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1. 发明申请

US20110020213A1 TITANIUM OXIDE AND METHOD OF PRODUCING THE SAME 审中-公开
标题翻译：氧化钛及其制造方法
公开(公告)号：US20110020213A1
公开(公告)日：2011-01-27
申请号：US12811611
申请日：2008-12-26
申请人： Tsutomu Mashimo , Omurzak Uulu Emil , Sulaimankulova Saadat , Makoto Okamoto , Hideharu Iwasaki
发明人： Tsutomu Mashimo , Omurzak Uulu Emil , Sulaimankulova Saadat , Makoto Okamoto , Hideharu Iwasaki
IPC分类号： C01G23/047 , C01G23/04 , C25B1/00
CPC分类号： C23C30/00 , B01J21/063 , B01J35/004 , B01J37/348 , B82Y30/00 , C01G23/047 , C01G23/08 , C01P2002/72 , C01P2002/82 , C01P2002/84 , C01P2002/88 , C01P2004/04 , C01P2004/64 , C01P2006/37 , C01P2006/82 , C23C8/10 , C23C8/36 , C23C26/00 , C25D11/026 , C25D11/26
摘要： An object is to provide a novel anatase titanium oxide having especially high photocatalytic activity as a photocatalyst useful as a material for environmental clean-up, such as removal of toxic substances, deodorization and decomposition of malodorous substances, prevention of fouling and sterilization, and a method of producing such an anatase titanium oxide.There is provided a titanium oxide having a reflectance of 80% or lower with respect to light having a wavelength of 400 nm to 700 nm. There is also provided a method of producing an anatase titanium oxide, comprising creating pulsed plasma by an electric current of lower than 5 amperes between titanium electrodes in water to oxidize a titanium. Preferably, the titanium oxide has a percentage weight loss of 1.0% or lower when heated at a temperature within the range of 400° C. to 800° C., and has the anatase structure or the anatase and rutile structures.
摘要翻译：目的是提供具有特别高的光催化活性的新颖锐钛矿型氧化钛，作为可用作环境净化材料的光催化剂，例如去除有毒物质，除臭和分解恶臭物质，防止结垢和灭菌。生产这种锐钛矿型氧化钛的方法。提供了相对于波长为400nm〜700nm的光，其反射率为80％以下的氧化钛。还提供了一种生产锐钛矿型氧化钛的方法，包括通过在水中钛电极之间的电流低于5安培的电流产生脉冲等离子体以氧化钛。优选地，当在400℃至800℃的温度范围内加热时，氧化钛的重量百分比损失为1.0％或更低，并且具有锐钛矿结构或锐钛矿和金红石结构。

2. 发明授权

US08551363B2 Method of producing group II-VI compound semiconductor, method of producing group II-VI compound semiconductor phosphor, and hexagonal group II-VI compound semiconductor 失效
标题翻译： II-VI族化合物半导体的制造方法，II-VI族化合物半导体荧光体的制造方法以及六方晶系II-VI族化合物半导体
公开(公告)号：US08551363B2
公开(公告)日：2013-10-08
申请号：US12866561
申请日：2009-02-05
申请人： Tsutomu Mashimo , Omurzak Uulu Emil , Makoto Okamoto , Hideharu Iwasaki
发明人： Tsutomu Mashimo , Omurzak Uulu Emil , Makoto Okamoto , Hideharu Iwasaki
IPC分类号： C09K11/54 , C09K11/56
CPC分类号： C01G9/08 , C01P2002/50 , C01P2002/52 , C01P2002/72 , C01P2004/04 , C01P2006/40 , C01P2006/88 , C09K11/565 , C09K11/574 , C09K11/584 , C25B1/00 , Y10T428/24355
摘要： A method of producing a Group II-VI compound semiconductor. The method involves generating a pulsed electrical discharge plasma between metallic electrodes in sulfur to produce a Group II-VI compound semiconductor. A method of producing a Group II-VI compound semiconductor phosphor using a pulsed electrical discharge plasma. A hexagonal crystal of Group II-VI compound semiconductor composed of a plurality of twin crystals.
摘要翻译：一种制备II-VI族化合物半导体的方法。该方法包括在硫的金属电极之间产生脉冲放电等离子体以产生II-VI族化合物半导体。使用脉冲放电等离子体制造II-VI族化合物半导体荧光体的方法。由多个双晶组成的II-VI族化合物半导体的六方晶体。

