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1. 发明专利

JP2015054282A 溶質の回収方法および溶質の回収装置审中-公开
标题翻译：解决方案和解决方案的恢复方法
公开(公告)号：JP2015054282A
公开(公告)日：2015-03-23
申请号：JP2013188848
申请日：2013-09-11
申请人：株式会社東芝 , Toshiba Corp
发明人： MIYAMOTO MASAYA , IKEI SHUKO , KAWAUCHI KANAE , NAGAMORI YASUHIKO , YAMASHITA TAKEO , MIKURA MICHITAKA
IPC分类号： C02F1/62 , C02F1/58
摘要：【課題】重金属およびリンを含有する強酸性の溶液から、重金属類とリンを選択的に回収することが可能な、溶質の回収方法および溶質の回収装置を提供することを目的とする。【解決手段】実施形態の溶質の回収方法は、初期溶液に重金属除去剤を添加する重金属除去ステップと、重金属除去剤が添加された初期溶液を第1の液相と第1の固相に固液分離する第1の固液分離ステップと、第1の液相にリン除去剤を添加するリン除去ステップと、リン除去剤が添加された第1の液相を第2の液相と第2の固相に固液分離する第2の固液分離ステップと、を備え、初期溶液は焼却灰から放射性核種を抽出した後に放射性核種が回収された溶液であるものとする。【選択図】図3
摘要翻译：要解决的问题：提供能够从包括重金属和磷的强酸性溶液中选择性地回收重金属和磷的溶质的溶质和回收装置的回收方法。解决方案：实施方案的溶质回收方法包括将重金属去除剂添加到初始溶液中的重金属去除步骤，将已经添加有重金属去除剂的初始溶液固液分离到第一液相中的第一固液分离步骤和第一固相，磷除去步骤，向第一液相中加入除磷剂;以及第二固 - 液分离步骤，将已经加入除磷剂的第一液相固液分离到第二液相中，第二固相; 初始溶液是通过从焚烧灰中提取放射性核素然后回收放射性核素获得的溶液。

2. 发明专利

JP2014019898A Method for recovering rhenium 有权
标题翻译：回收铑的方法
公开(公告)号：JP2014019898A
公开(公告)日：2014-02-03
申请号：JP2012159070
申请日：2012-07-17
申请人： Toshiba Corp , 株式会社東芝
发明人： KANEMURA SHOHEI , MIZUGUCHI KOJI , TAKAHASHI YUYA , YAMASHITA TAKEO , YAITA YUMI , OSATO TETSUO , OMORI TAKASHI , YAZAWA TAKASHI , FUJITA REIKO
IPC分类号： C22B61/00 , C22B3/04 , C22B3/44 , C25B1/00
CPC分类号： Y02P10/234
摘要： PROBLEM TO BE SOLVED: To provide a method for recovering rhenium not using an ion exchange resin or a solvent extraction method.SOLUTION: The method for recovering rhenium comprises: a step (S11) of adding bivalent iron ions (Fe)to a rhenium-containing liquid 1a; a step (S12) of adding a Ph regulator 3 to precipitate rhenium; a step (S13) of recovering precipitates 5 from a mother liquid 4 by solid-liquid separation; and a step of adding acid to the precipitates 5 to dissolve rhenium (S14) and producing a rhenium-concentrated liquid 6.
摘要翻译：要解决的问题：提供不使用离子交换树脂的铼的回收方法或溶剂萃取方法。解决方案：回收铼的方法包括：将二价铁离子（Fe）添加到铼 - 容纳液体1a; 添加Ph调节剂3以沉淀铼的步骤（S12）; 通过固液分离从母液4回收沉淀物5的步骤（S13）; 以及向沉淀物5中加入酸以溶解铼的步骤（S14）并产生铼浓缩液体6。

