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1. 发明专利

JP2013170304A β-TITANIUM ALLOY AND METHOD FOR MANUFACTURING THE SAME 审中-公开
标题翻译：钛合金及其制造方法
公开(公告)号：JP2013170304A
公开(公告)日：2013-09-02
申请号：JP2012036024
申请日：2012-02-22
申请人： Toyota Central R&D Labs Inc , 株式会社豊田中央研究所
发明人： TOWATA SHINICHI , FURUTA TADAHIKO , KURAMOTO SHIGERU
IPC分类号： C22C14/00 , C22F1/00 , C22F1/18 , C23C8/08
摘要： PROBLEM TO BE SOLVED: To provide a titanium alloy in which a modulus of elasticity can be controlled.SOLUTION: A β-titanium alloy is composed of crystals of body-centered cubic lattice structure (bcc) and contains 500-5,000 ppm of hydrogen (H) in the mass ratio to the whole. Such β-titanium alloy is obtained by the manufacturing method including a hydrogen introducing process, in which for example, a β-titanium alloy material having a β phase as a main phase is exposed into a hydrogen atmosphere at 100-500°C atmospheric temperature and 0.01-100 MPa hydrogen partial pressure to introduce hydrogen to the β-titanium alloy material. Thus, the β-titanium alloy, which is controlled to be a modulus of elasticity suitable to various kinds of products by regulating the contained hydrogen content in the suitable range, can be obtained. Especially, without adjusting the compositions, etc., of the alloy elements, the modulus of elasticity in the β-titanium alloy can be easily made very low.
摘要翻译：要解决的问题：提供可以控制弹性模量的钛合金。解决方案：钛合金由体心立方晶格结构（bcc）晶体组成，含有500-5,000ppm的氢（H）以质量比计。这种合金是通过包括氢引入工艺的制造方法获得的，其中例如具有＆bgr的钛合金材料; 相作为主相，暴露于氢气气氛中，在100-500℃的大气温度和0.01-100MPa的氢分压下将氢引入到合金材料中。因此，可以获得通过将含有氢含量调节在适当范围内而适用于各种产品的弹性模量的合金。特别是，在不调整合金元素的成分等的情况下，可以容易地使合金元素的弹性模量变得非常低。

2. 发明专利

JP2011173967A Manufacturing method of energy gas, and energy gas storage material 有权
标题翻译：能源气体的制造方法和能源储气体材料
公开(公告)号：JP2011173967A
公开(公告)日：2011-09-08
申请号：JP2010037931
申请日：2010-02-23
申请人： Tohoku Univ , Toyota Central R&D Labs Inc , 国立大学法人東北大学 , 株式会社豊田中央研究所
发明人： KAWAI YASUAKI , MATSUMOTO MITSURU , TOWATA SHINICHI , FUKUSHIMA YOSHIAKI , CHO KIBU , SAITO FUMIYOSHI
IPC分类号： C10J3/00 , C01B3/02 , C01B32/40
CPC分类号： Y02P20/52
摘要： PROBLEM TO BE SOLVED: To provide a manufacturing method of an energy gas that requires a relatively small charged amount of energy for a mixing treatment of raw materials, gives an energy gas by heating at a relatively low temperature and permits employment of an additive abundant in resources, and an energy gas storage material.
SOLUTION: The manufacturing method of an energy gas has the following constitutions. (1) The manufacturing method of an energy gas comprises a mixing step of adding a formic acid-iron additive or an aqueous solution thereof to a compound containing carbon, hydrogen and/or oxygen and subsequently mixing these and a heating step of heating the mixture obtained in the mixing step in an inert atmosphere. (2) The formic acid-iron additive is at least one selected from among a mixture of formic acid with an iron-based additive, a reaction product of formic acid with the iron-based additive and iron formate. The energy gas storage material is obtained by the mixing step above.
COPYRIGHT: (C)2011,JPO&INPIT
摘要翻译：要解决的问题：为了提供一种需要相对较少的用于混合处理原料的能量的能量气体的制造方法，通过在较低的温度下加热而产生能量气体，并允许使用资源丰富的添加剂和能源气体储存材料。解决方案：能量气体的制造方法具有以下构成。（1）能量气体的制造方法包括将甲酸 - 铁添加剂或其水溶液添加到含有碳，氢和/或氧的化合物中并随后将其混合的加热步骤和加热混合物的加热步骤在惰性气氛中在混合步骤中得到。（2）甲酸 - 铁添加剂是选自甲酸与铁基添加剂的混合物中的至少一种，甲酸与铁基添加剂的反应产物和甲酸铁。通过上述混合步骤获得能量气体储存材料。版权所有（C）2011，JPO＆INPIT