3. 发明授权

US09302917B2 Low valence titanium oxides and method of producing the same 有权
标题翻译：低价钛氧化物及其制造方法
公开(公告)号：US09302917B2
公开(公告)日：2016-04-05
申请号：US13255179
申请日：2010-03-11
申请人： Tsutomu Mashimo , Omurzak Uulu Emil , Naoto Kameyama , Makoto Okamoto , Yoshiaki Yasuda , Hideharu Iwasaki
发明人： Tsutomu Mashimo , Omurzak Uulu Emil , Naoto Kameyama , Makoto Okamoto , Yoshiaki Yasuda , Hideharu Iwasaki
IPC分类号： C01G23/04 , C25B1/00
CPC分类号： C01G23/043 , C01P2002/72 , C01P2002/82 , C01P2002/88 , C01P2006/40 , C25B1/00
摘要： The object of the present invention is to provide a method of producing low valence titanium oxides in a steady supply manner acceptable in industrial production. The low valence titanium oxides are produced by electrical discharge between two electrodes in an aqueous medium, wherein at least one of the electrodes is a titanium-containing electrode.
摘要翻译：本发明的目的是提供一种以工业生产中可接受的稳定供给方式生产低价钛氧化物的方法。低价钛氧化物通过水性介质中的两个电极之间的放电产生，其中至少一个电极是含钛电极。

4. 发明申请

US20120027668A1 LOW VALENCE TITANIUM OXIDES AND METHOD OF PRODUCING THE SAME 有权
标题翻译：低价钛金属氧化物及其生产方法
公开(公告)号：US20120027668A1
公开(公告)日：2012-02-02
申请号：US13255179
申请日：2010-03-11
申请人： Tsutomu Mashimo , Omurzak Uulu Emil , Naoto Kameyama , Makoto Okamoto , Yoshiaki Yasuda , Hideharu Iwasaki
发明人： Tsutomu Mashimo , Omurzak Uulu Emil , Naoto Kameyama , Makoto Okamoto , Yoshiaki Yasuda , Hideharu Iwasaki
IPC分类号： C01G23/04 , C25B11/04 , C25B1/00
CPC分类号： C01G23/043 , C01P2002/72 , C01P2002/82 , C01P2002/88 , C01P2006/40 , C25B1/00
摘要： The object of the present invention is to provide a method of producing low valence titanium oxides in a steady supply manner acceptable in industrial production. The low valence titanium oxides are produced by electrical discharge between two electrodes in an aqueous medium, wherein at least one of the electrodes is a titanium-containing electrode.
摘要翻译：本发明的目的是提供一种以工业生产中可接受的稳定供给方式生产低价钛氧化物的方法。低价钛氧化物通过在水性介质中的两个电极之间的放电产生，其中至少一个电极是含钛电极。

5. 发明申请

US20100320426A1 METHOD OF PRODUCING GROUP II-VI COMPOUND SEMICONDUCTOR, METHOD OF PRODUCING GROUP II-VI COMPOUND SEMICONDUCTOR PHOSPHOR, AND HEXAGONAL GROUP II-VI COMPOUND SEMICONDUCTOR 失效
标题翻译：制备II-VI族化合物半导体的方法，生产II-VI族化合物半导体磷光体的方法，和六角II-VI族化合物半导体
公开(公告)号：US20100320426A1
公开(公告)日：2010-12-23
申请号：US12866561
申请日：2009-02-05
申请人： Tsutomu Mashimo , Omurzak Uulu Emil , Makoto Okamoto , Hideharu Iwasaki
发明人： Tsutomu Mashimo , Omurzak Uulu Emil , Makoto Okamoto , Hideharu Iwasaki
IPC分类号： H01B1/10 , C01G9/08 , H05F3/06
CPC分类号： C01G9/08 , C01P2002/50 , C01P2002/52 , C01P2002/72 , C01P2004/04 , C01P2006/40 , C01P2006/88 , C09K11/565 , C09K11/574 , C09K11/584 , C25B1/00 , Y10T428/24355
摘要： An object of the invention is to provide a method for the stable production of a high-purity Group II-VI compound semiconductor on an industrial scale, and also a hexagonal crystal of Group II-VI compound semiconductor in which a metal can be doped easily. Another object of the invention is to provide a method of producing a Group II-VI compound semiconductor phosphor.The objects are achieved by a method of producing a Group II-VI compound semiconductor comprising generating a pulsed electrical discharge plasma between metallic electrodes in sulfur to produce a Group II-VI compound semiconductor; a method of producing a Group II-VI compound semiconductor phosphor using a pulsed electrical discharge plasma; and a hexagonal crystal of Group II-VI compound semiconductor composed of a plurality of twin crystals.
摘要翻译：本发明的目的是提供一种在工业规模上稳定生产高纯度II-VI族化合物半导体的方法，以及其中易于掺杂金属的II-VI族化合物半导体的六方晶。本发明的另一个目的是提供一种制备II-VI族化合物半导体荧光体的方法。目的是通过生产II-VI族化合物半导体的方法来实现，其包括在硫的金属电极之间产生脉冲放电等离子体以产生II-VI族化合物半导体; 使用脉冲放电等离子体制造II-VI族化合物半导体荧光体的方法; 以及由多个双晶组成的II-VI族化合物半导体的六方晶。

