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1. 发明授权

US5708175A Process for producing 4-trifluoromethylnicotinic acid 失效
标题翻译：生产4-三氟甲基烟酸的方法
公开(公告)号：US5708175A
公开(公告)日：1998-01-13
申请号：US648761
申请日：1996-05-16
申请人： Toru Koyanagi , Tetsuo Yoneda , Fumio Kanamori , Shigehisa Kanbayashi , Toyoshi Tanimura , Noriyuki Horiuchi
发明人： Toru Koyanagi , Tetsuo Yoneda , Fumio Kanamori , Shigehisa Kanbayashi , Toyoshi Tanimura , Noriyuki Horiuchi
IPC分类号： C07C45/45 , C07C49/255 , C07C221/00 , C07C225/14 , C07C229/22 , C07C229/30 , C07C251/08 , C07D213/80 , C07D213/12 , C07D213/08
CPC分类号： C07D213/80 , C07C221/00 , C07C229/22 , C07C229/30 , C07C251/08 , C07C45/455 , C07C49/255
摘要： A process for producing 4-trifluoromethylnicotinic acid of the formula (VIII) or its salt: ##STR1## which comprises (i) a first step of reacting a halide of the formula (I): CF.sub.3 COHal (I) wherein Hal is a halogen atom, with a compound of the formula (II): CH.sub.2 .dbd.CHOR.sup.1 (II) wherein R.sup.1 is an alkyl group, in the presence of a base to obtain a 4-alkoxy-1,1,1-trifluoro-3-buten-2-one of the formula (III): CF.sub.3 CO--CH.dbd.CH--OR.sup.1 (III) wherein R.sup.1 is as defined above, and reacting this compound with ammonia to obtain 4-amino-1,1,1-trifluoro-3-buten-2-one of the formula (IV): ##STR2## and (ii) a second step of subjecting the 4-amino-1,1,1-trifluoro-3-buten-2-one obtained in the first step and a compound of the formula (V): ACO.sub.2 R.sup.2 (V) wherein R.sup.2 is an ester-forming residue, and A is (R.sup.3 O)CH.dbd.CH-- or (R.sup.3 O).sub.2 CHCH.sub.2 --, wherein R.sup.3 is an alkyl group, to a condensation reaction to obtain a compound of the formula (VI) (inclusive of its salt): ##STR3## wherein R.sup.2 is as defined above, and/or a compound of the formula (VII) (inclusive of its salt): ##STR4## wherein R.sup.2 and R.sup.3 are as defined above, as the reaction product, and then subjecting the reaction product to ring closure and hydrolysis.
摘要翻译：（VIII）的4-三氟甲基烟酸或其盐：（Ⅷ）的方法，其包括（ⅰ）使式（I）的卤化物：CF 3 COHal（I）（其中Hal为卤素原子与式（II）的化合物：CH 2 = CHOR 1（II）其中R 1是烷基，在碱的存在下，得到4-烷氧基-1,1,1-三氟-3- （III）的丁烯-2-酮：CF 3 CO-CH = CH-OR 1（III）其中R 1如上定义，并使该化合物与氨反应，得到4-氨基-1,1,1-三氟-3 （IV）的2-丁烯-2-酮：（IV）和（ii）第二步，将得到的4-氨基-1,1,1-三氟-3-丁烯-2-酮第一步和式（V）化合物：其中R 2为酯形成残基，A为（R 3 O）CH = CH-或（R 3 O）2 CHCH 2 - ，其中R 3为烷基，进行缩合反应，得到式（VI）化合物（包括其盐）：其中R 2如上所定义，和/或式（VII）（包括其盐）：其中R2和R3如上定义，作为反应产物，然后使反应产物闭环并水解。