3. 发明专利

JP2011046583A Mixed body and method for producing the same, method for producing gaseous hydrogen, and hydrogen generator 有权
标题翻译：混合体及其制造方法，生产氢气的方法和氢发生器
公开(公告)号：JP2011046583A
公开(公告)日：2011-03-10
申请号：JP2009198827
申请日：2009-08-28
申请人： Toyota Central R&D Labs Inc , 株式会社豊田中央研究所
发明人： AOKI MASAKAZU , MATSUMOTO MITSURU , TOWATA SHINICHI , NORITAKE TATSUO , KITAJIMA SATSUKI , SATO MASAHIRO
IPC分类号： C01B3/06 , H01M8/06
CPC分类号： Y02E60/362
摘要： PROBLEM TO BE SOLVED: To provide a mixed body which enables LiBH
4 and NH
3 to be reacted with each other at low temperature and also under low pressure and also can release a relatively large quantity of hydrogen, to provide a method for producing the mixed body, to provide a method for producing gaseous hydrogen, and to provide a hydrogen generator.
SOLUTION: The mixed body is obtained by mixing a blend comprising LiBH
4 and NiCl
2 , and is used for being reacted with ammonia, and the method for producing the mixed body is also provided. The method for producing a gaseous hydrogen includes a step where the mixed body is reacted with ammonia. The hydrogen generator includes a mixed body vessel for storing the mixed body; an ammonia vessel for storing ammonia; an ammonia feeder for feeding the ammonia from the ammonia vessel to the mixed body vessel, and a hydrogen exhaust apparatus which, in the mixed body vessel, exhausts the hydrogen produced by the reaction between the mixed body and the ammonia from the mixed body vessel.
COPYRIGHT: (C)2011,JPO&INPIT
摘要翻译：要解决的问题：为了提供使LiBH 4 和NH 3 在低温和低压下彼此反应的混合体，并且还可以释放相当大量的氢气，以提供制造混合体的方法，提供一种生产气态氢的方法，并提供氢气发生器。解决方案：通过混合包含LiBH 4 和NiCl SB SB2的共混物获得混合体，并用于与氨反应，还提供混合体。制造气态氢的方法包括使混合体与氨反应的工序。氢气发生器包括用于储存混合体的混合体容器; 用于储存氨的氨容器; 用于将氨从氨容器供给到混合体容器的氨供料器，以及在混合体容器中从混合体容器排出由混合体和氨之间的反应产生的氢的氢气排出装置。版权所有（C）2011，JPO＆INPIT

4. 发明专利

JP2009143790A Hydride complex and hydrogen storage material 审中-公开
标题翻译：氢化复合物和氢储存材料
公开(公告)号：JP2009143790A
公开(公告)日：2009-07-02
申请号：JP2008202274
申请日：2008-08-05
申请人： Toyota Central R&D Labs Inc , 株式会社豊田中央研究所
发明人： AOKI MASAKAZU , MATSUMOTO MITSURU , TOWATA SHINICHI , NORITAKE TATSUO
IPC分类号： C01B3/00 , B01J20/04 , C01B6/00
CPC分类号： Y02E60/327 , Y02P20/129
摘要： PROBLEM TO BE SOLVED: To provide a hydride complex which has low rare element content, is lightweight and from/in which a large quantity of hydrogen can be released/absorbed at relatively low temperature and to provide a hydrogen storage material. SOLUTION: The hydride complex comprises Mg(BH 4 ) 2 and Mg(NH 2 ) 2 . The hydrogen storage material is obtained by releasing the whole or a part of the hydrogen contained in the hydride complex. The hydride complex shown by (Mg(BH 4 ) 2 +xMg(NH 2 ) 2 (1/3≤x≤3.0)) is preferably used. COPYRIGHT: (C)2009,JPO&INPIT
摘要翻译：要解决的问题：为了提供稀有元素含量低的氢化物络合物，其重量轻且能够在较低温度下释放/吸收大量氢并提供储氢材料。解决方案：氢化物配合物包含Mg（BH 4 ） 2 和Mg（NH SB 2）。通过释放氢化物络合物中所含的全部或一部分氢来获得储氢材料。由（Mg（BH 4 ） + xMg（NH SB 2）/ SB> 2（/ 3≤x≤3.0））。版权所有（C）2009，JPO＆INPIT