6. 发明授权

US08188299B2 Acrylate derivatives, alcohol derivatives, and method for producing them 有权
标题翻译：丙烯酸酯衍生物，醇衍生物及其制备方法
公开(公告)号：US08188299B2
公开(公告)日：2012-05-29
申请号：US12884677
申请日：2010-09-17
申请人： Kazuya Shimizu , Masayoshi Yamanaka , Tatsuhiko Hayashibara , Hideharu Iwasaki
发明人： Kazuya Shimizu , Masayoshi Yamanaka , Tatsuhiko Hayashibara , Hideharu Iwasaki
IPC分类号： C07D209/56
CPC分类号： C07D209/02 , C07D491/18
摘要： Provided are an acrylate derivative useful as a raw material of a polymer compound for resist compositions capable of giving resist patterns which are excellent in lithographic performance and have a good shape, an intermediate thereof (alcohol derivative) and production processes for them. To be specific, it is an acrylate derivative represented by a formula shown below: (wherein R1 represents a hydrogen atom, methyl or trifluoromethyl; R2, R3, R5, R7, R8, R9 and R10 each represent independently a hydrogen atom, an alkyl group having 1 to 6 carbon atoms, a cycloalkyl group having 3 to 6 carbon atoms or an alkoxy group having 1 to 6 carbon atoms; R4 and R6 each represent independently a hydrogen atom, an alkyl group having 1 to 6 carbon atoms, a cycloalkyl group having 3 to 6 carbon atoms or an alkoxy group having 1 to 6 carbon atoms, or both of R4 and R6 are combined to represent an alkylene group having 1 to 3 carbon atoms, —O— or —S—; and R11 represents a hydrogen atom, an alkyl group having 1 to 6 carbon atoms or a cyclic hydrocarbon group having 3 to 10 carbon atoms).
摘要翻译：提供可用作抗蚀剂组合物的聚合物化合物的原料的丙烯酸酯衍生物，其能够提供平版印刷性能优异且形状良好的抗蚀剂图案，其中间体（醇衍生物）及其制备方法。具体来说，它是由下式表示的丙烯酸酯衍生物：其中R1表示氢原子，甲基或三氟甲基; R2，R3，R5，R7，R8，R9和R10各自独立地表示氢原子，烷基具有1至6个碳原子的基团，具有3至6个碳原子的环烷基或具有1至6个碳原子的烷氧基; R 4和R 6各自独立地表示氢原子，具有1至6个碳原子的烷基，环烷基具有3至6个碳原子的烷基或具有1至6个碳原子的烷氧基，或者R 4和R 6都被结合以表示具有1至3个碳原子的亚烷基，-O-或-S-; R 11表示氢原子，碳原子数1〜6的烷基或碳原子数3〜10的环状烃基）。

