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1. 发明授权

US5183892A Anthrapyridone compounds 失效
标题翻译：蒽吡啶酮化合物
公开(公告)号：US5183892A
公开(公告)日：1993-02-02
申请号：US621236
申请日：1990-11-30
申请人： Toshio Nakamatsu , Masanobu Terao , Shigetoshi Muneishi , Norio Kometani , Yoshiaki Hayashi
发明人： Toshio Nakamatsu , Masanobu Terao , Shigetoshi Muneishi , Norio Kometani , Yoshiaki Hayashi
IPC分类号： C08K5/00 , C08K5/3437 , C09B5/14
CPC分类号： C08K5/3437 , C08K5/0041 , C09B5/14
摘要： An anthrapyridone compound of the following formula (I), which is useful for coloring synthetic resins: ##STR1## wherein Q is --NH.sub.2, --NHCH.sub.3 or --NHCOZ where Z is phenyl or alkyl which may be substituted; X.sub.1, X.sub.2 and X.sub.3 are each hydrogen, halogen, alkyl, alkoxy, hydroxy, --NHCOR.sup.1, --CONR.sup.2 R.sup.3 m --COR.sup.4, --COOR.sup.5, --SO.sub.2 R.sup.6 or --SO.sub.2 NR.sup.7 R.sup.8 where R.sup.1 and R.sup.4 are each C.sub.1-4 alkyl, R.sup.2 and R.sup.3 are each hydrogen or C.sub.1-4 alkyl, R.sup.5 and R.sup.6 are each alkyl or hydroxyalkyl and R.sup.7 and R.sup.8 are each hydrogen or C.sub.1-4 alkyl, with proviso that when Q is --NHCH.sub.3, X.sub.1, X.sub.2 and X.sub.3 are each hydrogen, halogen, alkoxy, hydroxy, --NHCOR.sup.1, --CONR.sup.2 R.sup.3, --COR.sup.4, --COOR.sup.5, --SO.sub.2 R.sup.6 or --SO.sub.2 NR.sup.7 R.sup.8.Process for producing the anthrapyridone compound is also provided.
摘要翻译：用于着色合成树脂的下式（I）的蒽并吡啶酮化合物：其中Q是-NH 2，-NHCH 3或-NHCOZ，其中Z是苯基或可被取代的烷基; X1，X2和X3各自为氢，卤素，烷基，烷氧基，羟基，-NHCOR1，-CONR2R3m -COR4，-COOR5，-SO2R6或-SO2NR7R8，其中R1和R4各自为C1-4烷基，R2和R3各自为氢或C 1-4烷基，R 5和R 6各自为烷基或羟烷基，且R 7和R 8各自为氢或C 1-4烷基，条件是当Q为-NHCH 3时，X 1，X 2和X 3各自为氢，卤素，烷氧基，羟基，-NHCOR1，-CONR2R3，-COR4，-COOR5，-SO2R6或-SO2NR7R8。还提供了制备蒽吡啶酮化合物的方法。

2. 发明授权

US5304677A Method for producing 2,6-dihydroxybenzoic acid 失效
标题翻译： 2,6-二羟基苯甲酸的制备方法
公开(公告)号：US5304677A
公开(公告)日：1994-04-19
申请号：US7782
申请日：1993-01-22
申请人： Toshio Nakamatsu , Yasuhiro Nishida , Norio Kometani
发明人： Toshio Nakamatsu , Yasuhiro Nishida , Norio Kometani
IPC分类号： C07C51/43 , C07C51/487 , C07C65/03 , C07C65/01
CPC分类号： C07C51/487
摘要： A method for producing 2,6-dihydroxybenzoic acid, which comprises heating an aqueous solution which contains a mixture of 2,6-dihydroxybenzoic acid and 2,4-dihydroxybenzoic acid and has a pH value of 4 or more, to selectively decompose 2,4-dihydroxybenzoic acid, and separating 2,6-dihydroxybenzoic acid from the decomposition reaction mixture.
摘要翻译：制备2,6-二羟基苯甲酸的方法，其包括加热含有2,6-二羟基苯甲酸和2,4-二羟基苯甲酸的混合物并且pH值为4以上的水溶液以选择性分解2，并从分解反应混合物中分离出2,6-二羟基苯甲酸。

