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1. 发明授权

US07619120B2 Processes for the preparation of diphenylsulfone compounds 有权
标题翻译：二苯砜化合物的制备方法
公开(公告)号：US07619120B2
公开(公告)日：2009-11-17
申请号：US10950889
申请日：2004-09-27
申请人： Kiyoshi Katsuura , Tomoya Hidaka , Yutaka Takashina , Yasuo Ohnuki
发明人： Kiyoshi Katsuura , Tomoya Hidaka , Yutaka Takashina , Yasuo Ohnuki
IPC分类号： C07C315/06
CPC分类号： C07C315/04 , C07C315/06 , C07C317/22
摘要： The present invention is to provide methods for producing highly pure 4,4′-dihydroxydiphenyl sulfone monoethers advantageously in industrial production.In a process for producing a compound represented by Formula (I) (wherein, R1 and R2 are each independently halogen, alkyl having 1 to 8 carbons or alkenyl having 2 to 8 carbons; m and n are each independently 0 or an integer of 1 to 4; and R3 is alkyl having 1 to 8 carbons, alkenyl having 2 to 8 carbons, cycloalkyl having 3 to 8 carbons or optionally substituted aralkyl), (1) a pH adjustment is carried out twice or more in the purification process, (2) an excessive amount of alkyl halide used is removed, (3) a solvent, such as water, containing 0.05 ppm or less of iron components is used, (4) tanks with corrosion-resistant layers over the inner walls are used, (6) a chelating agent is added, and (7) a means of drying with mechanical stir is applied.
摘要翻译：本发明提供在工业生产中有利地生产高纯度4,4'-二羟基二苯砜单醚的方法。在制备由式（I）表示的化合物的方法中（其中，R 1和R 2各自独立地为卤素，具有1至8个碳的烷基或具有2至8个碳的烯基; m和n各自独立地为0或整数1 至4; R3为具有1至8个碳的烷基，具有2至8个碳的烯基，3至8个碳原子的环烷基或任选取代的芳烷基），（1）在纯化过程中进行两次或更多次的pH调节（ 2）除去过量的烷基卤，（3）使用含有0.05ppm以下铁组分的溶剂如水，（4）使用内壁上具有耐腐蚀层的罐（ 6）加入螯合剂，（7）用机械搅拌干燥的方法。

2. 发明申请

US20080213494A1 Organic Thin Film Forming Method, Auxiliary Agent For Forming an Organic Thin Film, and Solution For Forming and Organic Thin Film 有权
标题翻译：有机薄膜成型方法，用于形成有机薄膜的辅助剂，以及用于形成和有机薄膜的溶液
公开(公告)号：US20080213494A1
公开(公告)日：2008-09-04
申请号：US11658108
申请日：2005-07-21
申请人： Nobuo Kimura , Yoshitaka Fujita , Tomoya Hidaka
发明人： Nobuo Kimura , Yoshitaka Fujita , Tomoya Hidaka
IPC分类号： B05D1/18
CPC分类号： B05D7/24 , B05D1/185 , B82Y30/00 , B82Y40/00 , C03C17/28 , C03C17/30 , C03C2217/76
摘要： An organic thin film forming method for forming an organic thin film on a substrate surface comprising: contacting the substrate with a solution for forming an organic thin film obtained from an auxiliary agent for forming an organic thin film obtained by mixing a metal surfactant (1) having at least one hydrolytic group and a compound capable of interacting with the metal surfactant (1), and a metal surfactant (2) having at least one hydrolytic group, in an organic solvent, wherein a solution for forming an organic thin film is used in which the moisture content has been adjusted or maintained to be within a predetermined range; and, an auxiliary agent for forming an organic thin film and a solution for forming an organic thin film used in this method.
摘要翻译：一种用于在基材表面上形成有机薄膜的有机薄膜形成方法，包括：使基材与用于形成有机薄膜的溶液接触，所述溶液由用于形成有机薄膜的辅助剂获得，所述有机薄膜通过将金属表面活性剂（1）具有至少一种水解基团和能够与金属表面活性剂（1）相互作用的化合物和在有机溶剂中具有至少一个水解基团的金属表面活性剂（2），其中使用用于形成有机薄膜的溶液其中水分含量已被调节或维持在预定范围内; 以及用于形成有机薄膜的辅助剂和用于形成用于该方法的有机薄膜的溶液。