7. 发明授权

US08110124B2 Method of preparing fluorescent body precursor 有权
标题翻译：制备荧光体前体的方法
公开(公告)号：US08110124B2
公开(公告)日：2012-02-07
申请号：US12373989
申请日：2007-07-26
申请人： Yoshihisa Tsuji , Hideharu Iwasaki
发明人： Yoshihisa Tsuji , Hideharu Iwasaki
IPC分类号： C09K11/56
CPC分类号： C09K11/7702 , C01G9/00 , C01G9/006 , C01G9/08 , C01G45/006 , C01G45/02 , C01P2002/52 , C01P2002/72 , C01P2006/80 , C09K11/574 , C09K11/876
摘要： To produce fluorescent bodies providing high brightness and high energy efficiency, a method of preparing a fluorescent body precursor is provided to enable an activator having a large ionic radius to be doped arbitrarily. The problems described above are solved by a method of preparing a fluorescent body precursor, which method is characterized by comprising applying a shock pressure of 0.1 GPa or higher to a mixture consisting essentially of a fluorescent body base, an activator and a co-activating particle-growth promoter to dope the activator into the fluorescent body base in the presence of the co-activating particle-growth promoter.
摘要翻译：为了产生提供高亮度和高能量效率的荧光体，提供了制备荧光体前体的方法，以使得具有大离子半径的活化剂能够被任意掺杂。上述问题是通过制备荧光体前体的方法来解决的，该方法的特征在于包括对基本上由荧光体碱，活化剂和共活化颗粒组成的混合物施加0.1GPa或更高的冲击压力生长促进剂，在共活化的颗粒生长促进剂存在下将活化剂掺入荧光体碱中。

8. 发明申请

US20110147663A1 METHOD FOR PRODUCING ZINC SULFIDE BASED PHOSPHOR 失效
标题翻译：生产基于硫化锌的磷光体的方法
公开(公告)号：US20110147663A1
公开(公告)日：2011-06-23
申请号：US13057168
申请日：2009-07-30
申请人： Yoshihisa Tsuji , Kazuma Inoue , Jun Takai , Hideharu Iwasaki
发明人： Yoshihisa Tsuji , Kazuma Inoue , Jun Takai , Hideharu Iwasaki
IPC分类号： C09K11/56
CPC分类号： C09K11/625 , C09K11/876 , H05B33/14
摘要： The present invention provides a method for producing a zinc sulfide based phosphor by firing a zinc sulfide based phosphor precursor, comprising at least: a first firing step of firing a mixture containing a zinc sulfide based phosphor precursor, sulfur, and a chlorine-containing flux; and a second firing step of further firing the fired product obtained from the first firing step, wherein the first firing step comprises: heating the mixture in an atmosphere wherein an air stream is introduced so that a temperature of the mixture is increased from normal temperature to a transformation temperature at which a crystal system of the phosphor precursor is transformed; when a temperature of the mixture is increased above the transformation temperature, switching the atmosphere to a nitrogen atmosphere and continuing the heating of the mixture; and when the temperature of the mixture reaches a temperature in a range of 1000° C. to 1200° C., inclusive, maintaining the temperature of the mixture at a constant level and thereafter rapidly quenching the mixture and washing the mixture to obtain a fired product; and wherein the second firing step comprises heating in the nitrogen atmosphere the fired product obtained from the first firing step so that the temperature of the fired product is increased from normal temperature to a temperature in a range of 650° C. to 1000° C., inclusive; and when a temperature of the fired product reaches the temperature in the range of 650° C. to 1000° C., inclusive, introducing oxygen while maintaining the temperature of the fired product and thereafter rapidly quenching the fired product and washing the fired product to obtain a zinc sulfide based phosphor. Use of the method of the present invention makes it possible to provide a zinc sulfide based phosphor material suitable for use in the production of an EL device that shows high brightness.
摘要翻译：本发明提供了一种通过焙烧硫化锌系荧光体前体来制造硫化锌系荧光体的方法，该方法至少包括：将含有硫化锌系荧光体前体，硫和含氯助熔剂的混合物进行烧成的第一烧成工序 ; 以及第二烧成工序，对从所述第一烧成工序得到的烧成品进一步进行烧成，其中，所述第一烧成工序包括：在导入空气流的气氛中加热所述混合物，使得所述混合物的温度从常温升高到改变荧光体前体的晶体体系的相变温度; 当混合物的温度升高到转化温度以上时，将气氛切换至氮气氛并继续加热混合物; 并且当混合物的温度达到1000℃至1200℃的范围内的温度时，将混合物的温度保持在恒定水平，然后快速骤冷混合物并洗涤该混合物以获得烧制产品; 并且其中所述第二烧制步骤包括在所述氮气气氛中加热从所述第一烧制步骤获得的烧制产品，使得所述烧制产品的温度从常温升高至650℃至1000℃的温度。，包括的; 并且当烧制品的温度达到650℃至1000℃的温度时，在保持烧制产品的温度的同时引入氧气，然后迅速骤冷烧制产品并将烧制产品洗涤至得到硫化锌系荧光体。通过使用本发明的方法，可以提供一种适用于制造高亮度的EL器件的硫化锌系荧光体材料。

