is completely cured prior to treatment with the plasma discharge. To treat the automotive coating, either 1) a precursor material is introduced into the plasma discharge to form a thin film on the automotive coating, or 2) the plasma discharge is free of a precursor material and weak bonds are destroyed on or near the surface of the automotive coating.
摘要翻译：一种处理汽车涂层以修饰其表面特定物理性能同时保持汽车涂料的大量物理性质的技术包括在等离子体产生组件中产生等离子体放电的步骤。汽车涂层用等离子体放电处理。在用等离子体放电处理之前，汽车涂层完全固化。为了处理汽车涂层，要么1）将前体材料引入等离子体放电中以在汽车涂层上形成薄膜，或者2）等离子体放电不含前体材料，并且弱键在表面或附近被破坏的汽车涂料。

9. 发明申请

US20080124472A1 Clearcoating composition with unblocked acid catalyst 审中-公开
标题翻译：具有未封端的酸催化剂的透漆组合物
公开(公告)号：US20080124472A1
公开(公告)日：2008-05-29
申请号：US11998295
申请日：2007-11-29
申请人： David K. Lau , Donald H. Campbell , Gregory G. Menovcik
发明人： David K. Lau , Donald H. Campbell , Gregory G. Menovcik
IPC分类号： B05D3/00
CPC分类号： C09D5/00 , C08K5/42 , C08K5/521 , C08L61/28 , C09D167/00 , C08L2666/16
摘要： A two-component solvent-borne clearcoat composition comprising an unblocked acid catalyst, a film-forming binder, and an aminoplast crosslinking agent (e.g., a melamine formaldehyde crosslinking agent) surprisingly provides enhanced appearance when compared to a one-component clearcoating composition containing blocked acid catalyst cured at temperatures above 121° C. (250° F.).
摘要翻译：包含未封端的酸催化剂，成膜粘合剂和氨基塑料交联剂（例如，三聚氰胺甲醛交联剂）的双组分溶剂型透明涂料组合物与含有封闭的单组分澄清涂层组合物相比令人惊讶地提供了增强的外观酸催化剂在121°C（250°F）以上固化。

10. 发明授权

US07232863B2 Functional addition polymers and a method for their preparation 有权
标题翻译：官能加成聚合物及其制备方法
公开(公告)号：US07232863B2
公开(公告)日：2007-06-19
申请号：US10957568
申请日：2004-10-01
申请人： Walter H. Ohrbom , Donald H. Campbell , Donald L. St. Aubin , Swaminathan Ramesh , Paul J. Harris , Ulrike Röckrath
发明人： Walter H. Ohrbom , Donald H. Campbell , Donald L. St. Aubin , Swaminathan Ramesh , Paul J. Harris , Ulrike Röckrath
IPC分类号： C08F8/14
CPC分类号： C08F222/20 , C08F8/14 , C08F220/06 , C08F220/08 , C08F222/22 , C08G18/00 , C09D201/025 , Y10T428/31511 , C08F265/06
摘要： Disclosed is a method for making nongelled functional addition polymers from linear unsaturated anhydrides. The method subjects a linear unsaturated anhydride compound, an active hydrogen compound, and an epoxide compound to reaction conditions such that each of the following three reactions occur: (i) polymerization of polymerizable C═C bonds, (ii) ring opening of an anhydride functional group of the linear unsaturated anhydride compound by the active hydrogen compound to create an acid functional group, and (iii) reaction of the acid functional group resulting from the anhydride ring opening with the epoxide compound. At the time of reaction (iii), the acid functional group resulting from the anhydride ring opening may be selected from an ethylenically unsaturated monomer, a polymer, or both. In one embodiment, the method does not include the physical removal of any acid functional monomers or polymerization products. Also disclosed are a curable coating composition and a coated substrate.
摘要翻译：公开了一种从线性不饱和酸酐制造非功能性加成聚合物的方法。该方法使线性不饱和酸酐化合物，活性氢化合物和环氧化合物反应，使得发生以下三个反应中的每一个：（i）可聚合的CC键的聚合，（ii）酸酐官能团的开环的线性不饱和酸酐化合物，以产生酸官能团，和（iii）由酸酐开环产生的酸官能团与环氧化合物的反应。在反应（iii）时，由酸酐开环产生的酸官能团可以选自烯属不饱和单体，聚合物或两者。在一个实施方案中，该方法不包括物理去除任何酸官能单体或聚合产物。还公开了可固化涂料组合物和涂布的基材。

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