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1. 发明申请

US20090281238A1 METHOD FOR FORMING ORGANIC THIN FILM 有权
标题翻译：形成有机薄膜的方法
公开(公告)号：US20090281238A1
公开(公告)日：2009-11-12
申请号：US12312096
申请日：2007-11-13
申请人： Tomoya Hidaka , Yoshitaka Fujita , Norifumi Nakamoto , Kazuhisa Kumazawa , Eiji Hoshi
发明人： Tomoya Hidaka , Yoshitaka Fujita , Norifumi Nakamoto , Kazuhisa Kumazawa , Eiji Hoshi
IPC分类号： C09D5/00
CPC分类号： C09D7/1233 , B05D1/185 , B05D7/24 , B05D2202/00 , B05D2203/35 , C03C17/30 , C03C2217/76 , C03C2218/113 , C08K5/01 , C08K5/04 , C08K5/05 , C08K5/5419 , C09D7/63 , C09K3/18
摘要： The object is to provide a method for forming an organic thin film which enables to form quickly a dense monomolecular film with less impurity. It is a method for forming an organic thin film which comprises:1) a step of preparing a hydroxyl group-containing solution by mixing the following (a), (b) and (c) so that the total amount of (A) and (B) in the hydroxyl group-containing solution becomes 0.1 wt % to 80 wt %, and conducting hydrolysis to generate a hydroxyl group-containing compound; a) an adjuvant for forming an organic thin film comprising a metal surfactant (A) having at least one or more hydrolysable group, and a compound (C) that can interact with the metal surfactant in an organic solvent b) a metal surfactant having at least one or more hydrolysable group (B), and c) water 2) a step of preparing a solution for forming an organic thin film by mixing an organic solvent and the hydroxyl group-containing solution obtained in the above step 1); and 3) a step of allowing the substrate to contact with the solution for forming an organic thin film obtained in the above step 2).
摘要翻译：本发明的目的是提供一种形成有机薄膜的方法，其能够快速形成具有较少杂质的致密单分子膜。形成有机薄膜的方法包括：1）通过混合以下（a），（b）和（c）制备含羟基溶液的步骤，使得（A）和含羟基溶液中的（B）成为0.1重量％〜80重量％，进行水解生成含羟基化合物; a）用于形成包含具有至少一个或多个可水解基团的金属表面活性剂（A）的有机薄膜的助剂和可在有机溶剂中与金属表面活性剂相互作用的化合物（C）b）具有至少一个或多个可水解基团（B）和c）水2）通过混合有机溶剂和在上述步骤1）中获得的含羟基溶液来制备用于形成有机薄膜的溶液的步骤; 和3）允许基板与用于形成上述步骤2）中获得的有机薄膜的溶液接触的步骤。

2. 发明授权

US08864896B2 Method for forming organic thin film 有权
标题翻译：有机薄膜形成方法
公开(公告)号：US08864896B2
公开(公告)日：2014-10-21
申请号：US12312096
申请日：2007-11-13
申请人： Tomoya Hidaka , Yoshitaka Fujita , Norifumi Nakamoto , Kazuhisa Kumazawa , Eiji Hoshi
发明人： Tomoya Hidaka , Yoshitaka Fujita , Norifumi Nakamoto , Kazuhisa Kumazawa , Eiji Hoshi
IPC分类号： C04B41/49 , B05D7/24 , C03C17/30 , C09K3/18 , B05D1/18
CPC分类号： C09D7/1233 , B05D1/185 , B05D7/24 , B05D2202/00 , B05D2203/35 , C03C17/30 , C03C2217/76 , C03C2218/113 , C08K5/01 , C08K5/04 , C08K5/05 , C08K5/5419 , C09D7/63 , C09K3/18
摘要： A method is provided for forming an organic thin film comprising: 1) preparing a hydroxyl group-containing solution by mixing the following (a), (b) and (c) so that the total amount of (A) and (B) in the hydroxyl group-containing solution becomes 0.1 wt% to 80 wt%, and conducting hydrolysis to generate a hydroxyl group-containing compound; a) an adjuvant for forming an organic thin film comprising a metal surfactant (A) having at least one or more hydrolysable group, and a compound (C) that can interact with the metal surfactant in an organic solvent b) a metal surfactant having at least one or more hydrolysable group (B), and c) water 2) preparing a solution for forming an organic thin film by mixing an organic solvent and the hydroxyl group-containing solution of 1); and 3) allowing the substrate to contact with the solution for forming an organic thin film of 2).
摘要翻译：提供一种用于形成有机薄膜的方法，其包括：1）通过混合以下（a），（b）和（c）来制备含羟基溶液，使得（A）和（B）的总量在含羟基溶液为0.1重量％〜80重量％，进行水解而生成含羟基的化合物; a）用于形成包含具有至少一个或多个可水解基团的金属表面活性剂（A）的有机薄膜的助剂和可在有机溶剂中与金属表面活性剂相互作用的化合物（C）b）具有至少一个或多个可水解基团（B），和c）水2）通过混合有机溶剂和含有羟基的溶液1）制备用于形成有机薄膜的溶液; 和3）允许基底与溶液接触以形成2）的有机薄膜。