3. 发明申请

US20060063669A1 Recording material comprising diphenyl sulfone derivative and novel diphenyl sulfone derivative compound 审中-公开
标题翻译：含二苯砜衍生物和新型二苯砜衍生物的记录材料
公开(公告)号：US20060063669A1
公开(公告)日：2006-03-23
申请号：US10532857
申请日：2003-10-27
申请人： Tomoya Hidaka , Hiroshi Fujii , Shinichi Sato
发明人： Tomoya Hidaka , Hiroshi Fujii , Shinichi Sato
IPC分类号： B41M5/24
CPC分类号： C07C317/22 , B41M5/155 , B41M5/323 , B41M5/3336
摘要： The present invention provides a recording material which has excellent background stability, specifically heat resistance and heat and humidity resistance of the background. The recording material containing a color forming dye is characterized by containing at least one kind of diphenylsulfone derivative represented by the general formula (I): (wherein R1 and R2 each represents a hydrogen atom or a C1 to C6 alkyl group, n represents an integer of 1 to 6, R3 and R4 each represents a halogen atom, a C1 to C6 alkyl group, etc., p and q each represents an integer of 0 to 4, X represents OR5 or NR6R7 wherein R5 represents a C1 to C6 alkyl group, a C1 to C6 hydroxyalkyl group, or a C1 to C6 alkoxy-C1 to C6 alkyl group, and R6 and R7 each represents a hydrogen atom, a C1 to C6 alkyl group, etc).
摘要翻译：本发明提供了具有优异的背景稳定性，特别是耐热性和背景耐热和耐湿性的记录材料。含有成色染料的记录材料的特征在于含有至少一种由通式（I）表示的二苯砜衍生物：

4. 发明申请

US20050096222A1 Phenolic compound and recording material containing the same 失效
标题翻译：酚醛化合物和含有其的记录材料
公开(公告)号：US20050096222A1
公开(公告)日：2005-05-05
申请号：US10507781
申请日：2003-03-13
申请人： Tomoya Hidaka , Tadashi Kawakami
发明人： Tomoya Hidaka , Tadashi Kawakami
IPC分类号： G11B7/244 , B41M5/30 , B41M5/333 , C07C317/22 , C07C317/44 , C07C323/22 , C07C323/52 , C07C323/60 , C07C327/28 , C07C333/08 , C07C335/26 , C07C335/42 , G11B7/245 , G11B7/246 , B41M5/20
CPC分类号： B41M5/3336 , B41M5/155 , B41M5/3335 , C07C317/22 , C07C317/44 , C07C323/52 , C07C323/60 , C07C327/28 , C07C333/08 , G11B7/244 , G11B7/245
摘要： An object of the present invention is to provide a novel phenolic compound, and a recording material containing the same, which is excellent in storage stability. The object can be achieved by a phenolic compound represented by the formula (I): [wherein m represents an integer of 0 to 2; R1 and R2 each independently represents a C1-C6 alkyl group or a C1-C6 alkoxy group; p and q each independently represents an integer of 0 to 4; t and u each independently represents 0 or 1 and do not simultaneously represent 0; and X represents a group represented by any of the formulas (II) to (VII): (wherein R3, R4, R5, R6, R7, R8, R9, R10 and R11 each independently represents a hydrogen atom or a C1-C6 alkyl group; a represents an integer of 1 to 6; b represents an integer of 0 to 4; and c represents an integer of 0 to 6)] and a recording material containing the same.
摘要翻译：本发明的目的是提供一种新型酚类化合物及含有该酚类化合物的记录材料，其储存稳定性优异。该目的可以通过式（I）表示的酚类化合物来实现：[其中m表示0〜2的整数， R 1和R 2各自独立地表示C 1 -C 6烷基或C 1 -C 6烷氧基; p和q各自独立地表示0〜4的整数; t和u各自独立地表示0或1并且不同时表示0; 并且X表示由式（II）至（VII）中的任一个表示的基团：其中R 3，R 4，R 5， R 6，R 7，R 8，R 9，R 10，和R 11各自独立地表示氢原子或C 1 -C 6烷基; a表示1〜6的整数; b表示0〜4的整数，c表示0〜 6）]和含有该记录材料的记录材料。