5. 发明专利

JP2009067668A Method of manufacturing metal amide, amide compound complex and its manufacturing method, and hydrogen storage material and its manufacturing method 审中-公开
标题翻译：制备金属酰胺，复合复合材料及其制造方法，氢储存材料及其制造方法
公开(公告)号：JP2009067668A
公开(公告)日：2009-04-02
申请号：JP2008081186
申请日：2008-03-26
申请人： Toyota Central R&D Labs Inc , 株式会社豊田中央研究所
发明人： AOKI MASAKAZU , MATSUMOTO MITSURU , NORITAKE TATSUO , TOWATA SHINICHI , KITAJIMA SATSUKI , SATO MASAHIRO
IPC分类号： C01B21/092 , C01B3/00 , C01B6/04 , H01M8/06
CPC分类号： Y02E60/327 , Y02E60/328 , Y02P20/129
摘要： PROBLEM TO BE SOLVED: To provide a method of manufacturing a metal amide compound which is thermally unstable, and easy to take out hydrogen, an amide compound complex using the metal amide compound prepared by the method and a hydrogen storage material, and methods of manufacturing the compounds. SOLUTION: The method of manufacturing the metal amide comprises reacting an organic metal compound expressed by the general formula: (R) x M and ammonia. In the formula, R is any of one or more organic groups chosen from a group consisting of a 1-10C normal chain alkyl group, branched alkyl group, and an aromatic group. M is a metallic element. X is the valence of M. The amide compound complex is obtained by reacting the organic metal compound: (R) x M and ammonia and mixing an obtained solid and the second component and its manufacture method is disclosed. The hydrogen storage material is obtained by reacting the organic compound: (R) x M containing two or more metallic elements and ammonia and heat-treating under reduced pressure or inert gas atmosphere, and its manufacturing method is disclosed. COPYRIGHT: (C)2009,JPO&INPIT
摘要翻译：待解决的问题：提供一种使用通过该方法制备的金属酰胺化合物和储氢材料制造热不稳定并易于除去氢的金属酰胺化合物的方法和酰胺化合物络合物，以及制造化合物的方法。解决方案：制备金属酰胺的方法包括使由通式（R）-Si x SB / M表示的有机金属化合物与氨反应。在该式中，R是选自1-10C正链烷基，支链烷基和芳族基团中的一种或多种有机基团中的任何一种。 M是金属元素。酰胺化合物络合物是通过使有机金属化合物：（R）＆lt; SB＆gt; M＆amp; M＆amp; M与氨反应，并将得到的固体和第2成分并公开了其制造方法。储氢材料通过使含有两种或更多种金属元素的氨基的有机化合物（R） xS / M与氨反应并在减压或惰性气体气氛下进行热处理而得到，其制造方法公开。版权所有（C）2009，JPO＆INPIT

6. 发明专利

JP2009018292A Hydrogen storage material and method for manufacturing the same 审中-公开
标题翻译：氢储存材料及其制造方法
公开(公告)号：JP2009018292A
公开(公告)日：2009-01-29
申请号：JP2007185063
申请日：2007-07-13
申请人： Toyota Central R&D Labs Inc , 株式会社豊田中央研究所
发明人： AOKI MASAKAZU , TOWATA SHINICHI
IPC分类号： B01J20/04 , C01B3/00 , C01B6/04 , C01B21/092 , C22C1/00 , C22C14/00 , C22C19/00 , C22C22/00 , C22C27/06
CPC分类号： Y02E60/327 , Y02P20/128 , Y02P20/129
摘要： PROBLEM TO BE SOLVED: To provide a hydrogen storage material where storage/discharge speeds of hydrogen are high, speed drop along with cycle repetition, and storage/discharge amounts of hydrogen in the entire material are large and a method for manufacturing the same. SOLUTION: Provided are a hydrogen storage material that comprises a mixture of metallic amide A(NH 2 ) n and metal hydride BH m and a hydrogen-storage alloy, wherein for the hydrogen-storage, the ratio (P 2A /P 1A ) of the plateau pressure (P 2A ) of the hydrogen-storage alloy at the same temperature as the hydrogen-storage temperature to the plateau pressure (P 1A ) at the hydrogen-storage temperature of the mixture is 0.01 or more and 100 or less, and the ratio (P 2D /P 1D ) of the plateau pressure (P 2D ) of the hydrogen-storage alloy at the same temperature as the hydrogen-discharge temperature to the plateau pressure (P 1D ) at the hydrogen-discharge temperature of the mixture is 0.01 or more and 100 or less and where n, m are each valence of metals A, B; and a method for manufacturing the hydrogen storage material 1. COPYRIGHT: (C)2009,JPO&INPIT
摘要翻译：要解决的问题：为了提供氢气的储存/排出速度高，循环重复的速度下降和整个材料中的氢的储存/排放量大的储氢材料，以及制造方法相同。解决方案：提供一种储氢材料，其包含金属酰胺A（NH 2 SBB）与SB金属氢化物BH 的混合物，和储氢合金，其中对于储氢，平台压力的比（P 2A / P 1A ）（P 2A 1A ）的储氢温度相同的温度下，储氢合金的含量为0.01以上且100以下，以及相同温度下储氢合金的平台压力（P 2D ）的比（P 2D / P 1D ）由于混合物的氢排出温度下的平均压力（P 1D ）的排氢温度为0.01以上且100以下，其中，n，m分别为金属A， B; 和储氢材料1的制造方法。（C）2009，JPO＆INPIT