3. 发明授权

US08197906B2 Method for producing organic thin film 有权
标题翻译：有机薄膜的制造方法
公开(公告)号：US08197906B2
公开(公告)日：2012-06-12
申请号：US12777666
申请日：2010-05-11
申请人： Nobuo Kimura , Yoshitaka Fujita , Norifumi Nakamoto , Tomoya Hidaka
发明人： Nobuo Kimura , Yoshitaka Fujita , Norifumi Nakamoto , Tomoya Hidaka
IPC分类号： B05D5/00
CPC分类号： C09D5/00 , B05D1/185 , C03C17/30 , Y10T428/261 , Y10T428/31504
摘要： A method for producing an organic thin film in which an organic thin film is formed on the surface of a substrate, including a step (A) of bringing the substrate into contact with an organic solvent solution containing a metal-based surfactant having at least one hydrolysable group, and a catalyst capable of interacting with the metal-based surfactant, wherein the water contact within the organic solvent solution is either set or maintained within a predetermined range.
摘要翻译：一种制造有机薄膜的方法，其中在基材表面上形成有机薄膜，该方法包括使基材与含有至少一种金属基表面活性剂的有机溶剂溶液接触的步骤（A）可水解基团和能够与金属基表面活性剂相互作用的催化剂，其中有机溶剂溶液中的水接触被设定或保持在预定范围内。

4. 发明授权

US08426019B2 Method for producing organic thin film 有权
标题翻译：有机薄膜的制造方法
公开(公告)号：US08426019B2
公开(公告)日：2013-04-23
申请号：US12833791
申请日：2010-07-09
申请人： Nobuo Kimura , Yoshitaka Fujita , Norifumi Nakamoto , Tomoya Hidaka
发明人： Nobuo Kimura , Yoshitaka Fujita , Norifumi Nakamoto , Tomoya Hidaka
IPC分类号： B32B33/00
CPC分类号： C09D5/00 , B05D1/185 , C03C17/30 , Y10T428/261 , Y10T428/31504
摘要： A method for producing an organic thin film, which enables rapid film formation, and enables a dense organic thin film with minimal impurities to be formed stably, and in a plurality of consecutive repetitions. Also, a method for producing an organic thin film in which an organic thin film is formed on the surface of a substrate, including bringing the substrate into contact with an organic solvent solution containing a metal-based surfactant having at least one hydrolysable group, and a catalyst capable of interacting with the metal-based surfactant, wherein the water contact within the organic solvent solution is either set or maintained within a predetermined range.
摘要翻译：一种制造有机薄膜的方法，其能够快速成膜，并且能够稳定地形成具有最小杂质的致密有机薄膜，并且能够连续重复多次。另外，制造有机薄膜的方法，其中有机薄膜形成在基片的表面上，包括使基片与含有至少一个可水解基团的金属基表面活性剂的有机溶剂溶液接触，以及能够与金属基表面活性剂相互作用的催化剂，其中有机溶剂溶液内的水接触被设定或保持在预定范围内。