5. 发明授权

US08197906B2 Method for producing organic thin film 有权
标题翻译：有机薄膜的制造方法
公开(公告)号：US08197906B2
公开(公告)日：2012-06-12
申请号：US12777666
申请日：2010-05-11
申请人： Nobuo Kimura , Yoshitaka Fujita , Norifumi Nakamoto , Tomoya Hidaka
发明人： Nobuo Kimura , Yoshitaka Fujita , Norifumi Nakamoto , Tomoya Hidaka
IPC分类号： B05D5/00
CPC分类号： C09D5/00 , B05D1/185 , C03C17/30 , Y10T428/261 , Y10T428/31504
摘要： A method for producing an organic thin film in which an organic thin film is formed on the surface of a substrate, including a step (A) of bringing the substrate into contact with an organic solvent solution containing a metal-based surfactant having at least one hydrolysable group, and a catalyst capable of interacting with the metal-based surfactant, wherein the water contact within the organic solvent solution is either set or maintained within a predetermined range.
摘要翻译：一种制造有机薄膜的方法，其中在基材表面上形成有机薄膜，该方法包括使基材与含有至少一种金属基表面活性剂的有机溶剂溶液接触的步骤（A）可水解基团和能够与金属基表面活性剂相互作用的催化剂，其中有机溶剂溶液中的水接触被设定或保持在预定范围内。

6. 发明申请

US20100324210A1 SOLUTION FOR FORMATION OF ORGANIC THIN FILM, AND METHOD FOR PRODUCTION THEREOF 有权
标题翻译：用于形成有机薄膜的方法及其生产方法
公开(公告)号：US20100324210A1
公开(公告)日：2010-12-23
申请号：US12866899
申请日：2009-02-23
申请人： Tomoya Hidaka , Toshiaki Takahashi , Kazuhisa Kumazawa
发明人： Tomoya Hidaka , Toshiaki Takahashi , Kazuhisa Kumazawa
IPC分类号： C08K5/1535 , C08L83/06 , C08K5/1545
CPC分类号： C09D183/04 , C08G77/045 , C08G77/06 , C08G77/16 , C08G77/18 , C08G79/00 , C08G79/12 , C09D185/00 , C23C2222/20
摘要： It is to provide a solution for forming an organic metal thin film that can form rapidly a dense monomolecular film with less impurity. A solution for forming an organic thin film comprising(A) at least one organic metal compound shown by the following formula (I) (provided that at least one organic metal compound contains a hydroxyl group); and (B) at least one organic metal compound shown by the following formula (II), R3mM2X54-m (II) wherein the solution is 40≦[(A)/{(A)+(B)}]×100≦100 (mass %), and 0≦[(B)/{(A)+(B)}]×100≦60 (mass %); or a solution for forming an organic thin film comprising an organic metal compound having at least one hydroxyl group and at least one hydrolysable group among the organic metal compounds shown by the following formula (I); or a solution for forming an organic thin film wherein the mass ratio of trimer with respect to dimer is greater than 0.5 among the metal organic compound shown by formula (I).
摘要翻译：提供形成有机金属薄膜的解决方案，其可以形成快速形成较少杂质的致密单分子膜。一种形成有机薄膜的溶液，其包含（A）至少一种由下式（I）表示的有机金属化合物（条件是至少一种有机金属化合物含有羟基）; （B）至少一种下式（II）所示的有机金属化合物，其中溶液为40＆lt;（A）/ {（A）+（B）}]×100＆amp; （质量％），0＆nlE; [（B）/ {（A）+（B）}]×100＆nlE; 60（质量％）或用于形成有机薄膜的溶液，所述有机薄膜包含由下式（I）表示的有机金属化合物中具有至少一个羟基和至少一个可水解基团的有机金属化合物; 或形成有机薄膜的溶液，其中三聚物相对于二聚体的质量比在式（I）所示的金属有机化合物中大于0.5。