2. 发明申请

US20110034696A1 PROCESS FOR PRODUCING ANTHRANILAMIDE COMPOUND 有权
标题翻译：生产苯磺酰胺化合物的方法
公开(公告)号：US20110034696A1
公开(公告)日：2011-02-10
申请号：US12937647
申请日：2009-04-10
申请人： Kazuhiro Yamamoto , Tetsuo Yoneda , Fumio Kanamori , Shigehisa Kanbayashi , Toyoshi Tanimura , Yohei Taguchi , Tatsunori Yoshida
发明人： Kazuhiro Yamamoto , Tetsuo Yoneda , Fumio Kanamori , Shigehisa Kanbayashi , Toyoshi Tanimura , Yohei Taguchi , Tatsunori Yoshida
IPC分类号： C07D401/04
CPC分类号： C07D401/04
摘要： To provide a process for producing an anthranilamide having the 3-position of pyrazole substituted by a bromine atom, or its salt.A process for producing an anthranilamide compound represented by the formula (I) or its salt: which comprises reacting a compound represented by the formula (II): (wherein Z is 2-pyridyl, 3-pyridyl, 4-pyridyl or benzene substituted by a nitro group), with a brominating agent, to produce a compound represented by the formula (III): and further reacting the compound of the formula (III) with an oxidizing agent.
摘要翻译：提供制备具有由溴原子取代的吡唑3-位的邻氨基苯甲酰胺或其盐的方法。一种制备由式（I）表示的邻氨基苯甲酰胺化合物或其盐的方法：其包括使式（II）表示的化合物：其中Z为2-吡啶基，3-吡啶基，4-吡啶基或被硝基）与溴化剂反应，生成由式（III）表示的化合物：进一步使式（III）的化合物与氧化剂反应。

3. 发明授权

US08481744B2 Process for producing anthranilamide compound 有权
标题翻译：邻氨基苯甲酰胺化合物的制备方法
公开(公告)号：US08481744B2
公开(公告)日：2013-07-09
申请号：US12937647
申请日：2009-04-10
申请人： Kazuhiro Yamamoto , Tetsuo Yoneda , Fumio Kanamori , Shigehisa Kanbayashi , Toyoshi Tanimura , Yohei Taguchi , Tatsunori Yoshida
发明人： Kazuhiro Yamamoto , Tetsuo Yoneda , Fumio Kanamori , Shigehisa Kanbayashi , Toyoshi Tanimura , Yohei Taguchi , Tatsunori Yoshida
IPC分类号： C07D401/04
CPC分类号： C07D401/04
摘要： To provide a process for producing an anthranilamide having the 3-position of pyrazole substituted by a bromine atom, or its salt.A process for producing an anthranilamide compound represented by the formula (I) or its salt: which comprises reacting a compound represented by the formula (II): (wherein Z is 2-pyridyl, 3-pyridyl, 4-pyridyl or benzene substituted by a nitro group), with a brominating agent, to produce a compound represented by the formula (III): and further reacting the compound of the formula (III) with an oxidizing agent.
摘要翻译：提供制备具有由溴原子取代的吡唑3-位的邻氨基苯甲酰胺或其盐的方法。一种制备由式（I）表示的邻氨基苯甲酰胺化合物或其盐的方法：其包括使式（II）表示的化合物：其中Z为2-吡啶基，3-吡啶基，4-吡啶基或被硝基）与溴化剂反应，生成由式（III）表示的化合物：进一步使式（III）的化合物与氧化剂反应。

4. 发明授权

US08115006B2 Process for producing anthranilamide compound 有权
标题翻译：邻氨基苯甲酰胺化合物的制备方法
公开(公告)号：US08115006B2
公开(公告)日：2012-02-14
申请号：US12519177
申请日：2007-12-14
申请人： Toru Koyanagi , Kazuhiro Yamamoto , Tetsuo Yoneda , Shigehisa Kanbayashi , Toyoshi Tanimura , Yohei Taguchi , Tatsunori Yoshida
发明人： Toru Koyanagi , Kazuhiro Yamamoto , Tetsuo Yoneda , Shigehisa Kanbayashi , Toyoshi Tanimura , Yohei Taguchi , Tatsunori Yoshida
IPC分类号： C07D401/04
CPC分类号： C07D401/04 , C07C237/30 , C07C237/42 , C07C2601/02 , C07C2601/04 , C07D231/08 , C07D267/06
摘要： To provide a process for producing a specific anthranilamide compound or its salt.To provide a process for producing an anthranilamide compound represented by the formula (I) or its salt: wherein each of R1a and R3 which are independent of each other, is halogen or haloalkyl; R2 is cyclopropyl alkyl or cyclobutyl alkyl; and Hal is a chlorine atom or a bromine atom, which comprises a step of selectively halogenating a compound represented by the formula (II): wherein R1a, R2 and R3 are as defined above.
摘要翻译：提供制备特定的邻氨基苯甲酰胺化合物或其盐的方法。提供一种制备由式（I）表示的邻氨基苯甲酰胺化合物或其盐：其中彼此独立的R 1a和R 3各自为卤素或卤代烷基; R2是环丙基烷基或环丁基烷基; 和Hal是氯原子或溴原子，其包括选择性卤化由式（II）表示的化合物的步骤：其中R 1a，R 2和R 3如上所定义。