3. 发明专利

JP2013101008A Treatment method and treatment device for radioactive cesium and radioactive strontium contained substance 审中-公开
标题翻译：用于放射性硒和放射性锶含有物质的处理方法和处理装置
公开(公告)号：JP2013101008A
公开(公告)日：2013-05-23
申请号：JP2011244091
申请日：2011-11-08
申请人： Toshiba Corp , 株式会社東芝
发明人： MIKURA MICHITAKA , HARUGUCHI YOSHIKO , OMURA TSUNEO , AKAI YOSHIE , YAMASHITA TAKEO , SUGIMORI TOSHIAKI , MIYAMOTO MASAYA
IPC分类号： G21F9/28 , G21F9/08
摘要： PROBLEM TO BE SOLVED: To easily and efficiently remove radioactive cesium and radioactive strontium from a substance such as soil or mud contaminated by the radioactive cesium and the radioactive strontium.SOLUTION: An organic substance from which cesium and strontium is selectively extractable is brought into contact with a substance containing radioactive cesium and radioactive strontium. Then, at least supercritical carbon dioxide is supplied to and brought into contact with at least the organic substance, and the organic substance is dissolved in the supercritical carbon dioxide. Then, the supercritical carbon dioxide is decompressed, and the supercritical carbon dioxide is converted into carbon dioxide gas so that the organic substance can be separated and removed from the supercritical carbon dioxide.
摘要翻译：要解决的问题：从放射性铯和放射性锶污染的土壤或泥土等物质容易有效地清除放射性铯和放射性锶。解决方案：将铯和锶选择性萃取的有机物质与含有放射性铯和放射性锶的物质接触。然后，至少将超临界二氧化碳供给至少与有机物质接触，有机物质溶解在超临界二氧化碳中。然后，将超临界二氧化碳减压，将超临界二氧化碳转化成二氧化碳，使有机物质从超临界二氧化碳中分离除去。版权所有（C）2013，JPO＆INPIT

4. 发明专利

JP2013014793A Method of producing rare metal 有权
标题翻译：生产稀有金属的方法
公开(公告)号：JP2013014793A
公开(公告)日：2013-01-24
申请号：JP2011146565
申请日：2011-06-30
申请人： Toshiba Corp , 株式会社東芝
发明人： MIZUGUCHI KOJI , KANEMURA SHOHEI , OSATO TETSUO , TAKAHASHI YUYA , YAITA YUMI , YAMASHITA TAKEO , FUJITA REIKO , OMORI TAKASHI , YAZAWA TAKASHI
IPC分类号： C25C1/22 , C22B3/04 , C22B3/26 , C22B3/42 , C22B3/44 , C22B59/00 , C22B61/00 , C25C3/34
CPC分类号： C22B3/0005 , C22B3/42 , C22B3/46 , C22B59/00 , C22B61/00 , C25C3/34 , Y02P10/234
摘要： PROBLEM TO BE SOLVED: To provide a method of producing rare metal of high robustness with respect to a solution composition, including a process of removing impurities from a raw material solution.SOLUTION: The method of producing rare metal includes steps (S11 to S14) of recovering a first residual liquid, steps (S15, S16) of extracting ReO, a step (S17) of back-extracting the same into a first eluent, steps (S18, S19) of collecting Re onto a cathode by way of electrolysis, a step (S20) of recovering a second residual liquid, steps (S21, S22) of adjusting hydrogen ion exponent in a range of not lower than pH 3 and lower than pH 5, steps (S23, S24) of extracting rare earth metal ion (Re), a step (S25) of back-extracting the same into a second eluent, a step (S26) of adding (COOH)to precipitate Re(CO), steps (S27, S28) of converting it to a rare earth metal oxide (ReO), and steps (S29, S30) of collecting rare earth metal (Re) onto a cathode by way of molten salt electrolysis.
摘要翻译：待解决的问题：提供一种制备相对于溶液组合物具有高坚固性的稀有金属的方法，包括从原料溶液中除去杂质的方法。解决方案：稀土金属的制造方法包括回收第一残留液的工序（S11〜S14），提取ReO 4 3 + ），将第二洗脱液反萃取的步骤（S25），添加（COOH） 2 以沉淀Re 2 （C 2 O 4 ） 3 ，将其转换为稀土金属氧化物的步骤（S27，S28）（Re 2 O 3）和通过熔融盐电极将稀土金属（Re）收集到阴极上的步骤（S29,301）裂解。版权所有（C）2013，JPO＆INPIT