3. 发明授权

US5276198A Process for producing 2-methyl-1,3-cyclohexanedione and 2-methylresorcinol 失效
标题翻译： 2-甲基-1,3-环己二酮和2-甲基间苯二酚的制备方法
公开(公告)号：US5276198A
公开(公告)日：1994-01-04
申请号：US933175
申请日：1992-08-21
申请人： Toshio Nakamatsu , Yasuhiro Nishida , Norio Kometani
发明人： Toshio Nakamatsu , Yasuhiro Nishida , Norio Kometani
IPC分类号： B01J23/42 , B01J23/44 , B01J25/02 , C07B61/00 , C07C37/06 , C07C37/07 , C07C39/08 , C07C45/65 , C07C45/67 , C07C49/403 , C07C211/00 , C07C225/12
CPC分类号： C07C211/00 , C07C37/07 , C07C45/673 , C07C2101/14
摘要： A process for producing 2-methyl-1,3-cyclohexanedione which comprises subjecting 1,3-cyclohexanedione, formaldehyde and a dialkylamine to Mannich reaction to obtain a 2-dialkylaminomethyl-1,3-cyclohexanedione, and subjecting the 2-dialkylaminomethyl to hydrogenolysis, and a process for producing 2-methylresorcinol which comprises aromatizing 2-methyl-1,3-cyclohexanedione obtained. According to these processes, it is possible to produce high-purity 2-methylresorcinol and 2-methyl-1,3-cyclohexanedione commercially easily and advantageously.
摘要翻译：一种2-甲基-1,3-环己二酮的制备方法，其包括使1,3-环己二酮，甲醛和二烷基胺进行曼尼希反应，得到2-二烷基氨基甲基-1,3-环己二酮，并使2-二烷基氨基甲基氢解，以及制备2-甲基间苯二酚的方法，其包括使得到的2-甲基-1,3-环己二酮芳构化。根据这些方法，可以容易且有利地生产高纯度2-甲基间苯二酚和2-甲基-1,3-环己二酮。

4. 发明授权

US5599971A Method for producing 1,4-dihydroxy-2-naphthoic acid 失效
标题翻译： 1,4-二羟基-2-萘甲酸的制造方法
公开(公告)号：US5599971A
公开(公告)日：1997-02-04
申请号：US383688
申请日：1995-02-01
申请人： Toshio Nakamatsu , Yasuhiro Nishida , Shinichi Watanabe , Norio Kometani
发明人： Toshio Nakamatsu , Yasuhiro Nishida , Shinichi Watanabe , Norio Kometani
IPC分类号： C07B61/00 , C07C51/15 , C07C65/11
CPC分类号： C07C51/15
摘要： A method for producing 1,4-dihydroxy-2-naphthoic acid which comprises the steps of: subjecting 1,4-dihydroxynaphthalene into an alkali metal salt formation reaction in an organic medium capable of dissolving 1,4-dihydroxynaphthalene using an alkali metal alcoholate; and subjecting the salt formation reaction mixture to carboxylation using carbon dioxide gas.
摘要翻译：一种1,4-二羟基-2-萘甲酸的制造方法，该方法包括以下步骤：使用碱金属醇化物在能够溶解1,4-二羟基萘的有机介质中使1,4-二羟基萘进行碱金属盐形成反应 ; 并使用二氧化碳气体使成盐反应混合物进行羧化。

5. 发明授权

US5136045A Pyrazole containing methine compounds 失效
标题翻译：含吡咯的甲基化合物
公开(公告)号：US5136045A
公开(公告)日：1992-08-04
申请号：US581114
申请日：1990-09-12
申请人： Toshio Nakamatsu , Masanobu Terao
发明人： Toshio Nakamatsu , Masanobu Terao
IPC分类号： C09B23/00 , C08K5/41 , C08K5/43 , C08K5/435 , C09B23/10
CPC分类号： C08K5/43 , C09B23/10 , C09B23/105
摘要： A methine compound represented by the following formula and an agent containing the same for coloring resins such as polystyrene, ABS. ##STR1## wherein R.sup.1 is a hydrogen atom, a lower alkyl group, a lower alkoxy group, a nitro group or a lower carboxylic ester group; R.sup.2 is a lower alkyl group, a lower carboxylic amide group or a lower carboxylic ester group; and X is --SO.sub.2 NR.sup.3 R.sup.4, --SO.sub.2 NCHNR.sup.5 R.sup.6 or --SO.sub.2 R.sup.7, where R.sup.3 and R.sup.4 each is a hydrogen atom, a lower alkyl group or a phenyl group, R.sup.5 and R.sup.6 each is a lower alkyl group, and R.sup.7 is a lower alkyl group or a hydroxyethyl group.