7. 发明专利

JP2011011936A Hydride composite and hydrogen storage material 审中-公开
标题翻译：氢化复合材料和氢储存材料
公开(公告)号：JP2011011936A
公开(公告)日：2011-01-20
申请号：JP2009156394
申请日：2009-06-30
申请人： Toyota Central R&D Labs Inc , 株式会社豊田中央研究所
发明人： MATSUMOTO MITSURU , AOKI MASAKAZU , NORITAKE TATSUO , TOWATA SHINICHI
IPC分类号： C01B6/24 , B01J20/02 , C01B3/00 , H01M8/06
CPC分类号： Y02E60/327 , Y02P20/129
摘要： PROBLEM TO BE SOLVED: To provide a novel hydride composite from which hydrogen can be taken out, even at ≤200°C, and a hydrogen storage material that can be obtained by releasing the hydrogen from the hydride composite.SOLUTION: The hydride composite is obtained by mixing and pulverizing a mixture of a metal borohydride M(BH)(wherein M is a first metal element; and n is the oxidation number of M) and a metal aluminum hydride compound M'(AlH)(wherein M' is a second metal element; and n' is the oxidation number of M'). The hydrogen storage material is obtained by releasing all or a portion of the hydrogen contained in the hydride composite.
摘要翻译：要解决的问题：提供即使在≤200℃也可以从其中取出氢的新型氢化物复合物，以及可以通过从氢化物复合物中释放氢而获得的储氢材料。溶液：氢化物复合物通过混合并粉碎金属硼氢化物M（BH）（其中M是第一金属元素; n是M的氧化数）和金属氢化铝化合物M'（AlH）（其中M'是第二金属元素; n'是M'的氧化数）。通过释放氢化物复合材料中所含的全部或一部分氢来获得储氢材料。

8. 发明专利

JP2010265136A Hydride composite, imide material and method for producing hydrogen gas 审中-公开
标题翻译：氢化物复合材料，生产氢气的材料和方法
公开(公告)号：JP2010265136A
公开(公告)日：2010-11-25
申请号：JP2009117054
申请日：2009-05-13
申请人： Toyota Central R&D Labs Inc , 株式会社豊田中央研究所
发明人： AOKI MASAKAZU , MATSUMOTO MITSURU , TOWATA SHINICHI , NORITAKE TATSUO , KITAJIMA SATSUKI , SATO MASAHIRO
IPC分类号： C01B6/24 , C01B3/04 , C01B21/092
CPC分类号： Y02E60/364 , Y02P20/129
摘要： PROBLEM TO BE SOLVED: To provide a hydride composite from which hydrogen can be taken out even at ≤100°C, an imide compound that can be obtained by releasing hydrogen from the hydride composite material, and a method for producing hydrogen gas using the hydride composite. SOLUTION: The hydride composite comprises LiAlH x (NH 2 ) 4-x (wherein x=0 or 1) and LiAlH 4 . The imide material is obtained by releasing all or a portion of hydrogen contained in the hydride composite. The method for producing the hydrogen gas comprises a hydrogen releasing step of releasing hydrogen from the hydride composite. COPYRIGHT: (C)2011,JPO&INPIT
摘要翻译：要解决的问题：为了提供即使在≤100℃也可以取出氢的氢化物复合物，可以通过从氢化物复合材料中释放氢而获得的酰亚胺化合物，以及氢气的制造方法使用氢化物复合材料。解决方案：氢化物复合材料包含LiAlH x SB SB（4）x-x SB（x = 0或1）和LiAlH < SB> 4 。酰亚胺材料是通过释放氢化物复合材料中所含的全部或部分氢而获得的。制造氢气的方法包括从氢化物复合物中释放氢的氢释放步骤。版权所有（C）2011，JPO＆INPIT

