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1. 发明专利

JP2014182037A Volatile cracked component collection and recovery device, liquid chromatograph and volatile cracked component analysis method 有权
标题翻译：挥发性破碎组件收集和恢复装置，液相色谱和挥发性破碎组分分析方法
公开(公告)号：JP2014182037A
公开(公告)日：2014-09-29
申请号：JP2013057391
申请日：2013-03-19
申请人： Toyota Central R&D Labs Inc , 株式会社豊田中央研究所 , Nagoya Institute Of Technology , 国立大学法人名古屋工業大学
发明人： ITO HIROSHI , IWAI KOICHIRO , OTANI HAJIME , KITAGAWA SHINYA , IIKUNI YOSHINORI , KUNO MINORU
IPC分类号： G01N1/22 , G01N30/06 , G01N30/88
摘要： PROBLEM TO BE SOLVED: To provide a volatile cracked component collection and recovery device capable of analyzing almost all volatile cracked components by liquid chromatograph, including volatile cracked components difficult to analyze by conventional gas chromatograph (GC).SOLUTION: The volatile cracked component collection and recovery device of the present invention includes: a sample holder for holding a sample in a flow path of carrier gas; heating means for heating the sample held by the sample holder; a guide and adhesion tube having an upper opening part attachable to/detachable from a downstream end of the sample holder, an extending part extending from the upper opening part, and a lower opening part existing at a downstream side of the extending part, for guiding the volatile cracked components from the upper opening part to the lower opening part, or making the volatile cracked components adhere to an inner wall; and a switching valve capable of switching positions between a first position where the upper opening part of the guide and adhesion tube is attached to the downstream end of the sample holder, and a second position where the upper opening part of the guide and adhesion tube is detached from the downstream end of the sample holder and solvent is supplied into the guide and adhesion tube.
摘要翻译：要解决的问题：提供一种能够通过液相色谱分析几乎所有挥发性裂纹组分的挥发性裂解组分收集和回收装置，包括常规气相色谱（GC）难以分析的挥发性裂解组分。解决方案：挥发性裂化组分收集和本发明的回收装置包括：用于将样品保持在载气流动路径中的样品保持器; 用于加热由样品架保持的样品的加热装置; 引导和粘附管，其具有可从样品保持器的下游端附接/拆卸的上部开口部，从上部开口部延伸的延伸部和存在于延伸部的下游侧的下部开口部，从上部开口部到下部开口部的挥发性裂纹成分，或使挥发性裂纹成分附着在内壁上; 以及切换阀，其能够在引导件的上部开口部和粘附管的第一位置与样品保持器的下游端连接的第一位置和引导和粘附管的上部开口部的第二位置从样品保持器的下游端分离并将溶剂供应到引导和粘附管中。

2. 发明专利

JP2015058416A 気泡固定流路装置及びそれを用いた測定装置审中-公开
标题翻译：泡沫固定流量传送装置和使用该装置的测量装置
公开(公告)号：JP2015058416A
公开(公告)日：2015-03-30
申请号：JP2013195613
申请日：2013-09-20
申请人：国立大学法人名古屋工業大学 , Nagoya Institute Of Technology , 国立大学法人名古屋工業大学
发明人： KITAGAWA SHINYA
IPC分类号： B01J19/00
摘要：【課題】水溶液中で発生させた気泡を用いる分離法の高性能化のため、気泡表面または気泡表面に存在する界面活性剤と、物質との相互作用を評価する手法を提供する。【解決手段】気泡を流路内に固定した状態で流路内に試料を流すことで気泡表面、または、気泡表面に存在する界面活性剤と物質の相互作用を、比較的少量(数十mL以下)の試料溶液で評価可能とした。【選択図】図2
摘要翻译：要解决的问题：提供评估气泡表面之间或存在于气泡表面中的表面活性剂之间的相互作用的方法以及使用在水溶液中产生的气泡的分离方法的性能提高的物质。解决方案：通过流动在气流被固定在流路中的状态下的样品流入通道中，气泡表面之间或气泡表面中存在的表面活性剂之间的相互作用可以以相对少量（几十毫升或更低）的样品来评估解。

3. 发明专利

JP2012093092A Planer column, and separation system and separation method using the same 审中-公开
标题翻译：平面图和分离系统以及使用该分离系统的分离方法
公开(公告)号：JP2012093092A
公开(公告)日：2012-05-17
申请号：JP2009253775
申请日：2009-11-05
申请人： Nagoya Institute Of Technology , 国立大学法人名古屋工業大学
发明人： KITAGAWA SHINYA
IPC分类号： G01N30/02 , G01N27/447 , G01N30/16 , G01N30/26 , G01N30/60 , G01N30/88
摘要： PROBLEM TO BE SOLVED: To perform chromatographic separation and electrophoretic separation.SOLUTION: A flow channel in which samples flow is formed between a pair of glass substrates. In the flow channel, a planer column with a structure having an organic monolith in the sample flow direction and having a pair of electrodes to apply voltage in the direction perpendicular to the sample flow is used to perform chromatographic separation in the flow direction and, by simultaneously applying voltage in the direction perpendicular to the flow, to perform electrophoretic separation. Consequently, sample components are two-dimensionally separated in the planer column.
摘要翻译：要解决的问题：进行色谱分离和电泳分离。
解决方案：在一对玻璃基板之间形成样品流动的流动通道。在流动通道中，使用具有在样品流动方向上具有有机整料的结构的平面柱，并且具有一对在垂直于样品流动的方向上施加电压的电极，以在流动方向上执行色谱分离，并且通过同时沿垂直于流动方向施加电压，进行电泳分离。因此，样品组分在平面柱中二维分离。版权所有（C）2012，JPO＆INPIT