6. 发明授权

US4396549A Copper phthalocyanine blue reactive dye 失效
标题翻译：铜酞菁蓝活性染料
公开(公告)号：US4396549A
公开(公告)日：1983-08-02
申请号：US296480
申请日：1981-08-26
申请人： Toshio Nakamatsu , Naoki Harada , Yasuo Tezuka
发明人： Toshio Nakamatsu , Naoki Harada , Yasuo Tezuka
IPC分类号： C09B62/517 , C09B62/44 , D06P3/66
CPC分类号： C09B62/4418
摘要： A turquoise blue reactive dye represented by a free acid of the formula, ##STR1## wherein [CuPc] is a copper phthalocyanine nucleus, W is ##STR2## in which R.sub.1 and R.sub.2 are each a hydrogen atom or a methyl group and i is an integer of 2 to 6 both inclusive, Y.sub.1 and Y.sub.2 are each a hydrogen atom, a methyl, methoxy or sulfonic acid group, l and m are each a number of 0 to 3, and n is a number of 1 to 3, provided that l+m+n is not more than 4.This dye is suitable for dyeing cellulose fibers to produce a turquoise blue dyed product superior in fastnesses, acid stability, build-up property, level dyeing property, and low-temperature dyeability.
摘要翻译：由下式游离酸代表的绿松石蓝色活性染料其中[CuPc]是铜酞菁核，W是其中R 1和R 2各自是氢原子或甲基，且i是 2〜6的整数，Y 1和Y 2各自为氢原子，甲基，甲氧基或磺酸基，l和m各自为0〜3，n为1〜3的数，条件是 l + m + n不大于4.这种染料适用于染色纤维素纤维，以生产出坚固耐性，酸稳定性，增强性能，水平染色性能和低温可染性优越的绿松石蓝染色产品。

7. 发明授权

US5789590A Double cone-like crystal form of 2-amino-6-chloropurine and preparation 失效
标题翻译：双锥形晶体形式的2-氨基-6-氯嘌呤及其制备方法
公开(公告)号：US5789590A
公开(公告)日：1998-08-04
申请号：US741223
申请日：1996-10-29
申请人： Masatoshi Sakai , Masaki Fujiwara , Toshio Nakamatsu
发明人： Masatoshi Sakai , Masaki Fujiwara , Toshio Nakamatsu
IPC分类号： C07D473/40
CPC分类号： C07D473/40
摘要： The present invention is directed to a method for preparing 2-amino-6-chloropurine having a double cone-like crystal form, comprising the steps of: (A) suspending 2-amino-6-chloropurine having an acicular or irregular-shaped crystal form in a liquid consisting essentially of water having a pH of from 3 to 10; and (B) heating the resulting suspension at a temperature of from 70.degree. to 100.degree. C. to complete the double cone-like crystal form conversion.
摘要翻译：本发明涉及一种制备具有双锥状晶体形式的2-氨基-6-氯嘌呤的方法，包括以下步骤：（A）悬浮具有针状或不规则形状晶体的2-氨基-6-氯嘌呤在基本上由pH为3至10的水组成的液体中形成; 和（B）在70℃至100℃的温度下加热得到的悬浮液以完成双锥状晶体形式的转化。

8. 发明授权

US4667022A Reactive dye having both monochlorotriozinyl and vinylsulfone type reactive groups 失效
标题翻译：具有一氯三乙烯基和乙烯基砜型反应性基团的活性染料
公开(公告)号：US4667022A
公开(公告)日：1987-05-19
申请号：US234157
申请日：1981-02-13
申请人： Toshio Nakamatsu , Yoshikazu Matsuo , Yasuo Tezuka
发明人： Toshio Nakamatsu , Yoshikazu Matsuo , Yasuo Tezuka
IPC分类号： C09B62/51 , C09B62/44 , C09B62/085 , C09B62/53 , D06P1/382 , D06P1/384
CPC分类号： C09B62/4413
摘要： A red reactive dye represented by a free acid of the formula, ##STR1## wherein X is a hydrogen atom, a methyl, methoxy or sulfonic acid group, Y is --CH.dbd.CH.sub.2, --CH.sub.2 CH.sub.2 Y.sub.1 or --CH.sub.2 CH.sub.2 OY.sub.2 (in which Y.sub.1 is a halogen atom, and Y.sub.2 is the residue of polybasic acids), R is a C.sub.1 -C.sub.4 alkyl group, R.sub.1 and R.sub.2 are each a hydrogen atom, a methyl or ethyl group, and the azo group is located on a meta-or para-position of the benzene ring A with respect to the --NR.sub.2 -- group and the sulfonic acid group on the benzene ring A is adjacent to the azo group. This dye is suitable for dyeingcellulose fibers red to afford dyeings superior in fastnesses, acid stability, build-up property, level dyeing property and white dischargeability.
摘要翻译：由下式游离酸代表的红色活性染料，其中X是氢原子，甲基，甲氧基或磺酸基，Y是-CH = CH 2，-CH 2 CH 2 Y 1或-CH 2 CH 2 OY 2（其中 Y1是卤素原子，Y2是多元酸的残基），R是C1-C4烷基，R1和R2各自是氢原子，甲基或乙基，偶氮基位于元 - 或苯环A相对于-NR2-基的对位，苯环A上的磺酸基与偶氮基相邻。这种染料适用于红色染色纤维素纤维，以提供优异的耐晒牢度，酸稳定性，增强性能，水平染色性能和白色放电性能的染色。