5. 发明专利

JP2012225663A Quantitative analysis method of plutonium 审中-公开
标题翻译：钚的定量分析方法
公开(公告)号：JP2012225663A
公开(公告)日：2012-11-15
申请号：JP2011090701
申请日：2011-04-15
申请人： Toshiba Corp , 株式会社東芝
发明人： YAMASHITA TAKEO , MIKURA MICHITAKA , KUROSAWA SETSUMI , MURATA EIICHI , MATSUYAMA KANAE , HARUGUCHI YOSHIKO , SAKURAI JIRO , HIROSE EMIKO
IPC分类号： G01T1/167
摘要： PROBLEM TO BE SOLVED: To provide Pu (plutonium) quantitative analysis method capable of quantitatively analyzing Pu by using radiation measurement such as α-ray spectrometry even in an analysis target sample solution containing much impurity elements such as Ca interrupting α-ray measurement.SOLUTION: The Pu quantitative analysis method for quantitatively analyzing Pu in an analysis target sample solution 10 includes: an iron hydroxide coprecipitation step S101 for generating iron hydroxide coprecipitate 12 containing a rare earth element by adding rare earth compound and iron compound to the analysis target sample solution 10; a rare earth fluoride coprecipitation step S104 for generating rare earth fluoride coprecipitate 15 by adding fluoride to an iron hydroxide coprecipitate solution 13 obtained by dissolving the iron hydroxide coprecipitate 12; and a radiation measurement step S107 for quantitatively analyzing Pu by radiation measurement of a measuring sample 16 prepared from the rare earth fluoride coprecipitate 15.
摘要翻译：要解决的问题：为了提供能够通过使用诸如α射线光谱法的辐射测量来定量分析Pu的Pu（钚）定量分析方法，即使在含有大量杂质元素如Ca中断α-射线的分析目标样品溶液中测量。解决方案：用于在分析对象样品溶液10中定量分析Pu的Pu定量分析方法包括：通过向稀土化合物和铁化合物添加含有稀土元素的氢氧化铁共沉淀物12的氢氧化铁共沉淀步骤S101，分析目标样品溶液10; 稀土氟化物共沉淀步骤S104，用于通过将氟化氢沉淀物12溶解得到的氢氧化铁共沉淀溶液13中加入氟化物来生成稀土氟化物共沉淀物15; 以及辐射测量步骤S107，用于通过由稀土氟化物共沉淀物15制备的测量样品16的辐射测量来定量分析Pu。（C）2013，JPO和INPIT