5. 发明申请

US20110135878A1 Dispersoid having metal-oxygen bonds, metal oxide film, and monomolecular film 审中-公开
标题翻译：具有金属氧键的分散体，金属氧化物膜和单分子膜
公开(公告)号：US20110135878A1
公开(公告)日：2011-06-09
申请号：US12929592
申请日：2011-02-02
申请人： Nobuo Kimura , Yoshitaka Fujita , Norifumi Nakamoto , Motoyuki Toki , Akiji Higuchi , Kazuo Ono , Tomoya Hidaka , Hiroyuki Takeda
发明人： Nobuo Kimura , Yoshitaka Fujita , Norifumi Nakamoto , Motoyuki Toki , Akiji Higuchi , Kazuo Ono , Tomoya Hidaka , Hiroyuki Takeda
IPC分类号： B32B3/30 , B32B27/06 , C09D1/00 , C01B13/00
CPC分类号： C01B13/32 , C01G23/053 , C23C18/1216 , C23C18/122 , Y10T428/24355
摘要： Dispersoids having metal-oxygen groups that are suitable for the production of metal oxide thin-films at a low temperature of 200° C. or below and for the production of homogeneous organic-inorganic hybrid materials. The dispersoid having metal-oxygen bonds may be obtained by mixing a metal compound having at least three hydrolyzable groups with at least 0.5 mole but less than 2 moles of water per mole of the metal compound in an organic solvent, in the absence of an acid, a base, and/or a dispersion stabilizer, and at a temperature at or below the temperature at which the metal compound begins to hydrolyze, then raising the temperature to at least the temperature at which hydrolysis begins.
摘要翻译：具有适合于在200℃或更低的低温下生产金属氧化物薄膜并用于生产均相有机 - 无机杂化材料的金属 - 氧基的分散体。具有金属 - 氧键的分散质可以通过在不存在酸的情况下，在有机溶剂中将具有至少三个可水解基团的金属化合物与每摩尔金属化合物相混合至少0.5摩尔但小于2摩尔的水，碱和/或分散稳定剂，并且在等于或低于金属化合物开始水解的温度的温度下，然后将温度升至至少水解开始的温度。

6. 发明申请

US20100313789A1 METHOD FOR PRODUCING ORGANIC THIN FILM 有权
标题翻译：生产有机薄膜的方法
公开(公告)号：US20100313789A1
公开(公告)日：2010-12-16
申请号：US12833791
申请日：2010-07-09
申请人： Nobuo KIMURA , Yoshitaka Fujita , Norifumi Nakamoto , Tomoya Hidaka
发明人： Nobuo KIMURA , Yoshitaka Fujita , Norifumi Nakamoto , Tomoya Hidaka
IPC分类号： B05D1/02 , B05D1/18 , B05D1/28 , B05D5/00 , B05D3/12 , C09D7/00
CPC分类号： C09D5/00 , B05D1/185 , C03C17/30 , Y10T428/261 , Y10T428/31504
摘要： A method for producing an organic thin film, which enables rapid film formation, and enables a dense organic thin film with minimal impurities to be formed stably, and in a plurality of consecutive repetitions. Also, a method for producing an organic thin film in which an organic thin film is formed on the surface of a substrate, including bringing the substrate into contact with an organic solvent solution containing a metal-based surfactant having at least one hydrolysable group, and a catalyst capable of interacting with the metal-based surfactant, wherein the water contact within the organic solvent solution is either set or maintained within a predetermined range.
摘要翻译：一种制造有机薄膜的方法，其能够快速成膜，并且能够稳定地形成具有最小杂质的致密有机薄膜，并且能够连续重复多次。另外，制造有机薄膜的方法，其中有机薄膜形成在基片的表面上，包括使基片与含有至少一个可水解基团的金属基表面活性剂的有机溶剂溶液接触，以及能够与金属基表面活性剂相互作用的催化剂，其中有机溶剂溶液内的水接触被设定或保持在预定范围内。