5. 发明申请

US20100063293A1 PROCESS FOR PRODUCING ANTHRANILAMIDE COMPOUND 有权
标题翻译：生产苯磺酰胺化合物的方法
公开(公告)号：US20100063293A1
公开(公告)日：2010-03-11
申请号：US12519177
申请日：2007-12-14
申请人： Toru Koyanagi , Kazuhiro Yamamoto , Tetsuo Yoneda , Shigehisa Kanbayashi , Toyoshi Tanimura , Yohei Taguchi , Tatsunori Yoshida
发明人： Toru Koyanagi , Kazuhiro Yamamoto , Tetsuo Yoneda , Shigehisa Kanbayashi , Toyoshi Tanimura , Yohei Taguchi , Tatsunori Yoshida
IPC分类号： C07D401/04 , C07C233/00 , C07D231/00
CPC分类号： C07D401/04 , C07C237/30 , C07C237/42 , C07C2601/02 , C07C2601/04 , C07D231/08 , C07D267/06
摘要： To provide a process for producing a specific anthranilamide compound or its salt.To provide a process for producing an anthranilamide compound represented by the formula (I) or its salt: wherein each of R1a and R3 which are independent of each other, is halogen or haloalkyl; R2 is cyclopropyl alkyl or cyclobutyl alkyl; and Hal is a chlorine atom or a bromine atom, which comprises a step of selectively halogenating a compound represented by the formula (II): wherein R1a, R2 and R3 are as defined above.
摘要翻译：提供制备特定的邻氨基苯甲酰胺化合物或其盐的方法。提供一种制备由式（I）表示的邻氨基苯甲酰胺化合物或其盐：其中彼此独立的R 1a和R 3各自为卤素或卤代烷基; R2是环丙基烷基或环丁基烷基; 和Hal是氯原子或溴原子，其包括选择性卤化由式（II）表示的化合物的步骤：其中R 1a，R 2和R 3如上所定义。

6. 发明授权

US08729106B2 Pesticidal compositions 有权
标题翻译：杀虫剂组合物
公开(公告)号：US08729106B2
公开(公告)日：2014-05-20
申请号：US12516649
申请日：2007-12-12
申请人： Toru Koyanagi , Masayuki Morita , Tetsuo Yoneda , Tsuyoshi Ueda , Kazuhisa Kiriyama , Taku Hamamoto
发明人： Toru Koyanagi , Masayuki Morita , Tetsuo Yoneda , Tsuyoshi Ueda , Kazuhisa Kiriyama , Taku Hamamoto
IPC分类号： A01N43/40 , A01N25/32
CPC分类号： A01N43/56 , A01N43/08 , A01N43/40 , A01N43/78 , A01N53/00 , A01N57/32 , A01N2300/00
摘要： A pesticidal composition comprising synergistically effective amounts of at least one anthranilamide compound represented by the formula (I) or its salt and other pesticide: wherein each of R1a and R1b which are independent of each other, is halogen; each of R2 and R3 is halogen, alkyl, haloalkyl, alkoxy, haloalkoxy or cyano; A is alkyl substituted by Y; Y is C3-4 cycloalkyl which may be substituted by at least one substituent selected from the group consisting of halogen, alkyl and haloalkyl; n is 0 or 1; and q is an integer of from 0 to 4; provided that R1a and R1b are not simultaneously chlorine nor bromine.
摘要翻译：一种杀虫组合物，其包含协同有效量的由式（I）表示的至少一种邻氨基苯甲酰胺化合物或其盐和其它农药：其中彼此独立的R 1a和R 1b各自为卤素; R2和R3各自为卤素，烷基，卤代烷基，烷氧基，卤代烷氧基或氰基; A是被Y取代的烷基; Y是可被至少一个选自卤素，烷基和卤代烷基的取代基取代的C3-4环烷基; n为0或1; q为0〜4的整数，条件是R1a和R1b不同时为氯或溴。