6. 发明专利

JP2012150044A Method and device for analyzing nuclide in reactor water 审中-公开
标题翻译：用于分析反应器水中的核素的方法和装置
公开(公告)号：JP2012150044A
公开(公告)日：2012-08-09
申请号：JP2011009794
申请日：2011-01-20
申请人： Toshiba Corp , 株式会社東芝
发明人： MURATA EIICHI , MIKURA MICHITAKA , YAMASHITA TAKEO , OBATA MASAMICHI
IPC分类号： G01N1/28 , G01N1/10 , G01N31/00 , G01T1/167 , G21C17/02
摘要： PROBLEM TO BE SOLVED: To provide a nuclide analysis technology for reactor water which improves accuracy in quantifying radioactive nuclide included in reactor water.SOLUTION: The nuclide analysis technology for reactor water involves steps of: collecting reactor water and passing it through a filter (S11); heating the filter in which nuclide have been collected, with alkali hydroxide and alkaline nitrate (S15); dissolving a product from the heating step into water (S16); and separating a first filtrate in which at least radioactive chlorine and radioactive iodine are dissolved, and a first precipitate which is insoluble to the water (S17).
摘要翻译：要解决的问题：为反应堆水提供核素分析技术，提高定量反应堆水中放射性核素的准确性。解决方案：反应堆水的核素分析技术包括以下步骤：收集反应堆水并通过过滤器（S11）; 用碱性氢氧化物和碱性硝酸盐加热其中已经收集了核素的过滤器（S15）; 将产品从加热步骤溶解到水中（S16）; 并分离其中至少溶解有放射性氯和放射性碘的第一滤液和不溶于水的第一沉淀物（S17）。版权所有（C）2012，JPO＆INPIT

7. 发明专利

JP2012093284A Radioactive effluent treatment method and treatment equipment 审中-公开
标题翻译：放射性治疗方法和治疗设备
公开(公告)号：JP2012093284A
公开(公告)日：2012-05-17
申请号：JP2010241960
申请日：2010-10-28
申请人： Toshiba Corp , 株式会社東芝
发明人： HARUGUCHI YOSHIKO , MIYAMOTO MASAYA , MATSUYAMA KANAE , MIKURA MICHITAKA , YAMASHITA TAKEO , MURAI MASATO
IPC分类号： G21F9/12
摘要： PROBLEM TO BE SOLVED: To avoid corrosion of facility equipment by conveniently removing halogen-based ions from effluents containing halogen-based ions (compounds) such as effluents from scrubber treatment of off-gas generated by nuclear facilities.SOLUTION: An adsorbate and a radioactive effluent containing halogen-based ions are brought into contact for absorption of the halogen-based ions into the adsorbate to remove the halogen-based ions from the radioactive effluent. Then, the adsorbate is brought into contact with a solution containing carbonate ions to desorb and collect the halogen-based ions from the adsorbate.
摘要翻译：要解决的问题：为了通过方便地从含有卤素离子（化合物）的废水中除去卤素离子以避免设备设备的腐蚀，例如来自洗涤器处理由核设施产生的废气的废气。解决方案：使含有卤素离子的吸附物和放射性污染物接触，以将卤素基离子吸收到吸附物中以从放射性流出物中除去卤素基离子。然后，将吸附物与含有碳酸根离子的溶液接触以解吸并从被吸附物中收集卤素类离子。版权所有（C）2012，JPO＆INPIT

8. 发明专利

JP2011158353A Method and system for treatment of solid-state radioactive waste 审中-公开
标题翻译：用于处理固态放射性废物的方法和系统
公开(公告)号：JP2011158353A
公开(公告)日：2011-08-18
申请号：JP2010020157
申请日：2010-02-01
申请人： Toshiba Corp , 株式会社東芝
发明人： SHOJI YUICHI , SATO TATSUAKI , KANEKO MASAAKI , MIYAMOTO MASAYA , YAMASHITA TAKEO , KOMATSUBARA MASARU
IPC分类号： G21F9/36 , G21F9/30
摘要： PROBLEM TO BE SOLVED: To provide a method and system for treatment of solid-state radioactive waste, capable of decreasing the percentage of void in a disposal cask, without generating a hydrogen gas caused by the radiolysis of water.
SOLUTION: The method has an injection step S11 for injecting solid-state radioactive waste into a disposal cask, a stowing step S12 for stowing disposal casks into which the solid-state radioactive waste is injected in a waste storage cask and a filling step S17 for filling two or more kinds of powder and granular materials into interstices between the solid-state radioactive waste and the disposal cask and those between the waste storage cask and the disposal cask by combining two or more kinds of power and granular materials whose average particle diameters are different and injecting them into the waste storage cask.
COPYRIGHT: (C)2011,JPO&INPIT
摘要翻译：要解决的问题：提供一种处理固体放射性废物的方法和系统，其能够降低处理桶中空隙的百分比，而不产生由水的辐射分解引起的氢气。解决方案：该方法具有用于将固体放射性废物注入到处理桶中的注射步骤S11，用于将固体放射性废物注入到废物储存桶中的收集处理桶的收集步骤S12和填充物步骤S17，将两种或更多种粉末和颗粒材料通过组合两种或更多种动力和颗粒材料，将两种或更多种粉末和颗粒材料填充到固态放射性废物和处理桶之间的空隙中以及废物储存桶和处理桶之间的间隙颗粒直径不同，并将其注入废物储存桶。版权所有（C）2011，JPO＆INPIT