7. 发明授权

US07776403B2 Method for producing organic thin film 有权
标题翻译：有机薄膜的制造方法
公开(公告)号：US07776403B2
公开(公告)日：2010-08-17
申请号：US10553109
申请日：2004-04-14
申请人： Nobuo Kimura , Yoshitaka Fujita , Norifumi Nakamoto , Tomoya Hidaka
发明人： Nobuo Kimura , Yoshitaka Fujita , Norifumi Nakamoto , Tomoya Hidaka
IPC分类号： B05D1/00 , B05D1/02 , B05D1/18 , B05D1/28 , B05D7/24 , C08J7/06 , C03C17/30
CPC分类号： C09D5/00 , B05D1/185 , C03C17/30 , Y10T428/261 , Y10T428/31504
摘要： An object of the present invention is to provide a method for producing an organic thin film, which enables rapid film formation, and enables a dense organic thin film with minimal impurities to be formed stably, and in a plurality of consecutive repetitions.The present invention provides a method for producing an organic thin film in which an organic thin film is formed on the surface of a substrate, including a step (A) of bringing the substrate into contact with an organic solvent solution containing a metal-based surfactant having at least one hydrolyzable group, and a catalyst capable of interacting with the metal-based surfactant, wherein the water content within the organic solvent solution is either set or maintained within a predetermined range.
摘要翻译：本发明的目的在于提供一种能够快速成膜的有机薄膜的制造方法，能够稳定地形成具有最小杂质的致密有机薄膜，并且能够连续重复多次。本发明提供一种有机薄膜的制造方法，其中在基材表面上形成有机薄膜，其包括使基板与含有金属类表面活性剂的有机溶剂溶液接触的工序（A）具有至少一个可水解基团和能够与金属基表面活性剂相互作用的催化剂，其中有机溶剂溶液中的水含量被设定或保持在预定范围内。

8. 发明授权

US08361375B2 Forming mold or electroforming mother die having release layer and method for manufacturing the same 有权
标题翻译：具有脱模层的成型模具或电铸母模及其制造方法
公开(公告)号：US08361375B2
公开(公告)日：2013-01-29
申请号：US13344210
申请日：2012-01-05
申请人： Tomoya Hidaka , Norifumi Nakamoto , Yoshitaka Fujita
发明人： Tomoya Hidaka , Norifumi Nakamoto , Yoshitaka Fujita
IPC分类号： B28B7/36 , B28B7/38
CPC分类号： B29C33/64 , B29C33/56 , C25D1/22
摘要： A forming mold or electroforming mother die including a mold or mother die, and a release layer composed of an organic thin film on a mold surface or mother die surface which is formed by contacting the mold or mother die with an organic solvent solution including a silane surfactant represented by formula [1] Rn—Si—X4-n [1] where R represents an optionally substituted hydrocarbon group or halogenated hydrocarbon having 1 to 20 carbon atoms, or a hydrocarbon group or a halogenated hydrocarbon group having a linking group which has 1 to 20 carbon atoms, X represents a hydroxyl group, a halogen atom, an alkoxy group having 1 to 6 carbon atoms, or an acyloxy group, and n represents an integer of 1 to 3; and a catalyst capable of interacting with the silane surfactant, and a production method thereof.
摘要翻译：包括模具或母模的成形模具或电铸母模以及由模具表面或母模表面上的有机薄膜构成的剥离层，其通过使模具或母模与包含硅烷的有机溶剂溶液接触而形成由式[1]表示的表面活性剂Rn-Si-X4-n [1]其中R表示任选取代的烃基或具有1至20个碳原子的卤代烃，或具有连接基团的烃基或卤代烃基， 1〜20个碳原子，X表示羟基，卤素原子，碳原子数1〜6的烷氧基或酰氧基，n表示1〜3的整数。和能够与硅烷表面活性剂相互作用的催化剂及其制造方法。