7. 发明申请

US20090281238A1 METHOD FOR FORMING ORGANIC THIN FILM 有权
标题翻译：形成有机薄膜的方法
公开(公告)号：US20090281238A1
公开(公告)日：2009-11-12
申请号：US12312096
申请日：2007-11-13
申请人： Tomoya Hidaka , Yoshitaka Fujita , Norifumi Nakamoto , Kazuhisa Kumazawa , Eiji Hoshi
发明人： Tomoya Hidaka , Yoshitaka Fujita , Norifumi Nakamoto , Kazuhisa Kumazawa , Eiji Hoshi
IPC分类号： C09D5/00
CPC分类号： C09D7/1233 , B05D1/185 , B05D7/24 , B05D2202/00 , B05D2203/35 , C03C17/30 , C03C2217/76 , C03C2218/113 , C08K5/01 , C08K5/04 , C08K5/05 , C08K5/5419 , C09D7/63 , C09K3/18
摘要： The object is to provide a method for forming an organic thin film which enables to form quickly a dense monomolecular film with less impurity. It is a method for forming an organic thin film which comprises:1) a step of preparing a hydroxyl group-containing solution by mixing the following (a), (b) and (c) so that the total amount of (A) and (B) in the hydroxyl group-containing solution becomes 0.1 wt % to 80 wt %, and conducting hydrolysis to generate a hydroxyl group-containing compound; a) an adjuvant for forming an organic thin film comprising a metal surfactant (A) having at least one or more hydrolysable group, and a compound (C) that can interact with the metal surfactant in an organic solvent b) a metal surfactant having at least one or more hydrolysable group (B), and c) water 2) a step of preparing a solution for forming an organic thin film by mixing an organic solvent and the hydroxyl group-containing solution obtained in the above step 1); and 3) a step of allowing the substrate to contact with the solution for forming an organic thin film obtained in the above step 2).
摘要翻译：本发明的目的是提供一种形成有机薄膜的方法，其能够快速形成具有较少杂质的致密单分子膜。形成有机薄膜的方法包括：1）通过混合以下（a），（b）和（c）制备含羟基溶液的步骤，使得（A）和含羟基溶液中的（B）成为0.1重量％〜80重量％，进行水解生成含羟基化合物; a）用于形成包含具有至少一个或多个可水解基团的金属表面活性剂（A）的有机薄膜的助剂和可在有机溶剂中与金属表面活性剂相互作用的化合物（C）b）具有至少一个或多个可水解基团（B）和c）水2）通过混合有机溶剂和在上述步骤1）中获得的含羟基溶液来制备用于形成有机薄膜的溶液的步骤; 和3）允许基板与用于形成上述步骤2）中获得的有机薄膜的溶液接触的步骤。

8. 发明授权

US06831201B2 Process for producing diphenyl sulfone compound 有权
标题翻译：二苯砜化合物的制备方法
公开(公告)号：US06831201B2
公开(公告)日：2004-12-14
申请号：US10239483
申请日：2002-09-20
申请人： Kiyoshi Katsuura , Tomoya Hidaka , Yutaka Takashina , Yasuo Ohnuki
发明人： Kiyoshi Katsuura , Tomoya Hidaka , Yutaka Takashina , Yasuo Ohnuki
IPC分类号： C07C31506
CPC分类号： C07C315/04 , C07C315/06 , C07C317/22
摘要： The present invention is to provide methods for producing highly pure 4,4′-dihydroxydiphenyl sulfone monoethers advantageously in industrial production. In a process for producing a compound represented by Formula (1) (wherein, R1 and R2 are each independently halogen, alkyl having 1 to 8 carbons or alkenyl having 2 to 8 carbons; m and n are each independently 0 or an integer of 1 to 4; and R3 is alkyl having 1 to 8 carbons, alkenyl having 2 to 8 carbons, cycloalkyl having 3 to 8 carbons or optionally substituted aralkyl), (1) a pH adjustment is carried out twice or more in the purification process, (2) an excessive amount of alkyl halide used is removed, (3) a solvent, such as water, containing 0.05 ppm or less of iron components is used, (4) tanks with corrosion-resistant layers over the inner walls are used, (6) a chelating agent is added, and (7) a means of drying with mechanical stir is applied.
摘要翻译：本发明提供了在工业生产中有利地生产高纯度4,4'-二羟基二苯基砜单醚的方法。在制备由式（1）表示的化合物（其中R 1和R 2为各自独立地为卤素，具有1至8个碳的烷基或具有2至8个碳的烯基; m和n各自独立地为0或1至4的整数;并且R 3为具有1至8个碳的烷基，具有2至 8个碳原子数为3〜8的环烷基或任意取代的芳烷基），（1）在纯化工序中进行两次以上的pH调节，（2）除去过量的烷基卤，（3）溶剂使用含有0.05ppm以下的铁成分的水，（4）使用内壁具有耐腐蚀层的罐，（6）添加螯合剂，（7）使用应用机械搅拌。