9. 发明专利

JP2010236084A Hydrogen storage alloy, method of preparing the same and hydrogen storage device 有权
标题翻译：氢存储合金，其制备方法和氢储存装置
公开(公告)号：JP2010236084A
公开(公告)日：2010-10-21
申请号：JP2009258344
申请日：2009-11-11
申请人： Toyota Central R&D Labs Inc , Toyota Motor Corp , トヨタ自動車株式会社 , 株式会社豊田中央研究所
发明人： AOKI MASAKAZU , TOWATA SHINICHI , NORITAKE TATSUO , ITO AKIO , WASHIO KOTA , ISHIKIRIYAMA MAMORU
IPC分类号： C22C27/02 , C01B3/00 , C22F1/00 , C22F1/18 , F17C11/00
CPC分类号： C22C27/02 , C01B3/0031 , C22C30/00 , C22F1/18 , Y02E60/327
摘要： PROBLEM TO BE SOLVED: To provide a hydrogen storage alloy having a high initial effective hydrogen amount and excellent cycle durability, and to provide a method of preparing the same, and a hydrogen storage device using such a hydrogen storage alloy. SOLUTION: There are disclosed the hydrogen storage alloy having, as a main phase thereof, a bcc structure phase having a composition represented by Ti x Cr y V z X w , and a hydrogen generator using the alloy. The method of preparing the hydrogen storage alloy includes: a melting/casting process of melting/casting raw materials mixed to be the composition represented by Ti x Cr y V z X w ; a heat treatment process of heat-treating an ingot obtained in the melting/casting process; and an activation process of executing the treatment of storing/releasing hydrogen to the heat-treated ingot at least once, wherein 3/2≤y/x≤3/1, 50≤z≤75 mol%, 0≤x≤5 mol%, (x+y+z+w) is 100 mol%, and X is at least one selected from Al, Si and Fe. COPYRIGHT: (C)2011,JPO&INPIT
摘要翻译：要解决的问题：提供具有高初始有效氢量和优异的循环耐久性的储氢合金，并提供其制备方法和使用这种储氢合金的储氢装置。解决方案：公开了一种储氢合金，其具有作为其主相的具有由Ti X X V SB表示的组成的bcc结构相＆gt; z＆lt; SB＆gt; w＆lt; / SB＆gt;和使用该合金的氢发生器。制备储氢合金的方法包括：熔融/浇铸原料的熔融/铸造方法，所述原料混合成由Ti X V ž X 瓦特; 在熔融/铸造过程中获得的锭的热处理过程; 以及将经过热处理的锭储存/释放氢的处理进行至少一次的活化处理，其中3 /2≤y/x≤3/1,50≤z≤75摩尔％，0≤x≤5摩尔％，（x + y + z + w）为100摩尔％，X为选自Al，Si，Fe中的至少1种。版权所有（C）2011，JPO＆INPIT

10. 发明专利

JP2013159852A Hydrogen storage alloy 有权
标题翻译：氢储存合金
公开(公告)号：JP2013159852A
公开(公告)日：2013-08-19
申请号：JP2012025584
申请日：2012-02-08
申请人： Toyota Central R&D Labs Inc , 株式会社豊田中央研究所
发明人： TOWATA SHINICHI , AOKI MASAKAZU , NORITAKE TATSUO , MIWA KAZUTOSHI
IPC分类号： C22C27/02 , B22F1/00 , B22F9/04 , C22C27/06 , C22C30/00
摘要： PROBLEM TO BE SOLVED: To provide a hydrogen storage alloy which can store and release hydrogen near a normal temperature, which has a high rechargeable hydrogen storage capacity, which requires a low cost, and which is excellent in cycle durability.SOLUTION: A hydrogen storage alloy includes a bcc structure phase represented by TiCrVNbFe(1.5≤y/x
摘要翻译：要解决的问题：提供一种能够在常温下储存和释放氢的储氢合金，其具有高的可再充电氢储存能力，这需要低成本，并且循环耐久性优异。解决方案：氢存储合金包括由TiCrVNbFe（1.5≤y/ x <3，15≤z<65,1≤v≤10,0≤w<5和x + y + z + v + w = 100）表示的bcc结构相作为主要阶段 y / x优选在1.6和2.8之间; v优选为1.5〜8.5。

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