9. 发明授权

US07909929B2 Dispersoid having metal-oxygen bonds, metal oxide film, and monomolecular film 有权
标题翻译：具有金属氧键的分散体，金属氧化物膜和单分子膜
公开(公告)号：US07909929B2
公开(公告)日：2011-03-22
申请号：US10533580
申请日：2003-11-12
申请人： Nobuo Kimura , Yoshitaka Fujita , Norifumi Nakamoto , Motoyuki Toki , Akiji Higuchi , Kazuo Ono , Tomoya Hidaka , Hiroyuki Takeda
发明人： Nobuo Kimura , Yoshitaka Fujita , Norifumi Nakamoto , Motoyuki Toki , Akiji Higuchi , Kazuo Ono , Tomoya Hidaka , Hiroyuki Takeda
IPC分类号： C01G23/047
CPC分类号： C01B13/32 , C01G23/053 , C23C18/1216 , C23C18/122 , Y10T428/24355
摘要： The invention provides dispersoids having metal-oxygen groups which are suitable for the production of metal oxide thin-films at a low temperature of 200° C. or below and for the production of homogeneous organic-inorganic hybrid materials. The invention also provides metal oxide thin-films and organic-inorganic hybrid materials endowed with various capabilities, particularly organic-inorganic hybrid materials having a high refractive index and high transparency. Use is made of a dispersoid having metal-oxygen bonds which is obtained by mixing a metal compound having at least three hydrolyzable groups with at least 0.5 mole but less than 2 moles of water per mole of the metal compound in an organic solvent, in the absence of an acid, a base and/or a dispersion stabilizer, and at a temperature at or below the temperature at which the metal compound begins to hydrolyze, then raising the temperature to at least the temperature at which hydrolysis begins.
摘要翻译：本发明提供了适用于在200℃或更低的低温下生产金属氧化物薄膜的金属 - 氧基分散体和用于生产均相有机 - 无机混合材料的分散体。本发明还提供具有各种能力的金属氧化物薄膜和有机 - 无机混合材料，特别是具有高折射率和高透明度的有机 - 无机混合材料。使用具有金属 - 氧键的分散体，其通过在有机溶剂中将具有至少三个可水解基团的金属化合物与每摩尔金属化合物混合至少0.5摩尔但小于2摩尔水而获得，不存在酸，碱和/或分散体稳定剂，并且在金属化合物开始水解或在低于金属化合物开始水解的温度的温度下，将温度升至至少水解开始的温度。

10. 发明申请

US20080290249A1 Forming Mold Or Electroforming Mother Die Having Release Layer And Method For Manufacturing The Same 审中-公开
标题翻译：具有脱模层的成型模具或电铸母模及其制造方法
公开(公告)号：US20080290249A1
公开(公告)日：2008-11-27
申请号：US11722847
申请日：2005-12-28
申请人： Tomoya Hidaka , Norifumi Nakamoto , Yoshitaka Fujita
发明人： Tomoya Hidaka , Norifumi Nakamoto , Yoshitaka Fujita
IPC分类号： B28B7/34 , B28B7/00
CPC分类号： B29C33/64 , B29C33/56 , C25D1/22
摘要： The present invention provides a forming mold or electroforming mother die comprising a mold or mother die, and a release layer composed of an organic thin film on a mold surface or mother die surface which is formed by contacting the mold or mother die with an organic solvent solution comprising a silane surfactant represented by the formula [1] Rn—Si—X4-n [1] (wherein, R represents an optionally substituted hydrocarbon group having 1 to 20 carbon atoms, an optionally substituted halogenated hydrocarbon group having 1 to 20 carbon atom, a hydrocarbon group having a linking group which has 1 to 20 carbon atoms, or a halogenated hydrocarbon group having a linking group which has 1 to 20 carbon atoms, and X represents a hydroxyl group, a halogen atom, an alkoxy group having 1 to 6 carbon atoms, or an acyloxy group, and n represents an integer of 1 to 3), and a catalyst capable of interacting with the silane surfactant, the release layer having excellent releasing properties and abrasion resistance, and a production method thereof.
摘要翻译：本发明提供了一种成型模具或电铸母模，其包括模具或母模，以及由模具表面或母模表面上的有机薄膜组成的剥离层，其通过使模具或母模与有机溶剂接触而形成包含由式[1]表示的硅烷表面活性剂的溶液<？in-line-formula description =“In-line Formulas”end =“lead”？> Rn-Si-X4-n [1] 式（式中，R表示可以具有取代基的碳原子数1〜20的烃基，可以具有取代基的碳原子数1〜20的卤代烃基，具有碳原子数1〜20的烃基）或具有1〜20个碳原子的连接基的卤代烃基，X表示羟基，卤素原子，碳原子数为1〜6的烷氧基，或者酰氧基，n表示1〜3的整数）和催化剂其能够与硅烷表面活性剂相互作用，脱模层具有优异的脱模性和耐磨性，及其制备方法。

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