7. 发明申请

US20100028304A1 PESTICIDAL COMPOSITIONS 有权
标题翻译：农药组合物
公开(公告)号：US20100028304A1
公开(公告)日：2010-02-04
申请号：US12516649
申请日：2007-12-12
申请人： Toru Koyanagi , Masayuki Morita , Tetsuo Yoneda , Tsuyoshi Ueda , Kazuhisa Kiriyama , Taku Hamamoto
发明人： Toru Koyanagi , Masayuki Morita , Tetsuo Yoneda , Tsuyoshi Ueda , Kazuhisa Kiriyama , Taku Hamamoto
IPC分类号： A01N43/40 , A01N63/02 , A01N63/04 , A01P7/04 , A01P3/00
CPC分类号： A01N43/56 , A01N43/08 , A01N43/40 , A01N43/78 , A01N53/00 , A01N57/32 , A01N2300/00
摘要： A pesticidal composition comprising synergistically effective amounts of at least one anthranilamide compound represented by the formula (I) or its salt and other pesticide: wherein each of R1a and R1b which are independent of each other, is halogen; each of R2 and R3 is halogen, alkyl, haloalkyl, alkoxy, haloalkoxy or cyano; A is alkyl substituted by Y; Y is C3-4 cycloalkyl which may be substituted by at least one substituent selected from the group consisting of halogen, alkyl and haloalkyl; n is 0 or 1; and q is an integer of from 0 to 4; provided that R1a and R1b are not simultaneously chlorine nor bromine.
摘要翻译：一种杀虫组合物，其包含协同有效量的由式（I）表示的至少一种邻氨基苯甲酰胺化合物或其盐和其它农药：其中彼此独立的R 1a和R 1b各自为卤素; R2和R3各自为卤素，烷基，卤代烷基，烷氧基，卤代烷氧基或氰基; A是被Y取代的烷基; Y是可被至少一个选自卤素，烷基和卤代烷基的取代基取代的C3-4环烷基; n为0或1; q为0〜4的整数，条件是R1a和R1b不同时为氯或溴。

8. 发明授权

US5360806A Amide compounds and their salts and pesticidal compositions containing them 失效
标题翻译：酰胺化合物及其盐和含有它们的农药组合物
公开(公告)号：US5360806A
公开(公告)日：1994-11-01
申请号：US95192
申请日：1993-07-23
申请人： Tadaaki Toki , Toru Koyanagi , Masayuki Morita , Tetsuo Yoneda , Chiharu Kagimoto , Hiroshi Okada
发明人： Tadaaki Toki , Toru Koyanagi , Masayuki Morita , Tetsuo Yoneda , Chiharu Kagimoto , Hiroshi Okada
IPC分类号： A01N43/40 , C07D213/82 , C07D213/89 , C07D401/12 , C07D401/14 , C07D413/12
CPC分类号： C07D213/82 , A01N43/40 , C07D213/89
摘要： The present invention relates to an amide compound and its salt, process for its production and a pesticidal composition containing it.The amide compound of the formula (I) or its salt: ##STR1## wherein the radicals are defined in the claims.
摘要翻译：本发明涉及酰胺化合物及其盐，其生产方法和含有它的杀虫组合物。式（I）的酰胺化合物或其盐：其中基团在权利要求中定义。