9. 发明授权

US06861549B2 Production method of 4′-bromomethyl-2-cyanobiphenyl 有权
标题翻译： 4'-溴甲基-2-氰基联苯的制备方法
公开(公告)号：US06861549B2
公开(公告)日：2005-03-01
申请号：US10322017
申请日：2002-12-17
申请人： Seiji Yamada , Ken Ishihara , Toshio Nakamatsu
发明人： Seiji Yamada , Ken Ishihara , Toshio Nakamatsu
IPC分类号： C07C253/30 , C07C255/50
CPC分类号： C07C253/30 , C07C255/50
摘要： The present invention relates to a production method of 4′-bromomethyl-2-cyanobiphenyl, which includes reacting 4′-methyl-2-cyanobiphenyl with bromine in the presence of a radical initiator and an oxidant. According to the present invention, since bromine can be regenerated by reacting hydrogen bromide, which is by-produced with the progress of bromination, with an oxidant, inhibition of bromination by hydrogen bromide, coloring by bromine and the like can be prevented. Thus, 4′-bromomethyl-2-cyanobiphenyl useful as a starting material of pharmaceutical products can be produced industrially beneficially.
摘要翻译：本发明涉及4'-溴甲基-2-氰基联苯的制备方法，其包括在自由基引发剂和氧化剂存在下使4'-甲基-2-氰基联苯与溴反应。根据本发明，由于溴可以通过与副产物反应的溴化氢与氧化剂反应而再生，可以防止溴化氢溴化，溴溴化等的反应。因此，可以在工业上有利地生产用作药物原料的4'-溴甲基-2-氰基联苯。

10. 发明授权

US4902798A Anthrapyridone compounds 失效
标题翻译：蒽吡啶酮化合物
公开(公告)号：US4902798A
公开(公告)日：1990-02-20
申请号：US126596
申请日：1987-11-30
申请人： Toshio Nakamatsu , Yoshitugu Egashira , Yasuyuki Suzuki
发明人： Toshio Nakamatsu , Yoshitugu Egashira , Yasuyuki Suzuki
IPC分类号： C08K5/3437 , C09B5/14
CPC分类号： C08K5/3437 , C09B5/14
摘要： An anthrapyridone compound of the following formula (I) and which is useful for coloring resins: ##STR1## wherein X.sup.1 is hydrogen, --NHCOR.sup.1, --CONR.sup.2 R.sup.3, --COR.sup.4, --SO.sub.2 R.sup.5 or --SO.sub.2 NR.sup.6 R.sup.7, in which R.sup.1 and R.sup.4 are each C.sub.1-4 alkyl, R.sup.2 and R.sup.3 are each hydrogen or C.sub.1-4 alkyl, R.sup.5 is C.sub.1-4 alkyl or hydroxyethyl, R.sup.6 and R.sup.7 are each hydrogen or C.sub.1-4 alkyl, X.sup.2 is hydrogen or imidomethyl of the formula (II): ##STR2## wherein n is a number of 1 to 2, X.sup.4 is hydrogen or carboxylic acid C.sub.1-4 alkyl-ester, X.sup.3 is hydrogen, halogen, hydroxyl, C.sub.1-4 alkyl or C.sub.1-4 alkoxyl, with the proviso that X.sup.1 is --NHCOR.sup.1, --CONR.sup.2 R.sup.3, --COR.sup.4, --SO.sub.2 R.sup.5 or --SO.sub.2 NR.sup.6 R.sup.7 when X.sup.2 is hydrogen, X.sup.2 is the imidomethyl of the formula (II) when X.sup.1 is the hydrogen, is provided, which is prepared by allowing the .alpha.-halonathraquinone compound with an acylated primary aromatic amine compound in a nonaqueous medium in the presence of metallic copper or a copper compound.
摘要翻译：用于着色树脂的下式（I）的蒽并吡啶酮化合物：其中X 1是氢，-NHCOR 1，-CONR 2 R 3，-COR 4，-SO 2 R 5或-SO 2 NR 6 R 7，其中R 1和R 4是每个C 1-4烷基，R 2和R 3各自为氢或C 1-4烷基，R 5为C 1-4烷基或羟乙基，R 6和R 7各自为氢或C 1-4烷基，X 2为氢或式（II）的亚氨基甲基）：其中n为1至2的数，X 4为氢或羧酸C 1-4烷基酯，X 3为氢，卤素，羟基，C 1-4烷基或C 1-4烷氧基，其中条件是当X 2是氢时，X 1是-NHCOR 1，-CONR 2 R 3，-COR 4，-SO 2 R 5或-SO 2 NR 6 R 7，X 2是当X1是氢时式（II）的亚氨基甲基，其通过使α - 在金属铜或铜化合物的存在下，在非水介质中使用具有酰化伯芳香胺化合物的卤代萘醌化合物。

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