9. 发明专利

JP2011115772A Method and apparatus for treating waste liquid 有权
标题翻译：用于处理废液的方法和装置
公开(公告)号：JP2011115772A
公开(公告)日：2011-06-16
申请号：JP2010034185
申请日：2010-02-19
申请人： Toshiba Corp , 株式会社東芝
发明人： MIYAMOTO MASAYA , MATSUYAMA KANAE , YAMASHITA TAKEO , HARUGUCHI YOSHIKO , MIKURA MICHITAKA , KANEKO MASAAKI , KAWABE AKIHIRO
IPC分类号： C02F1/28 , B01J20/06 , B01J20/08 , G21F9/10 , G21F9/12
摘要： PROBLEM TO BE SOLVED: To simply remove halogen from a waste liquid that contains halogen (or a halogenated compound), such as a scrubber treatment waste liquid of an offgas generated from a nuclear facility, to avoid the corrosion of facility equipment.
SOLUTION: The waste liquid containing a halogenated compound is fed into an adsorption device, to which an absorbing substance is filled, to contact with the absorbing substance to make the absorbing substance absorb the halogenated compound so that the halogenated compound is removed from the waste liquid.
COPYRIGHT: (C)2011,JPO&INPIT

10. 发明专利

JP2006071322A Method and system for disposing of radioactive metal waste 审中-公开
标题翻译：放射性金属废物处理方法与系统
公开(公告)号：JP2006071322A
公开(公告)日：2006-03-16
申请号：JP2004252049
申请日：2004-08-31
申请人： Toshiba Corp , Toshiba Plant Systems & Services Corp , 東芝プラントシステム株式会社 , 株式会社東芝
发明人： YAMASHITA TAKEO , KUMANOMIDOU HIRONORI , SATO TATSUAKI , MIKURA MICHITAKA , SAKURAI JIRO , TAKADA TAKAO , HIROSE EMIKO , NATSUI KAZUJI , TAJIMA FUMIO
IPC分类号： G21F9/36 , B09B1/00 , G21F9/30
摘要： PROBLEM TO BE SOLVED: To conveniently prepare radioactive metal waste bodies which do not emit any gases.
SOLUTION: A method and a system in this invention have processes of: (3) pouring radioactive metal waste 2 into a waste container 1; (4) drying the inside of the waste container 1 after the process 3; (6) drying particulates 5 made of inorganic substances; and (7) pouring the particulates 5 into the waste container 1 after the processes 4 and 6 and filling the interstices of metal waste 2 in the waste container 1 with the particulates 5.
COPYRIGHT: (C)2006,JPO&NCIPI
摘要翻译：要解决的问题：方便地制备不排放任何气体的放射性金属废物体。解决方案：本发明的方法和系统具有以下过程：（3）将放射性金属废物2倒入废物容器1中; （4）在处理3之后干燥废物容器1的内部; （6）由无机物质制成的干燥颗粒5; （7）在处理4和6之后将颗粒物5倒入废物容器1中，并用颗粒物5填充废弃物容器1中的金属废物2的间隙。（C）2006，JPO＆NCIPI

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