4. 发明专利

JP2011117950A Column for liquid chromatography, and preparation method for the same 审中-公开
标题翻译：液相色谱柱及其制备方法
公开(公告)号：JP2011117950A
公开(公告)日：2011-06-16
申请号：JP2010240429
申请日：2010-10-27
申请人： Nagoya Institute Of Technology , 国立大学法人名古屋工業大学
发明人： KITAGAWA SHINYA , HIRANO TOMOHIKO
IPC分类号： G01N30/88 , G01N30/50
摘要： PROBLEM TO BE SOLVED: To provide a column for liquid chromatography and its preparation method which can attain low channel resistance and full separation performance.
SOLUTION: In the method, an organic monolith column is prepared by photopolymerization for a period of 100-240 seconds, at light intensity of 100-250 mW/cm
2 under a low temperature range of -30 to 0°C. After the photopolymerization, the column is cleaned with methanol, so that "fragile" portion of column center is destroyed, and a huge through-hole is formed inside the column. As a result, as shown in (b) and (c) of Fig., a winding huge through-hole is formed at the center, allowing preparation of the column for liquid chromatography with a monolithic structure formed around the huge through-hole.
COPYRIGHT: (C)2011,JPO&INPIT
摘要翻译：要解决的问题：提供可以获得低通道阻力和完全分离性能的液相色谱柱及其制备方法。解决方案：在该方法中，通过光聚合制备有机整料柱，时间为100-240秒，光强度为100-250mW / cm 2，在低温范围内 -30至0℃。光聚合后，柱子用甲醇清洗，柱中心的“易碎”部分被破坏，柱内形成一个巨大的通孔。结果，如图所示（b）和（c）所示，在中心形成有一个绕组的巨大的通孔，从而可以在形成在巨大通孔周围的整体结构的液相色谱柱上制备。版权所有（C）2011，JPO＆INPIT

5. 发明专利

JP2011099741A Method for preparing organic monolithic column 审中-公开
标题翻译：制备有机单晶柱的方法
公开(公告)号：JP2011099741A
公开(公告)日：2011-05-19
申请号：JP2009254013
申请日：2009-11-05
申请人： Nagoya Institute Of Technology , 国立大学法人名古屋工業大学
发明人： KITAGAWA SHINYA , HIRANO TOMOHIKO
IPC分类号： G01N30/88
摘要： PROBLEM TO BE SOLVED: To prepare an organic monolithic column low in flow channel resistance and capable of obtaining sufficient separation capacity.
SOLUTION: The organic monolithic column is prepared using photopolymerization performed at a low temperature of -30 to 0°C over 100-200 sec under a condition of an optical intensity of 100-250 mW/cm
2 . By this method, flow channel resistance (gradient) can be suppressed to about 1/3 as shown by white squares as compared with a previous report (the black squares in the drawing).
COPYRIGHT: (C)2011,JPO&INPIT
摘要翻译：要解决的问题：制备流动阻力低的有机整体柱，并且能够获得足够的分离能力。解决方案：在光强度为100-250mW / cm 2的条件下，在100〜200秒的低温-30〜0℃下进行光聚合制备有机整体柱。 SP>。通过该方法，与前一报告（图中的黑色方块）相比，流路阻力（梯度）可以被抑制到大约1/3，如白平方所示。版权所有（C）2011，JPO＆INPIT

6. 发明专利

JP2006159148A Column for chromatography and column for electrochromatography 审中-公开
标题翻译：色谱柱和电子色谱柱
公开(公告)号：JP2006159148A
公开(公告)日：2006-06-22
申请号：JP2004357997
申请日：2004-12-10
申请人： Nagoya Institute Of Technology , 国立大学法人名古屋工業大学
发明人： KITAGAWA SHINYA , ODA TOYOJI
IPC分类号： B01J20/281 , G01N30/02 , G01N30/32 , G01N30/54 , G01N30/56 , G01N30/60 , G01N30/88
摘要： PROBLEM TO BE SOLVED: To provide a chromatography separation column capable of obtaining an effect similar to that by gradient elution for changing a moving phase composition, and to provide a chromatography separation column capable obtaining an effect similar to that by separation using a plurality of the conventional columns.
SOLUTION: The column, in which the capacity of the interaction between a sample and a fixed bed and the moving speed of the sample are different in portions in its flowing direction, is used, thereby obtaining the effect similar to that by gradient elution.
COPYRIGHT: (C)2006,JPO&NCIPI
摘要翻译：待解决的问题：提供能够获得与用于改变移动相组成的梯度洗脱类似的效果的色谱分离柱，并提供能够获得与通过使用多个传统的列。解决方案：使用其中样品和固定床之间的相互作用能力和样品的移动速度在其流动方向上部分不同的柱，从而获得与梯度相似的效果洗脱。版权所有（C）2006，JPO＆NCIPI

7. 发明专利

JP2010101795A Liquid chromatography and electrochromatography 审中-公开
标题翻译：液相色谱和电化学
公开(公告)号：JP2010101795A
公开(公告)日：2010-05-06
申请号：JP2008274371
申请日：2008-10-24
申请人： Nagoya Institute Of Technology , 国立大学法人名古屋工業大学
发明人： KITAGAWA SHINYA
IPC分类号： G01N30/88 , G01N30/02 , G01N30/34 , G01N30/54 , G01N30/56 , G01N30/60
摘要： PROBLEM TO BE SOLVED: To provide a procedure capable of improving separation performance and detection sensitivity by suppressing increase of a peak width in a separation column following separation in liquid chromatography and electrochromatography.
SOLUTION: In this chromatography, increase of the peak width can be suppressed by combining a chromatography gradient (uneven field) column with a gradient elution procedure of a moving phase composition.
COPYRIGHT: (C)2010,JPO&INPIT

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