9. 发明授权

US07709415B2 Method for manufacturing activated carbon, polarizable electrode, and electric double-layered capacitor 失效
标题翻译：活性炭，极化电极和双电层电容器的制造方法
公开(公告)号：US07709415B2
公开(公告)日：2010-05-04
申请号：US10509087
申请日：2003-04-22
申请人： Nozomu Sugo , Hideharu Iwasaki , Takanori Kitamura , Tatsuo Morotomi , Tsuyoshi Kowaka , Teruhiro Okada , Shushi Nishimura , Takeshi Fujino , Shigeki Oyama , Yuji Kawabuchi
发明人： Nozomu Sugo , Hideharu Iwasaki , Takanori Kitamura , Tatsuo Morotomi , Tsuyoshi Kowaka , Teruhiro Okada , Shushi Nishimura , Takeshi Fujino , Shigeki Oyama , Yuji Kawabuchi
IPC分类号： C01B31/08
CPC分类号： H01G9/155 , C01B32/342 , H01M4/0471 , H01M4/583 , Y02E60/13
摘要： Activated carbon useful as polarizable electrode material for an electric double-layer capacitor can be obtained by mixing a carbonaceous material and an alkali metal hydroxide while maintaining a solid state, granulating the obtained mixture while maintaining its solid state, dehydrating the obtained granulated substance while maintaining its solid state, and subjecting the granulated dehydration product obtained in the dehydration step to an activation treatment. The preferred pressure of the granulation treatment in the granulation step is 0.01 to 300 Torr, and the preferred temperature of the granulation treatment is 90 to 140° C. The preferred pressure of the dehydration treatment in the dehydration step is 0.01 to 10 Torr, and the preferred temperature of the dehydration treatment is 200 to 400° C.
摘要翻译：用作双电层电容器的可极化电极材料的活性炭可以通过在保持固体状态下混合碳质材料和碱金属氢氧化物同时保持固体状态使所得到的混合物成粒，同时保持所得粒状物质，同时保持其固体状态，并将脱水步骤中获得的造粒脱水产物进行活化处理。制粒工序中的造粒处理的优选压力为0.01〜300乇，造粒处理温度优选为90〜140℃。脱水工序中脱水处理的优选压力为0.01〜10乇，脱水处理的优选温度为200〜400℃。

10. 发明授权

US07700698B2 Process for producing ring-opening metathesis polymer 有权
标题翻译：开环易位聚合物的制备方法
公开(公告)号：US07700698B2
公开(公告)日：2010-04-20
申请号：US11815803
申请日：2006-02-07
申请人： Hideharu Iwasaki , Yasutaka Inubushi
发明人： Hideharu Iwasaki , Yasutaka Inubushi
IPC分类号： C08F4/80 , C08G61/08 , C08F2/44
CPC分类号： C08G61/08 , C08K5/13 , C08K5/50 , C08K5/526
摘要： A process of producing a ring-opening metathesis polymer characterized in that a treatment to decrease the amount of oxygen and/or peroxide in at least one kind of polymerization starting material is performed prior to the ring-opening metathesis polymerization reaction of a cyclic olefin performed in the presence of a ruthenium carbene complex (catalyst). Treatments to decrease the amount of oxygen and/or peroxide include applying an adsorbent to a polymerization starting material to remove oxygen and/or peroxide by adsorption, applying an antioxidant to a polymerization starting material to decompose oxygen or peroxide, and the like.
摘要翻译：一种制备开环易位聚合物的方法，其特征在于在至少一种聚合原料中减少氧和/或过氧化物的量的处理在环烯烃的开环易位聚合反应之前进行在钌卡宾络合物（催化剂）的存在下。减少氧和/或过氧化物的量的处理包括将吸附剂施加到聚合起始材料上以通过吸附除去氧和/或过氧化物，将抗氧化剂施加到聚合起始材料上以分解氧气或过氧化物等。

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