9. 发明授权

US6143060A Triazine derivatives and recording materials prepared therefrom 失效
标题翻译：三嗪衍生物及其制备的记录材料
公开(公告)号：US6143060A
公开(公告)日：2000-11-07
申请号：US68187
申请日：1998-05-01
申请人： Hiroshi Fujii , Tomoya Hidaka , Shinichi Sato , Izuo Aoki
发明人： Hiroshi Fujii , Tomoya Hidaka , Shinichi Sato , Izuo Aoki
IPC分类号： B41M5/132 , B41M5/155 , B41M5/333 , B41M5/337 , C07D251/26 , C07D251/34 , C07D251/38 , C07D251/46 , C09D11/02 , C07D251/30
CPC分类号： B41M5/3336 , B41M5/132 , B41M5/155 , B41M5/3375 , C07D251/26 , C07D251/34 , C07D251/38 , C07D251/46
摘要： Triazine derivatives of general formula (I); and recording materials excellent in the storage stability of developed images, particularly the resistance thereof to plasticizers.
摘要翻译： PCT No.PCT / JP96 / 03176 Sec。 371日期：1998年5月1日 102（e）日期1998年5月1日PCT提交1996年10月30日PCT公布。出版物WO97 / 16431 日期：1997年5月9日通式（I）的三嗪衍生物; 以及显影图像的保存稳定性优异的记录材料，特别是其对增塑剂的电阻。

10. 发明授权

US5609672A Composition for color development comprising 4-hydroxy-4'-isopropoxydiphenylsulfone, and a wet method for grinding and a dispersible solution for applying the same 失效
标题翻译：用于包含4-羟基-4'-异丙氧基二苯砜的显色组合物，以及用于研磨的湿法和用于其的可分散溶液
公开(公告)号：US5609672A
公开(公告)日：1997-03-11
申请号：US495442
申请日：1995-07-26
申请人： Tomoya Hidaka , Shinichi Sato , Hiroyasu Sato , Yutaka Takashina
发明人： Tomoya Hidaka , Shinichi Sato , Hiroyasu Sato , Yutaka Takashina
IPC分类号： B41M5/155 , B41M5/333 , C07C315/06 , C07C317/22 , C09D11/02
CPC分类号： B41M5/3336 , B41M5/155 , C07C315/06
摘要： A method for preventing the generation of the hydration of 4-hydroxy-4'-isopropoxydiphenylsulfone characterized in that the particles of 4-hydroxy-4'-isopropoxydiphenylsulfone are subjected to wet grinding in water in the presence of diphenylsulfone derivatives represented by the general formula (I); ##STR1## wherein R.sup.1 represents hydrogen or lower alkyl, R.sup.2 and R.sup.3 represent each independently lower alkyl, n and m denote 0 or an integer of from 1 to 4, with a proviso that n and m can never be 0 at the same time in case R.sup.1 represents hydrogen, is disclosed. By using the dispersible solution of color developer according to the present invention, the production of high sensitive and unclean background-free thermal sensitive recording papers can be accomplished.
摘要翻译： PCT No.PCT / JP94 / 02221 Sec。 371日期：1995年7月26日 102（e）日期1995年7月26日PCT 1994年12月26日PCT PCT。公开号WO95 / 18018 日期1995年7月6日一种防止4-羟基-4'-异丙氧基二苯基砜水合产生的方法，其特征在于在二苯基砜衍生物存在下将4-羟基-4'-异丙氧基二苯基砜的颗粒在水中进行湿磨由通式（I）表示; （I）其中R 1表示氢或低级烷基，R 2和R 3表示各自独立的低级烷基，n和m表示0或1至4的整数，条件是n和m不能为0 公开了在R1表示氢的情况下的相同时间。通过使用根据本发明的显色剂的可分散溶液，可以实现高灵敏度和不清洁的无背景的热敏记录纸的生产。

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