9. 发明授权

US5288727A Hydrazone compounds, processes for their production, intermediates useful for their production and pesticidal compositions containing them 失效
标题翻译：腙化合物，其制备方法，可用于其生产的中间体和含有它们的杀虫组合物
公开(公告)号：US5288727A
公开(公告)日：1994-02-22
申请号：US834835
申请日：1992-02-13
申请人： Tadaaki Toki , Toru Koyanagi , Kiyomitsu Yoshida , Hiroshi Sasaki , Masayuki Morita , Tetsuo Yoneda
发明人： Tadaaki Toki , Toru Koyanagi , Kiyomitsu Yoshida , Hiroshi Sasaki , Masayuki Morita , Tetsuo Yoneda
IPC分类号： H01L21/02 , A01N33/00 , A01N35/10 , A01N37/52 , A01N47/06 , A01N47/24 , A01N47/34 , A01N55/00 , C07C45/00 , C07C45/27 , C07C49/215 , C07C49/233 , C07C49/782 , C07C49/813 , C07C249/16 , C07C251/08 , C07C251/72 , C07C251/86 , C07C251/88 , C07C257/02 , C07C257/06 , C07C257/22 , C07C281/04 , C07C281/14 , C07C303/30 , C07C303/40 , C07C309/65 , C07C309/66 , C07C309/73 , C07C311/08 , C07C311/49 , C07C317/32 , C07C319/20 , C07C323/45 , C07C323/48 , C07C323/65 , C07F7/18 , C07F9/09 , H01L21/677 , H01L21/68 , C07C251/80 , A01N47/40
CPC分类号： C07C323/65 , A01N35/10 , A01N37/52 , A01N47/06 , A01N47/24 , A01N47/34 , A01N55/00 , C07C251/86 , C07C251/88 , C07C257/06 , C07C257/22 , C07C281/04 , C07C281/14 , C07C309/65 , C07C309/66 , C07C309/73 , C07C311/08 , C07C311/49 , C07C317/32 , C07C323/45 , C07C45/004 , C07C45/27 , C07C49/782 , C07C49/813
摘要： The present invention relates to a hydrazone compound of the formula (I) or its salt, a process for its preparation, an intermediate of the formula (II-5), a pesticidal composition containing said hydrazone compound or its salt as the active ingredient, and a pesticidal method of applying an effective amount thereof: ##STR1##
摘要翻译：本发明涉及式（I）的腙化合物或其盐，其制备方法，式（II-5）的中间体，含有所述腙化合物或其盐作为活性成分的杀虫组合物，（*化学结构*）（I）（*化学结构*）（II-5）的有效量的杀虫剂法

10. 发明授权

US08093241B2 Acid amide derivatives, process for their production and pesticides containing them 有权
标题翻译：酸酰胺衍生物，其生产工艺和含有它们的农药
公开(公告)号：US08093241B2
公开(公告)日：2012-01-10
申请号：US12640140
申请日：2009-12-17
申请人： Yuji Nakamura , Masayuki Morita , Tetsuo Yoneda , Kenji Izakura
发明人： Yuji Nakamura , Masayuki Morita , Tetsuo Yoneda , Kenji Izakura
IPC分类号： A01N43/84 , A01N37/18 , A01N43/60 , A01N43/40 , A01N43/56 , A01N43/42 , C07C233/64 , C07D409/02 , C07D231/10 , C07D213/46 , C07D215/14 , C07D263/54
CPC分类号： A01N37/20 , C07C233/76 , C07C307/02 , C07C309/65 , C07C309/66 , C07C311/08 , C07C317/32 , C07C323/42 , C07C329/06 , C07D209/14 , C07D213/50 , C07D213/61 , C07D317/46 , C07D317/58 , C07D319/20 , C07D333/22 , C07D333/28
摘要： The present invention relates to an acid amid derivative of the formula (I) or a salt thereof: wherein A is phenyl which may be substituted by X, benzyl which may be substituted by X, naphthyl which may be substituted by X, a heterocyclic group which may be substituted by X, a fused heterocyclic group which may be substituted by X, indanyl (the indanyl may be substituted by halogen, alkyl or alkoxy) or tetrahydronaphthyl (the tetrahydronaphthyl may be substituted by halogen, alkyl or alkoxy), B is alkyl, cycloalkyl, phenyl which may be substituted by Y, a heterocyclic group which may be substituted by Y, or a condensed heterocyclic group which may be substituted by Y, each of R1 and R2 is alkyl, cyano or —CO2R14, or R1 and R2 may together form a 3- to 6-membered saturated carbocyclic ring, R3 is hydrogen, alkyl, alkoxyalkyl, alkylthioalkyl, —COR15, —S(O)mR16 or —S(O)nNR17R18, which is useful as an active ingredient of pesticides.
摘要翻译：本发明涉及式（I）的酸酰胺衍生物或其盐：其中A为可被X取代的苯基，可被X取代的苄基，可被X取代的萘基，杂环基其可以被X取代，可以被X取代的稠合杂环基，茚满基（茚满基可以被卤素，烷基或烷氧基取代）或四氢萘基（四氢萘基可以被卤素，烷基或烷氧基取代），B是烷基，环烷基，可被Y取代的苯基，可被Y取代的杂环基或可被Y取代的稠合杂环基，R 1和R 2各自为烷基，氰基或-CO 2 R 14，或R 1和 R2可以一起形成3至6元饱和碳环，R 3是氢，烷基，烷氧基烷基，烷硫基烷基，-COR 15，-S（O）m R 16或-S（O）n NR 17 R 18，其可用作农药。

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